GB1100756A - Glazed refractory bodies - Google Patents

Glazed refractory bodies

Info

Publication number
GB1100756A
GB1100756A GB9338/65A GB933865A GB1100756A GB 1100756 A GB1100756 A GB 1100756A GB 9338/65 A GB9338/65 A GB 9338/65A GB 933865 A GB933865 A GB 933865A GB 1100756 A GB1100756 A GB 1100756A
Authority
GB
United Kingdom
Prior art keywords
film
coating
sio2
weight
frit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB9338/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Co
Original Assignee
Minnesota Mining and Manufacturing Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Minnesota Mining and Manufacturing Co filed Critical Minnesota Mining and Manufacturing Co
Publication of GB1100756A publication Critical patent/GB1100756A/en
Expired legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L23/00Details of semiconductor or other solid state devices
    • H01L23/12Mountings, e.g. non-detachable insulating substrates
    • H01L23/14Mountings, e.g. non-detachable insulating substrates characterised by the material or its electrical properties
    • H01L23/15Ceramic or glass substrates
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00Glass compositions
    • C03C3/04Glass compositions containing silica
    • C03C3/062Glass compositions containing silica with less than 40% silica by weight
    • C03C3/07Glass compositions containing silica with less than 40% silica by weight containing lead
    • C03C3/072Glass compositions containing silica with less than 40% silica by weight containing lead containing boron
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00Glass compositions
    • C03C3/04Glass compositions containing silica
    • C03C3/076Glass compositions containing silica with 40% to 90% silica, by weight
    • C03C3/102Glass compositions containing silica with 40% to 90% silica, by weight containing lead
    • C03C3/108Glass compositions containing silica with 40% to 90% silica, by weight containing lead containing boron
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/10Frit compositions, i.e. in a powdered or comminuted form containing lead
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/08Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on beryllium oxide
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10NELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N97/00Electric solid-state thin-film or thick-film devices, not otherwise provided for
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L2924/00Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
    • H01L2924/0001Technical content checked by a classifier
    • H01L2924/0002Not covered by any one of groups H01L24/00, H01L24/00 and H01L2224/00

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Physics & Mathematics (AREA)
  • Structural Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Power Engineering (AREA)
  • Computer Hardware Design (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Glass Compositions (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

A fired beryllia ceramic film has on at least one surface a glaze coating which does not soften below 700 DEG C. The film is not more than 0.1 inch thick and has a camber less than 0.004 inch/inch in any direction in the plane of the film. The coating is uniform with a weight of 0.08-0.12 g./in,2, and is substantially free of the oxides of K and Na. The surface of the coating is so smooth as to give a reading of not more than 1.0 micro inch (Centre Line Average) when measured with a "Tallysurf" (Registered Trade Mark) tester. The coefficient of thermal expansion of the coating is sufficiently analogous to that of the beryllia film and the adherence is so firm, that after a thermal shock test in which the article is heated to 550 DEG C., cooled to 23 DEG C. in 20 minutes, immersed in liquid nitrogen at -210 DEG C., and then allowed to come to equilibrium at room temperature, no visible defects in the coating or article develop. Tantalum may be sputtered on the glazed film for production of a component for an electric circuit. The beryllia film contains at least 98% BeO by weight, and may also contain, e.g. SiO2, manganese oxide and alkaline earth oxides. An example of the composition is in per cent by wt., BeO, 99.5; MgO, 0.40; Al2O3, 0.075; SiO2, 0.025. Raw material is ball-milled with an organic binder, and the slip is then de-aired and applied to a smooth carrier, e.g. "Cellophane" (Registered Trade Mark) as a coating of uniform thickness and density. Volatile vehicle is then removed, e.g. by heated forced air drying. The green film may then be stamped with score lines or holes for separation or perforation of the film after glazing. It is then fired at a maximum temperature of 1550 DEG C., and is thereafter cleaned. The glaze frit may comprise, by weight: PbO,20-50%; SiO2,30-60% and 10-40% of other ingredients, being: bivalent metal oxide, e.g. alkaline earth oxide, at least 5%; B2O3, at least 3%; oxides of Na and K, not more than 5% in total. To this frit may be added, e.g. 2-8% kaolin based on kaolin and frit. Based on the weight of inorganic solids, 55% water, 3% glycerine and 1.5% methyl cellulose are admixed, and the whole milled to form a slip, which may be applied, e.g. by spraying. The article is then air-dried and fired in air at 1020 DEG C. The following three frit compositions are exemplified in per cent by weight: SiO2 40.7/36.3/35.4; B2O3, 11.1/5.9/5.5; Al2O3, 3.5/4.0/4.0; PbO, 31.6/43.1/44.1; CaO, 9.8/10.4/11.0; Na2O, 1.9/-/-; K2O, 1.4/-/-; MgO, -/0.3/-. Two resulting glaze compositions are: SiO2 37.6/36.2; B2O3, 5.5/5.4; Al2O3, 6.9/4.3; PbO, 40.0/43.3; CaO, 9.7/10.8; MgO, 0.3/-.
GB9338/65A 1964-03-12 1965-03-04 Glazed refractory bodies Expired GB1100756A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US35156364A 1964-03-12 1964-03-12

Publications (1)

Publication Number Publication Date
GB1100756A true GB1100756A (en) 1968-01-24

Family

ID=23381415

Family Applications (1)

Application Number Title Priority Date Filing Date
GB9338/65A Expired GB1100756A (en) 1964-03-12 1965-03-04 Glazed refractory bodies

Country Status (3)

Country Link
JP (1) JPS4822806B1 (en)
DE (1) DE1646672A1 (en)
GB (1) GB1100756A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112679093A (en) * 2021-01-29 2021-04-20 广东宏威陶瓷实业有限公司 Novel glazed tile and preparation method thereof
CN112851303A (en) * 2021-01-22 2021-05-28 福建省德化县宝瑞陶瓷有限公司 Low-temperature lightweight high-strength household porcelain and preparation method thereof

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112830766B (en) * 2021-01-22 2022-06-07 福建省德化县宝瑞陶瓷有限公司 Low-temperature once-fired daily ceramic product and processing technology thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112851303A (en) * 2021-01-22 2021-05-28 福建省德化县宝瑞陶瓷有限公司 Low-temperature lightweight high-strength household porcelain and preparation method thereof
CN112851303B (en) * 2021-01-22 2022-06-07 福建省德化县宝瑞陶瓷有限公司 Low-temperature lightweight high-strength household porcelain and preparation method thereof
CN112679093A (en) * 2021-01-29 2021-04-20 广东宏威陶瓷实业有限公司 Novel glazed tile and preparation method thereof
CN112679093B (en) * 2021-01-29 2022-09-20 广东宏威陶瓷实业有限公司 Novel glazed tile and preparation method thereof

Also Published As

Publication number Publication date
JPS4822806B1 (en) 1973-07-09
DE1646672A1 (en) 1971-07-22

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