GB1342045A - Process for producing nitrilotriacetonitrile - Google Patents

Process for producing nitrilotriacetonitrile

Info

Publication number
GB1342045A
GB1342045A GB270072A GB270072A GB1342045A GB 1342045 A GB1342045 A GB 1342045A GB 270072 A GB270072 A GB 270072A GB 270072 A GB270072 A GB 270072A GB 1342045 A GB1342045 A GB 1342045A
Authority
GB
United Kingdom
Prior art keywords
nitrilotriacetonitrile
weight
jan
reaction mixture
final reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB270072A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of GB1342045A publication Critical patent/GB1342045A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00Carboxylic acid nitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1342045 Nitrilotriacetonitrile MONSANTO CO 20 Jan 1972 [21 Jan 1971] 2700/72 Heading C2C Nitrilotriacetonitrile is produced by reacting together hydrocyanic acid, formaldehyde and a nitrogen source in an acidic liquid medium containing less than 5 equivalents of acid per litre, using the stoichiometric amounts (Œ2% by weight) of CH 2 O and HCN required to react with the nitrogen source, controlling the amount of liquid present in the final reaction mixture at 50-65% by weight, based on the total weight thereof, and maintaining the temperature of the final reaction mixture at 75- 95‹ C. Preferred nitrogen sources are hexamethylenetetramine, NH 3 , a soluble ammonium salt and an aminoacetonitrile intermediate.
GB270072A 1971-01-21 1972-01-20 Process for producing nitrilotriacetonitrile Expired GB1342045A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10860371A 1971-01-21 1971-01-21

Publications (1)

Publication Number Publication Date
GB1342045A true GB1342045A (en) 1973-12-25

Family

ID=22323106

Family Applications (1)

Application Number Title Priority Date Filing Date
GB270072A Expired GB1342045A (en) 1971-01-21 1972-01-20 Process for producing nitrilotriacetonitrile

Country Status (2)

Country Link
BE (1) BE778280A (en)
GB (1) GB1342045A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1983004020A1 (en) * 1982-05-18 1983-11-24 Cemona Ag Method for the preparation of amino-cetonitriles

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1983004020A1 (en) * 1982-05-18 1983-11-24 Cemona Ag Method for the preparation of amino-cetonitriles

Also Published As

Publication number Publication date
BE778280A (en) 1972-07-20

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees