GB1169523A - Apparatus and Process for Distribution Separation. - Google Patents

Apparatus and Process for Distribution Separation.

Info

Publication number
GB1169523A
GB1169523A GB53461/66A GB5346166A GB1169523A GB 1169523 A GB1169523 A GB 1169523A GB 53461/66 A GB53461/66 A GB 53461/66A GB 5346166 A GB5346166 A GB 5346166A GB 1169523 A GB1169523 A GB 1169523A
Authority
GB
United Kingdom
Prior art keywords
foam
resin
sicl
packing
fractional distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB53461/66A
Inventor
Victor Pretorius Kl Waterkloof
Hans Helmut Hahn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB1169523A publication Critical patent/GB1169523A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D69/00Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10Supported membranes; Membrane supports
    • B01D69/106Membranes in the pores of a support, e.g. polymerized in the pores or voids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0242Moving bed of solid material in towers, e.g. comprising contacting elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416Systems
    • G01N27/447Systems using electrophoresis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/34Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/38Flow patterns
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • G01N30/56Packing methods or coating methods
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/62Detectors specially adapted therefor
    • G01N30/64Electrical detectors
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/84Preparation of the fraction to be distributed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30Details relating to random packing elements
    • B01J2219/302Basic shape of the elements
    • B01J2219/30207Sphere
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32203Sheets
    • B01J2219/32206Flat sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32203Sheets
    • B01J2219/32213Plurality of essentially parallel sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32203Sheets
    • B01J2219/32224Sheets characterised by the orientation of the sheet
    • B01J2219/32227Vertical orientation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32203Sheets
    • B01J2219/32224Sheets characterised by the orientation of the sheet
    • B01J2219/32231Horizontal orientation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32286Grids or lattices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32296Honeycombs
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/32Control of physical parameters of the fluid carrier of pressure or speed
    • G01N2030/324Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • G01N30/52Physical parameters
    • G01N2030/524Physical parameters structural properties
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • G01N30/52Physical parameters
    • G01N2030/524Physical parameters structural properties
    • G01N2030/528Monolithic sorbent material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/38Flow patterns
    • G01N30/42Flow patterns using counter-current
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/38Flow patterns
    • G01N30/46Flow patterns using more than one column
    • G01N30/461Flow patterns using more than one column with serial coupling of separation columns
    • G01N30/463Flow patterns using more than one column with serial coupling of separation columns for multidimensional chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Thermal Sciences (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

1,169,523. Chromatography; fractional distillation; packing for fractionating columns. V. PRETORIUS and H. H. HAHN. 29 Nov., 1966 [8 Dec., 19651, No. 53461/66. Headings BIL, B1R and B1X. An open pore foam is used as a packing in liquid and gas chromatography and fractional distillation, and has a substantially uniform porosity at least in planes at right angles to the direction of nett flow of fluid. The foam may comprise a matrix of cured polyester or epoxy resin, cement, plaster of paris, clay, fusible resins; low-melting metals or glasses, slag, polyurethane foams, silicones, ureaformaldehyde resin, melamine formaldehyde resin, phenol or resorcinol formaldehyde foams, P.V.C. The foam may be enclosed in a skin of polyethylene P.V.C., polyamides, polyacetals, polyurethane. The foam may be surface treated with colloidal carbon, active Al 2 O 3 , silica gel, ion exchange resin, (CH 3 ) 3 SiCl, (CH 3 ) 2 SiCl 2 , waterglass.
GB53461/66A 1965-12-08 1966-11-29 Apparatus and Process for Distribution Separation. Expired GB1169523A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ZA656633 1965-12-08

Publications (1)

Publication Number Publication Date
GB1169523A true GB1169523A (en) 1969-11-05

Family

ID=25560938

Family Applications (1)

Application Number Title Priority Date Filing Date
GB53461/66A Expired GB1169523A (en) 1965-12-08 1966-11-29 Apparatus and Process for Distribution Separation.

Country Status (8)

Country Link
BE (1) BE690885A (en)
CH (1) CH507724A (en)
DE (1) DE1517944A1 (en)
FR (1) FR1506648A (en)
GB (1) GB1169523A (en)
LU (1) LU52522A1 (en)
NL (1) NL6617253A (en)
SE (1) SE348557B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007041315A2 (en) * 2005-09-29 2007-04-12 Alltech Associates Inc. Composite chromatography column
US7350427B2 (en) * 2004-05-27 2008-04-01 Gerstel Systemtechnik Gmbh & Co. Sorbent collector material based on polyorganosiloxane
CN115317944A (en) * 2022-07-29 2022-11-11 华陆工程科技有限责任公司 Separation method of organic silicon ring body mixture

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19726164A1 (en) * 1997-06-20 1998-12-24 Merck Patent Gmbh Holder for monolithic sorbents
DE102008016049A1 (en) * 2008-03-28 2009-10-01 Quadbeck-Seeger, Hans-Jürgen, Prof. Dr. For separation or cleaning actions of mixtures, in distillation systems, a foam material is used with wholly or partially open cells
DE102009009703A1 (en) 2009-02-19 2010-08-26 Andrea Claudia Walter chromatography

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7350427B2 (en) * 2004-05-27 2008-04-01 Gerstel Systemtechnik Gmbh & Co. Sorbent collector material based on polyorganosiloxane
WO2007041315A2 (en) * 2005-09-29 2007-04-12 Alltech Associates Inc. Composite chromatography column
WO2007041315A3 (en) * 2005-09-29 2007-05-24 Alltech Associates Inc Composite chromatography column
CN115317944A (en) * 2022-07-29 2022-11-11 华陆工程科技有限责任公司 Separation method of organic silicon ring body mixture
CN115317944B (en) * 2022-07-29 2023-10-20 华陆工程科技有限责任公司 Separation method of organosilicon ring body mixture

Also Published As

Publication number Publication date
LU52522A1 (en) 1967-02-07
DE1517944A1 (en) 1970-04-02
FR1506648A (en) 1967-12-22
SE348557B (en) 1972-09-04
NL6617253A (en) 1967-06-09
CH507724A (en) 1971-05-31
BE690885A (en) 1967-05-16

Similar Documents

Publication Publication Date Title
IE41958L (en) Large scale chromatography
GB1169523A (en) Apparatus and Process for Distribution Separation.
ES475385A1 (en) Neutron absorbing articlem neutron absorbing plate and use of said plate as well as method for manufacture of such article.
GB1109759A (en) Chromatography method and apparatus therefor
ES301589A1 (en) Process for purifying liquids and particulate ion exchange material used therefor
DK134749B (en) Porous silica gel particles with modified surface properties for use in chromatography.
GB1085036A (en) Chromatographic analysis
GB947988A (en) A method of producing porous vitreous mouldings
ES8501308A1 (en) Process and apparatus for the continuous manufacture of composite foam panels.
ES372246A1 (en) Vehicle decelerating means
GB1101202A (en) Manufacture of thick sheets of synthetic resin material
FR2404018A1 (en) Hardening epoxy! resin with cyanamide - used as an opt. urea-contg. aq. soln. uniformly distributed in resin
GB1447756A (en) Method and apparatus for manufacturing a stone-faced surface elemeng
JPS5251697A (en) Method of building supporting legs of spherical tank in low tmperature liquified gas carrying vessel
GB1000412A (en) Improvements in or relating to plastic printing plates
JPS55765A (en) Fire and heat resistant phenolic resin foam
ES8102863A1 (en) Process for binding aggregates using a polymerizable binder.
GB1425357A (en) Impregnated chemical separation particles
GB945274A (en) Improvements in and relating to dielectric panels
Dahiya et al. Dynamics of calcium‐sodium exchange under unsaturated plow conditions
GB980335A (en) Improvements relating to ion-exchange apparatus
SE8206774D0 (en) COMPOSITION PRODUCT INCLUDING A FIBER MATT OF WHICH ONE MAIN SURFACE IS CONNECTED WITH A LAYER OF FOAM MATERIAL, AND PROCEDURE FOR PRODUCING THEREOF
Cockey Panel method for perturbations of transonic flows with finite shocks
ES238750A1 (en) Procedure for the manufacture of laminarium or customered articles (Machine-translation by Google Translate, not legally binding)
ES448767A1 (en) Isotope separation using vibrationally excited molecules