GB1337377A - Process for the preparation of ethyl 8-hydroxy-1,3-dioxolo - Google Patents

Process for the preparation of ethyl 8-hydroxy-1,3-dioxolo

Info

Publication number
GB1337377A
GB1337377A GB2984772A GB2984772A GB1337377A GB 1337377 A GB1337377 A GB 1337377A GB 2984772 A GB2984772 A GB 2984772A GB 2984772 A GB2984772 A GB 2984772A GB 1337377 A GB1337377 A GB 1337377A
Authority
GB
United Kingdom
Prior art keywords
mixture
dioxolo
hydroxy
ethyl
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2984772A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Warner Lambert Co LLC
Original Assignee
Warner Lambert Co LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Warner Lambert Co LLC filed Critical Warner Lambert Co LLC
Publication of GB1337377A publication Critical patent/GB1337377A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D491/00Heterocyclic compounds containing in the condensed ring system both one or more rings having oxygen atoms as the only ring hetero atoms and one or more rings having nitrogen atoms as the only ring hetero atoms, not provided for by groups C07D451/00 - C07D459/00, C07D463/00, C07D477/00 or C07D489/00
    • C07D491/02Heterocyclic compounds containing in the condensed ring system both one or more rings having oxygen atoms as the only ring hetero atoms and one or more rings having nitrogen atoms as the only ring hetero atoms, not provided for by groups C07D451/00 - C07D459/00, C07D463/00, C07D477/00 or C07D489/00 in which the condensed system contains two hetero rings
    • C07D491/04Ortho-condensed systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D317/00Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/44Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D317/46Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
    • C07D317/48Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
    • C07D317/62Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to atoms of the carbocyclic ring
    • C07D317/66Nitrogen atoms not forming part of a nitro radical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Quinoline Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

1337377 Dioxoloquinoline carboxylic acid ester preparation WARNER LAMBERT CO 26 June 1972 [20 July l9 29847/72 Heading C2C Ethyl 8 - hydroxy - 1,3 - dioxolo[4,5-g]- quinoline-7-carboxylate is prepared by (a) reacting ethanol and P 2 O 5 in xylene at below 120‹ C.; (b) adding diethyl (3,4-methylenedioxyphenyl)-aminomethylene malonate; (c) heating the mixture at 138-140‹ C. for one hour; (d) cooling the mixture; (e) pouring the mixture into a base and (f) recovering the precipitate.
GB2984772A 1971-07-20 1972-06-26 Process for the preparation of ethyl 8-hydroxy-1,3-dioxolo Expired GB1337377A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US16445171A 1971-07-20 1971-07-20

Publications (1)

Publication Number Publication Date
GB1337377A true GB1337377A (en) 1973-11-14

Family

ID=22594538

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2984772A Expired GB1337377A (en) 1971-07-20 1972-06-26 Process for the preparation of ethyl 8-hydroxy-1,3-dioxolo

Country Status (8)

Country Link
AU (1) AU466435B2 (en)
CA (1) CA966135A (en)
DE (1) DE2227743C3 (en)
FI (1) FI50973C (en)
FR (1) FR2146779A5 (en)
GB (1) GB1337377A (en)
NO (1) NO134987C (en)
SE (1) SE394437B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4284777A (en) * 1978-12-26 1981-08-18 E. I. Du Pont De Nemours And Company Antibacterials: 1-difluoromethyl-6,7-methylenedioxy-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid and its esters

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4284777A (en) * 1978-12-26 1981-08-18 E. I. Du Pont De Nemours And Company Antibacterials: 1-difluoromethyl-6,7-methylenedioxy-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid and its esters

Also Published As

Publication number Publication date
DE2227743A1 (en) 1973-02-08
AU4441272A (en) 1974-01-17
SE394437B (en) 1977-06-27
FR2146779A5 (en) 1973-03-02
DE2227743C3 (en) 1974-10-03
FI50973C (en) 1976-09-10
DE2227743B2 (en) 1974-02-21
NO134987B (en) 1976-10-11
AU466435B2 (en) 1975-10-30
FI50973B (en) 1976-05-31
CA966135A (en) 1975-04-15
NO134987C (en) 1977-01-19

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee