GB1219852A - Production of thioamides - Google Patents
Production of thioamidesInfo
- Publication number
- GB1219852A GB1219852A GB1232568A GB1232568A GB1219852A GB 1219852 A GB1219852 A GB 1219852A GB 1232568 A GB1232568 A GB 1232568A GB 1232568 A GB1232568 A GB 1232568A GB 1219852 A GB1219852 A GB 1219852A
- Authority
- GB
- United Kingdom
- Prior art keywords
- halomethyl group
- haloalkane
- terminal
- thioamides
- march
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/10—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Hydrogenated Pyridines (AREA)
Abstract
1,219,852. Thioamides. BADISCHE ANILIN- & SODA-FABRIK A.G. 14 March, 1968 [18 March, 1967], No. 12325/68. Heading C2C. N-substituted thioamides are prepared by reacting a haloalkane having at least one terminal halomethyl group with S and a primary or secondary amine, the S being used in about the stoichiometric amount per halomethyl group. The process may involve a haloalkane having more than one terminal halomethyl group and a monoamine or a haloalkane having one terminal halomethyl group and a polyamine. An acid binding agent such as an amine, amide and other organic and inorganic bases may be present. In the examples cyclohexylamine, di-n-butylamine and piperidine are converted to (a) N-cyclohexylthioformamide; (b) N,N-dibutylthioformamide; and (c) thioacetylpiperidine respectively using methylene chloride in (a) and (b), and 1,1-dichloroethane in (c).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1967B0091670 DE1272286C2 (en) | 1967-03-18 | 1967-03-18 | Process for the preparation of N-substituted aliphatic thiocarboxamides |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1219852A true GB1219852A (en) | 1971-01-20 |
Family
ID=6985973
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1232568A Expired GB1219852A (en) | 1967-03-18 | 1968-03-14 | Production of thioamides |
Country Status (6)
Country | Link |
---|---|
BE (1) | BE712266A (en) |
CH (1) | CH485684A (en) |
DE (1) | DE1272286C2 (en) |
FR (1) | FR1556715A (en) |
GB (1) | GB1219852A (en) |
NL (1) | NL6803574A (en) |
-
1967
- 1967-03-18 DE DE1967B0091670 patent/DE1272286C2/en not_active Expired
-
1968
- 1968-03-12 CH CH361068A patent/CH485684A/en not_active IP Right Cessation
- 1968-03-13 FR FR1556715D patent/FR1556715A/fr not_active Expired
- 1968-03-13 NL NL6803574A patent/NL6803574A/xx unknown
- 1968-03-14 GB GB1232568A patent/GB1219852A/en not_active Expired
- 1968-03-15 BE BE712266D patent/BE712266A/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE1272286C2 (en) | 1969-03-06 |
NL6803574A (en) | 1968-09-19 |
DE1272286B (en) | 1968-07-11 |
FR1556715A (en) | 1969-02-07 |
BE712266A (en) | 1968-09-16 |
CH485684A (en) | 1970-02-15 |
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