GB1276653A - Recovery of gases - Google Patents
Recovery of gasesInfo
- Publication number
- GB1276653A GB1276653A GB39734/68A GB3973468A GB1276653A GB 1276653 A GB1276653 A GB 1276653A GB 39734/68 A GB39734/68 A GB 39734/68A GB 3973468 A GB3973468 A GB 3973468A GB 1276653 A GB1276653 A GB 1276653A
- Authority
- GB
- United Kingdom
- Prior art keywords
- gas
- centrifuge
- rotor
- line
- passes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
- F25J3/0605—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the feed stream
- F25J3/062—Refinery gas, cracking gas, coke oven gas, gaseous mixtures containing aliphatic unsaturated CnHm or gaseous mixtures of undefined nature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D45/00—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
- B01D45/12—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces
- B01D45/14—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces generated by rotating vanes, discs, drums or brushes
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
- F25J3/063—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream
- F25J3/0655—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream separation of hydrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
- F25J3/063—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream
- F25J3/066—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream separation of nitrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
- F25J3/063—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream
- F25J3/0685—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream separation of noble gases
- F25J3/069—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream separation of noble gases of helium
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2200/00—Processes or apparatus using separation by rectification
- F25J2200/80—Processes or apparatus using separation by rectification using integrated mass and heat exchange, i.e. non-adiabatic rectification in a reflux exchanger or dephlegmator
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2205/00—Processes or apparatus using other separation and/or other processing means
- F25J2205/10—Processes or apparatus using other separation and/or other processing means using combined expansion and separation, e.g. in a vortex tube, "Ranque tube" or a "cyclonic fluid separator", i.e. combination of an isentropic nozzle and a cyclonic separator; Centrifugal separation
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2205/00—Processes or apparatus using other separation and/or other processing means
- F25J2205/40—Processes or apparatus using other separation and/or other processing means using hybrid system, i.e. combining cryogenic and non-cryogenic separation techniques
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2210/00—Processes characterised by the type or other details of the feed stream
- F25J2210/20—H2/N2 mixture, i.e. synthesis gas for or purge gas from ammonia synthesis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2240/00—Processes or apparatus involving steps for expanding of process streams
- F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S494/00—Imperforate bowl: centrifugal separators
- Y10S494/90—Imperforate bowl: centrifugal separators involving mixture containing one or more gases
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/902—Apparatus
- Y10S62/91—Expander
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/927—Natural gas from nitrogen
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/931—Recovery of hydrogen
- Y10S62/933—From helium
Abstract
1276653 Centrifugal separation of gases PETROCARBON DEVELOPMENTS Ltd. 19 Aug 1969 [20 Aug 1968] 39734/68 Heading B2P [Also in Division F1] Hydrogen or helium of increased purity is obtained from a gaseous mixture consisting predominantly of hydrogen or helium by introducing the gaseous mixture into the central part of a rotating gas centrifuge rotor under such conditions of temperature and pressure that the gaseous mixture is above its dew point but passes through its dew point as it is caused by centrifugal force to pass to the peripheral wall of the centrifuge rotor, the temperature being maintained substantially constant throughout the centrifuge, whereby an increase in pressure and a decrease in hydrogen or helium concentration results so that gaseous impurities are condensed and collect on the wall of the rotor and a hydrogen or helium gas stream of increased purity is recovered from the gas centrifuge. For mixtures of H 2 or He containing N 2 , and which may also contain CH 4 CO and/or A, temperatures of 64-110K and pressures of 10-50 atm. abs. may be used. The gaseous mixture may be subjected to a two-stage process in the gas centrifuge or it may first be subjected to a low temperature condensation process to increase the percentage of H 2 , or He in the mixture before centrifugation. The gas stream recovered from the centrifuge may be further purified by means of an adsorption or diffusion process. In one example of the process applied to the recovery of helium from natural gas containing He, N 2 and CH 4 , the gas is compressed and cooled in a separate plant to remove most of the CH 4 and some of the N 2 . The gas is then passed via a line 50, Fig. 2, through a heat exchanger 51 whereby the residual CH 4 and most of the N 2 are condensed. The resulting gas and liquid phases are passed by line 52 into a separator 53. The separated liquid from separator 53 passes through line 54 and expansion valve 55 to the heat exchanger 51 in which it is completely evaporated and which it leaves through line 56 to be returned to the previous separate plant. The gas phase from the separator 53 is fed via a line 57 to a centrifuge 58 driven by a gas expansion turbine 60. N 2 is liquefied in centrifuge 58 and is withdrawn from the centrifuge rotor periphery and passed through line 65 and expansion valve 66 to be mixed with the liquid from separator 53 downstream of valve 55. The temperature in the centrifuge is kept constant by controlling the pressure upstream of the valve 66. The purified He gas leaves the centrifuge through line 61, is warmed in heat exchanger 51 and passes via line 62 to the turbine 60 in which it is expanded and cooled. The cooled He gas leaves through line 63 and passes through heat exchanger 51 from which it is returned via line 64 to the previous plant. Another example applied to the recovery of hydrogen from ammonia synthesis purge gas is described. The centrifuge may be as shown in Fig. 3, its barrel-shaped rotor 34 being integral with an inward radial flow expansion gas turbine wheel 32 which drives a shaft 33 and is integral with a rotating tube 36 which carries away the exhaust gas to an outlet 37. A stationary tube 38 surrounds the tube 36 leaving an annulus through which a hydrogen-nitrogen gas mixture fed at 39 passes and enters the centrifuge rotor at 40. The light H 2 gas leaves the rotor at 41 and passes to outlet 42. The liquefied N 2 collects on the wall 43 of the centrifuge rotor and passes through openings 44 in the wall of the rotor and into the space between the rotor and a surrounding casing 45 to leave by outlet 46. The shaft 33 is connected to a compressor. Labyrinth seals are provided at 47. The bearing 49 for the tube 36 also acts as a seal. The turbine wheel 32 may be made of stainless steel or aluminium, the centrifuge rotor 35 of stainless steel and the casing 45 of aluminium.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB39734/68A GB1276653A (en) | 1968-08-20 | 1968-08-20 | Recovery of gases |
US851705A US3643452A (en) | 1968-08-20 | 1969-08-20 | Recovery of gases |
JP44065923A JPS4940788B1 (en) | 1968-08-20 | 1969-08-20 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB39734/68A GB1276653A (en) | 1968-08-20 | 1968-08-20 | Recovery of gases |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1276653A true GB1276653A (en) | 1972-06-07 |
Family
ID=10411181
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB39734/68A Expired GB1276653A (en) | 1968-08-20 | 1968-08-20 | Recovery of gases |
Country Status (3)
Country | Link |
---|---|
US (1) | US3643452A (en) |
JP (1) | JPS4940788B1 (en) |
GB (1) | GB1276653A (en) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1518372A (en) * | 1976-02-25 | 1978-07-19 | Tioxide Group Ltd | Chlorine recovery process |
US4659351A (en) * | 1986-01-29 | 1987-04-21 | Air Products And Chemicals, Inc. | Combined process to produce liquid helium, liquid nitrogen, and gaseous nitrogen from a crude helium feed |
US4701201A (en) * | 1986-09-24 | 1987-10-20 | Union Carbide Corporation | Process to produce cold helium gas for liquefaction |
US4701200A (en) * | 1986-09-24 | 1987-10-20 | Union Carbide Corporation | Process to produce helium gas |
US6716269B1 (en) * | 2002-03-05 | 2004-04-06 | Energent Corporation | Centrifuge and cascade for the separation of gases |
DE20311005U1 (en) * | 2003-07-17 | 2004-11-18 | Arvin Technologies Inc., Columbus | Assembly consisting of heat exchanger and housing, in particular for the exhaust systems of a motor vehicle |
EA007998B1 (en) * | 2003-08-06 | 2007-02-27 | Ганибал Арутюнян | Method of gas liquefaction and plant of its realization |
FR2914990B1 (en) * | 2007-04-13 | 2010-02-26 | Air Liquide | METHOD FOR COLDING A CRYOGENIC EXCHANGE LINE |
US20090068090A1 (en) * | 2007-09-06 | 2009-03-12 | Battelle Energy Alliance, Llc | Methods for reacting and separating components of a gas-phase equilibrium reaction and a centrifugal separation device for same |
CN101732884A (en) * | 2008-11-26 | 2010-06-16 | 华智系统科技股份有限公司 | Condensation device and method with high-efficiency temperature-reducing nucleation |
DE102016219850A1 (en) * | 2016-10-12 | 2018-04-12 | Thyssenkrupp Ag | Process for the separation of nitrogen from a process gas mixture |
US20210148632A1 (en) * | 2018-10-09 | 2021-05-20 | Chart Energy & Chemicals, Inc. | Dehydrogenation Separation Unit with Mixed Refrigerant Cooling |
US20220252342A1 (en) * | 2019-06-25 | 2022-08-11 | Petroliam Nasional Berhad (Petronas) | System and method for the processing of lng |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US379690A (en) * | 1888-03-20 | de layal | ||
US1124715A (en) * | 1911-11-09 | 1915-01-12 | William L D Olier | Centrifugal apparatus. |
FR602388A (en) * | 1924-11-25 | 1926-03-17 | Device for purifying lubricating and carburizing oils | |
FR704523A (en) * | 1930-01-16 | 1931-05-21 | Refrigeration appliance | |
FR697082A (en) * | 1930-06-04 | 1931-01-12 | Turbo-oil purifier for explosion or combustion engines | |
US2720313A (en) * | 1951-12-03 | 1955-10-11 | Garrett Corp | Liquid purification system |
DE1113909B (en) * | 1958-07-03 | 1961-09-14 | Karl Marx Stadt Maschf | Hydraulic braking of centrifuges and a device for braking |
FR1241864A (en) * | 1959-08-14 | 1960-09-23 | Commissariat Energie Atomique | Method and apparatus for the continuous purification of uranium hexafluoride by centrifugation and calfaction |
BE594130A (en) * | 1959-08-18 | |||
US3057167A (en) * | 1959-10-12 | 1962-10-09 | Union Carbide Corp | Process and apparatus for separating helium from helium-air mixtures |
US3205669A (en) * | 1960-08-15 | 1965-09-14 | Phillips Petroleum Co | Recovery of natural gas liquids, helium concentrate, and pure nitrogen |
US3251542A (en) * | 1963-05-29 | 1966-05-17 | Electro Nucleonics | Centrifugal separation of cryogenic gaseous mixtures |
GB1136040A (en) * | 1964-12-17 | 1968-12-11 | Petrocarbon Dev Ltd | Recovery of hydrogen from a gas mixture |
GB1057020A (en) * | 1964-12-17 | 1967-02-01 | Petrocarbon Dev Ltd | Recovery of hydrogen from a gas mixture |
US3358460A (en) * | 1965-10-08 | 1967-12-19 | Air Reduction | Nitrogen liquefaction with plural work expansion of feed as refrigerant |
-
1968
- 1968-08-20 GB GB39734/68A patent/GB1276653A/en not_active Expired
-
1969
- 1969-08-20 US US851705A patent/US3643452A/en not_active Expired - Lifetime
- 1969-08-20 JP JP44065923A patent/JPS4940788B1/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
JPS4940788B1 (en) | 1974-11-05 |
US3643452A (en) | 1972-02-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed [section 19, patents act 1949] | ||
PLNP | Patent lapsed through nonpayment of renewal fees |