GB1358846A - Probe for gyromagnetic resonance - Google Patents

Probe for gyromagnetic resonance

Info

Publication number
GB1358846A
GB1358846A GB3743170A GB3743170A GB1358846A GB 1358846 A GB1358846 A GB 1358846A GB 3743170 A GB3743170 A GB 3743170A GB 3743170 A GB3743170 A GB 3743170A GB 1358846 A GB1358846 A GB 1358846A
Authority
GB
United Kingdom
Prior art keywords
tube
joule
receiver coil
probe
thomson
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3743170A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PerkinElmer Ltd
Original Assignee
PerkinElmer Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by PerkinElmer Ltd filed Critical PerkinElmer Ltd
Priority to GB3743170A priority Critical patent/GB1358846A/en
Priority to DE19712137895 priority patent/DE2137895C3/en
Priority to FR7129025A priority patent/FR2101209B1/fr
Priority to JP5858771A priority patent/JPS5719379B1/ja
Publication of GB1358846A publication Critical patent/GB1358846A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/31—Temperature control thereof

Landscapes

  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

Abstract

1358846 Gyromagnetic resonance spectrometers PERKIN-ELMER Ltd 1 Nov 1971 [3 Aug 1970] 37431/70 Heading G1N In a variable temperature probe for nuclear magnetic resonance spectroscopy the Joule- Thomson effect is used. Working gas passes through coupling 21 and inlet tube 22, through the diffusion nozzle 5A of the Joule-Thomson cooling device 5, over an electric heater 6, flows upwardly in the annular space between the sample tube (not shown) and a glass tube 9 carrying a receiver coil 10, through apertures 3B in a plastics sleeve 3, downwardly in the annular space between tube 9 and a Dewar tube 2, spirals around heat-exchanging means 5D surrounding the Joule-Thomson device 5 and discharges to atmosphere via tube 16. A platinum temperature sensor 6C sealed in a bore in a copper bobbin 6A on which the heater coil 6B is wound is connected into a servo-loop for maintaining the temperature at a constant value. The path between the diffusion nozzle 5A and heater 6 has walls 17 of low thermal conductivity. For temperatures in the range -100‹ C to -50‹ C argon is used as the working gas. For temperatures up to 150‹ C, nitrogen is used. The Dewar tube 2 has an unmetallized window (2B) in the region of receiver coil 10 and the metallizing above and below the window is slit longitudinally in two opposite places to reduce eddy currents. The probe also includes an air turbine for sample spinning, field modulation coils 25, 26 and components 27 forming part of a receiver coil bridge.
GB3743170A 1970-08-03 1970-08-03 Probe for gyromagnetic resonance Expired GB1358846A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
GB3743170A GB1358846A (en) 1970-08-03 1970-08-03 Probe for gyromagnetic resonance
DE19712137895 DE2137895C3 (en) 1970-08-03 1971-07-29 Device for adjusting the temperature of a sample examined in a gyromagnetic resonance spectrometer
FR7129025A FR2101209B1 (en) 1970-08-03 1971-08-02
JP5858771A JPS5719379B1 (en) 1970-08-03 1971-08-03

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3743170A GB1358846A (en) 1970-08-03 1970-08-03 Probe for gyromagnetic resonance

Publications (1)

Publication Number Publication Date
GB1358846A true GB1358846A (en) 1974-07-03

Family

ID=10396437

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3743170A Expired GB1358846A (en) 1970-08-03 1970-08-03 Probe for gyromagnetic resonance

Country Status (4)

Country Link
JP (1) JPS5719379B1 (en)
DE (1) DE2137895C3 (en)
FR (1) FR2101209B1 (en)
GB (1) GB1358846A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10175311B2 (en) 2012-02-07 2019-01-08 Commissariat A L'energie Atomique Et Aux Energies Alternatives Thermal insulation device and method of operation of such a device

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111912132A (en) * 2020-06-05 2020-11-10 中国空间技术研究院 Joule-Thomson refrigerating device and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10175311B2 (en) 2012-02-07 2019-01-08 Commissariat A L'energie Atomique Et Aux Energies Alternatives Thermal insulation device and method of operation of such a device

Also Published As

Publication number Publication date
DE2137895A1 (en) 1972-02-17
FR2101209A1 (en) 1972-03-31
DE2137895C3 (en) 1981-02-19
DE2137895B2 (en) 1980-05-14
FR2101209B1 (en) 1973-06-29
JPS5719379B1 (en) 1982-04-22

Similar Documents

Publication Publication Date Title
US3525928A (en) Temperature variable sample apparatus for nmr analysis
GB1472183A (en) Refrigeration transfer apparatus
GB1422445A (en) Cryogenic surgical apparatus
US3810254A (en) Thermostatic system for nuclear gyromagnetic resonance spectroscopic permanent magnet apparatus
US20050202976A1 (en) Apparatus for use in nmr system
JPH03245504A (en) Magnet for critical magnetic field measuring device
US3412320A (en) Cryostat having an effective heat exchanger for cooling its input leads and other leak paths
US4794230A (en) Low-pressure water-cooled inductively coupled plasma torch
Osgood et al. Nuclear Cooling Applied to Measurements in He 3
GB1358846A (en) Probe for gyromagnetic resonance
US3805589A (en) Quenching dilatometer
CN110174630A (en) A kind of HIGH-TEMPERATURE NMR PROBE and system
US3805883A (en) Probe for gyromagnetic resonance spectroscopy
Hansen et al. A gas-flow system for control of the temperature of an electron paramagnetic resonance sample at temperatures between 80 and 273 degrees Kelvin
US3395565A (en) Gauge calibration by diffusion
Kamei Absorption Type 1H-{14N} Double Resonance Spectrometer
CN109212442A (en) The NMR of lower part insertion piece with multi-piece type pops one's head in
Ryan Rotating sample method for measuring the Hall mobility
Hensel et al. A pulsed nuclear magnetic resonance thermometer for use below 100 mK
Kharkovski et al. Nonadiabatic heat-capacity measurements using a superconducting quantum interference device magnetometer
MacDonald et al. Apparatus for Measuring the Temperature Dependence of Photo‐Hall Effects in High‐Resistivity Photoconductors
FR2417734A1 (en) Cryostat for superconducting coil - in which several concentric radiation shields with liq. nitrogen surround central liq. helium chamber
Anisimov et al. Thermostatic control of a sample tube in a nuclear magnetic resonance spin-echo spectrometer
Schmitz et al. Probe Cryostat to Fit He Supply Dewar
Hensel The nuclear refrigeration of copper

Legal Events

Date Code Title Description
PS Patent sealed
PE20 Patent expired after termination of 20 years