GB1408653A - Production of diamino-alpha,alpha,-dianthraquinonyls - Google Patents

Production of diamino-alpha,alpha,-dianthraquinonyls

Info

Publication number
GB1408653A
GB1408653A GB287473A GB287473A GB1408653A GB 1408653 A GB1408653 A GB 1408653A GB 287473 A GB287473 A GB 287473A GB 287473 A GB287473 A GB 287473A GB 1408653 A GB1408653 A GB 1408653A
Authority
GB
United Kingdom
Prior art keywords
group
primary amino
hydroxy
diamino
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB287473A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB1408653A publication Critical patent/GB1408653A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
    • C09B5/24—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position
    • C09B5/2409—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position not provided for in one of the sub groups C09B5/26 - C09B5/62
    • C09B5/2436—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position not provided for in one of the sub groups C09B5/26 - C09B5/62 only nitrogen-containing hetero rings
    • C09B5/2445—Phtaloyl isoindoles
    • C09B5/2454—5,6 phtaloyl dihydro isoindoles
    • C09B5/2463—1,3 oxo or imino derivatives
    • C09B5/2472—1,3 dioxo derivatives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D221/00—Heterocyclic compounds containing six-membered rings having one nitrogen atom as the only ring hetero atom, not provided for by groups C07D211/00 - C07D219/00
    • C07D221/02—Heterocyclic compounds containing six-membered rings having one nitrogen atom as the only ring hetero atom, not provided for by groups C07D211/00 - C07D219/00 condensed with carbocyclic rings or ring systems
    • C07D221/04—Ortho- or peri-condensed ring systems
    • C07D221/18—Ring systems of four or more rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/54—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings condensed with carbocyclic rings or ring systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/70—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings condensed with carbocyclic rings or ring systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D275/00—Heterocyclic compounds containing 1,2-thiazole or hydrogenated 1,2-thiazole rings
    • C07D275/04—Heterocyclic compounds containing 1,2-thiazole or hydrogenated 1,2-thiazole rings condensed with carbocyclic rings or ring systems
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/005—Di-anthraquinonyl and derivative compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
    • C09B5/02—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic ring being only condensed in peri position

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1408653 Preparing diamino-α,α<SP>1</SP>-dianthraquinonyls BADISCHE ANILIN- & SODAFABRIK AG 19 Jan 1973 [21 Jan 1972] 2874/73 Heading C4P Diamino α,α<SP>1</SP>-dianthraquinonyl compounds of the general formula wherein one X is primary amino and the others are H or hydroxy, one X<SP>1</SP> is primary amino and the others are H or hydroxy or in which one X or one X<SP>1</SP> forms together with the carbon atom of an adjacent anthraquinonoid keto group a fused six membered carbocyclic or five or six membered heterocyclic group and the others are H, hydroxy or primary amino including one primary amino group on each anthraquinonyl ring, and in which Y and Z are H, (R<SP>1</SP>) m wherein R<SP>1</SP> is a carbamoyl group or an N-(C 1 -C 4 alkyl)- carbamoyl group and m is 1 or a group (R<SP>2</SP>) n wherein R<SP>2</SP> is an o-dicarboximido group optionally substituted at the N atom by C 1 -C 4 alkyl or phenyl are prepared by reacting two molar parts of an aliphatic or aromatic sulphonamide with one molar part of a compound of the above formula wherein the amino groups are replaced by chlorine atoms in presence of an acid acceptor and as catalyst copper, a cupric salt, or a cuprone salt or mixture thereof to replace each chlorine atom by a sulphamoyl group which is hydrolysed to primary amino with a strong acid. The reaction preferably takes place at 150- 250‹ C. in an inert high boiling solvent using o-toluenesulphonamide, p-toluenesulphonamide or benzenesulphonamide in presence of sodium or potassium acetates or potassium carbonate as preferred acid acceptors. The hydrolysis takes place at 0-30‹ C. preferably using 88- 98% by weight sulphuric acid.
GB287473A 1972-01-21 1973-01-19 Production of diamino-alpha,alpha,-dianthraquinonyls Expired GB1408653A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19722202833 DE2202833A1 (en) 1972-01-21 1972-01-21 PROCESS FOR THE PRODUCTION OF DIAMINO ALPHA, ALPHA'-DIANTHRACHINONYLENE

Publications (1)

Publication Number Publication Date
GB1408653A true GB1408653A (en) 1975-10-01

Family

ID=5833630

Family Applications (1)

Application Number Title Priority Date Filing Date
GB287473A Expired GB1408653A (en) 1972-01-21 1973-01-19 Production of diamino-alpha,alpha,-dianthraquinonyls

Country Status (7)

Country Link
JP (1) JPS4883121A (en)
AU (1) AU467483B2 (en)
CH (1) CH572959A5 (en)
DE (1) DE2202833A1 (en)
FR (1) FR2168541B3 (en)
GB (1) GB1408653A (en)
IT (1) IT976969B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0293712A2 (en) * 1987-06-03 1988-12-07 Bayer Ag Process for the preparation of 4,4'-diamino-1,1'-dianthraquinonyl pigments

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4452741A (en) * 1981-02-09 1984-06-05 Eli Lilly And Company A-39183 Antibiotics and process for production thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0293712A2 (en) * 1987-06-03 1988-12-07 Bayer Ag Process for the preparation of 4,4'-diamino-1,1'-dianthraquinonyl pigments
EP0293712A3 (en) * 1987-06-03 1989-11-29 Bayer Ag Process for the preparation of 4,4'-diamino-1,1'-dianthraquinonyl pigments
US4969954A (en) * 1987-06-03 1990-11-13 Bayer Aktiengesellschaft Process for preparing 4,4'-diamino-1,1'-dianthraquinonyl pigments
US5078794A (en) * 1987-06-03 1992-01-07 Bayer Aktiengesellschaft Process for preparing 4,4'-diamino-1,1'-dianthraquinonyl pigments

Also Published As

Publication number Publication date
AU5115473A (en) 1974-07-18
FR2168541A1 (en) 1973-08-31
CH572959A5 (en) 1976-02-27
AU467483B2 (en) 1975-12-04
FR2168541B3 (en) 1976-01-23
JPS4883121A (en) 1973-11-06
DE2202833A1 (en) 1973-07-26
IT976969B (en) 1974-09-10

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee