GB1156834A - Process for the Preparation and Recovery of Monoepoxy-Butadiene. - Google Patents

Process for the Preparation and Recovery of Monoepoxy-Butadiene.

Info

Publication number
GB1156834A
GB1156834A GB3665266A GB3665266A GB1156834A GB 1156834 A GB1156834 A GB 1156834A GB 3665266 A GB3665266 A GB 3665266A GB 3665266 A GB3665266 A GB 3665266A GB 1156834 A GB1156834 A GB 1156834A
Authority
GB
United Kingdom
Prior art keywords
butadiene
monoepoxybutadiene
monoepoxy
collected
stage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3665266A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Societe Nationale des Petroles dAquitaine SA
Original Assignee
Societe Nationale des Petroles dAquitaine SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Societe Nationale des Petroles dAquitaine SA filed Critical Societe Nationale des Petroles dAquitaine SA
Publication of GB1156834A publication Critical patent/GB1156834A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings
    • C07D303/04Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)

Abstract

1,156,834. Monoepoxybutadiene. SOC. NATIONALE DES PETROLES D'AQUITAINE. 16 Aug., 1966 [22 Sept., 1965], No. 36652/66. Heading C2C. Monoepoxybutadiene is prepared and purified by mixing butadiene and a peracid with a fractionating agent comprising an alkyl carboxylic ester having a boiling point above 100‹ C. which is a solvent for, is inert to, and does not form azeotropic mixtures with, both the reactants and the products, neutralizing the product reaction mixture with a concentrated solution of an alkali or alkaline earth metal base, distilling the neutralized organic phase in two stages, the first stage comprising simple distillation by means of which a fraction rich in epoxybutadiene is collected, and the second stage comprising redistillation by means of which the fraction boiling between 68‹ and 70‹ C. is collected, consisting of substantially pure monoepoxy butadiene, and recycling the ester solvent and the unreacted material.
GB3665266A 1965-09-22 1966-08-16 Process for the Preparation and Recovery of Monoepoxy-Butadiene. Expired GB1156834A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR32229A FR1468814A (en) 1965-09-22 1965-09-22 Process for obtaining butadiene monoepoxide

Publications (1)

Publication Number Publication Date
GB1156834A true GB1156834A (en) 1969-07-02

Family

ID=8588821

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3665266A Expired GB1156834A (en) 1965-09-22 1966-08-16 Process for the Preparation and Recovery of Monoepoxy-Butadiene.

Country Status (7)

Country Link
BE (1) BE686543A (en)
DE (1) DE1295545B (en)
ES (1) ES330741A1 (en)
FR (1) FR1468814A (en)
GB (1) GB1156834A (en)
LU (1) LU51992A1 (en)
NL (1) NL6612841A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4946284B1 (en) * 1970-08-10 1974-12-09

Also Published As

Publication number Publication date
NL6612841A (en) 1967-03-23
BE686543A (en) 1967-02-15
ES330741A1 (en) 1967-06-16
FR1468814A (en) 1967-02-10
LU51992A1 (en) 1966-11-21
DE1295545B (en) 1969-05-22

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees