GB1151017A - Process and Apparatus for the Production of Metal Powders. - Google Patents

Process and Apparatus for the Production of Metal Powders.

Info

Publication number
GB1151017A
GB1151017A GB3579367A GB3579367A GB1151017A GB 1151017 A GB1151017 A GB 1151017A GB 3579367 A GB3579367 A GB 3579367A GB 3579367 A GB3579367 A GB 3579367A GB 1151017 A GB1151017 A GB 1151017A
Authority
GB
United Kingdom
Prior art keywords
metal
liquid
produce
retort
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3579367A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pfizer Inc
Original Assignee
Pfizer Inc
Charles Pfizer and Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pfizer Inc, Charles Pfizer and Co Inc filed Critical Pfizer Inc
Publication of GB1151017A publication Critical patent/GB1151017A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/12Making metallic powder or suspensions thereof using physical processes starting from gaseous material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/16Dry methods smelting of sulfides or formation of mattes with volatilisation or condensation of the metal being produced

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

1,151,017. The production of metal powder. CHAS. PFIZER & CO. Inc. Aug. 3, 1967 [Aug. 11, 1966], No. 35793/67. Heading C7X. In a process for the production of metal powder such as Mg, Ca, Sr, Ba, Zn, the metal vapour is contacted with a continuous stream of moving merit liquid at a temperature below the melting point of the metal and the entrained metal particles are removed from the liquid. As shown in Fig. 1 a metal source 1 is placed in a retort 2 contained in an electric furnace 3. The retort cover 6 is connected to retort 2 via flange 5 and a liquid inlet port 9 and exit port 10 attached to the end of the cover produce a flat liquid curtain 8. A ceramic tube 12 supported by spaces 13 protudes from the retort into the retort cover and the metal vapour from 1 is directed via the tube to the liquid curtain 8 and the metal particles formed are entrained in the liquid which flows via tank 14 to reservoir 16 and then to separation system 17 where filtering or centrifuging is carried out. The separated liquid is cooled in heat exchanger 61 and cooling coil 62 and recirculated to inlet 9. The separated metal particles are collected in storage tank 23. A vacuum pump 24 is connected to the system and the process is carried out under a vacuum of 50 microns or less. Alternatively an inert atmosphere may be used. Suitable merit liquids are low vapour pressure oils, hydrocarbons, halogenated hydrocarbons, oxygenated hydrocarbons and silicones. In an alternative arrangement the metal vapour conduit outlet may be immersed in a stirred mass of liquid. The source of the metal vapour may be a metal, an alloy or the metal ore or oxide plus a reducing agent such as Al. The following examples are specified: (a) Mixture of FeSi, CaF 2 and clolomitic quick lime to produce Mg. (b) Mg. (c) Mixture of CaO and Al to produce Ca. (d) Mixture of barium oxide and Al to produce Ba. (e) Zn. (f) Mixture of strontium oxide and Al to produce Sr.
GB3579367A 1966-08-11 1967-08-03 Process and Apparatus for the Production of Metal Powders. Expired GB1151017A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US57174966A 1966-08-11 1966-08-11

Publications (1)

Publication Number Publication Date
GB1151017A true GB1151017A (en) 1969-05-07

Family

ID=24284879

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3579367A Expired GB1151017A (en) 1966-08-11 1967-08-03 Process and Apparatus for the Production of Metal Powders.

Country Status (1)

Country Link
GB (1) GB1151017A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5654007A (en) * 1995-06-07 1997-08-05 Inhale Therapeutic Systems Methods and system for processing dispersible fine powders
CN113637866A (en) * 2021-08-09 2021-11-12 江西蓝微电子科技有限公司 Graphene bonded silver wire and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5654007A (en) * 1995-06-07 1997-08-05 Inhale Therapeutic Systems Methods and system for processing dispersible fine powders
CN113637866A (en) * 2021-08-09 2021-11-12 江西蓝微电子科技有限公司 Graphene bonded silver wire and preparation method thereof
CN113637866B (en) * 2021-08-09 2022-03-04 江西蓝微电子科技有限公司 Graphene bonded silver wire and preparation method thereof

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee