GB1100748A - Process for the manufacture of a terpene derivative - Google Patents

Process for the manufacture of a terpene derivative

Info

Publication number
GB1100748A
GB1100748A GB49115/65A GB4911565A GB1100748A GB 1100748 A GB1100748 A GB 1100748A GB 49115/65 A GB49115/65 A GB 49115/65A GB 4911565 A GB4911565 A GB 4911565A GB 1100748 A GB1100748 A GB 1100748A
Authority
GB
United Kingdom
Prior art keywords
manufacture
terpinen
terpinolene
nov
hydroperoxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB49115/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dragoco Gerberding and Co GmbH
Original Assignee
Dragoco Gerberding and Co GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dragoco Gerberding and Co GmbH filed Critical Dragoco Gerberding and Co GmbH
Publication of GB1100748A publication Critical patent/GB1100748A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
    • C07C35/08—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
    • C07C35/18—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings with unsaturation at least in the ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated

Abstract

1,100,748. Terpinen-1-ol-4. FIRMA DRAGOCO, GERBERDING & CO. G.m.b.H. 18 Nov., 1965 [13 Nov., 1965], No. 49115/65. Heading C2C. Terpinen-1-ol-4 is prepared by oxidizing terpinolene to 4 - hydroperoxy - 4 - isopropenyl - 1 - methylcyclohexene, reducing the 4-hydroperoxy group to hydroxyl and hydrogenating the isopropenyl group to isopropyl. The oxidation may be effected with a dyestuff sensitizer using up to 1 mole O 2 per mole terpinolene, the reduction with aq. Na 2 SO 3 , Ph 3 P or LiAlH 4 , and the hydrogenation with Raney Ni or Co.
GB49115/65A 1965-11-13 1965-11-18 Process for the manufacture of a terpene derivative Expired GB1100748A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DED48643A DE1235306B (en) 1965-11-13 1965-11-13 Process for the preparation of terpinen-1-ol- (4)

Publications (1)

Publication Number Publication Date
GB1100748A true GB1100748A (en) 1968-01-24

Family

ID=7051326

Family Applications (1)

Application Number Title Priority Date Filing Date
GB49115/65A Expired GB1100748A (en) 1965-11-13 1965-11-18 Process for the manufacture of a terpene derivative

Country Status (6)

Country Link
US (1) US3505412A (en)
CH (1) CH453344A (en)
DE (1) DE1235306B (en)
FR (1) FR1456297A (en)
GB (1) GB1100748A (en)
NL (1) NL6515048A (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3609197A (en) * 1968-03-08 1971-09-28 Reynolds Tobacco Co R Preparation of a terpene alcohol
US3676504A (en) * 1970-09-10 1972-07-11 Reynolds Tobacco Co R Preparation of a terepene alcohol
US4000050A (en) * 1975-02-19 1976-12-28 International Flavors & Fragrances Inc. Photochemical preparation of polycycloalkyl oxyalkanes and oxyalkenes
US4570022A (en) * 1984-01-16 1986-02-11 Union Camp Corporation Preparation of terpinen-4-ols
DE4344163A1 (en) * 1993-12-23 1995-06-29 Haarmann & Reimer Gmbh Process for the photooxidation of terpene olefins
US5894020A (en) * 1997-04-18 1999-04-13 Concha; Jose Soap composition containing antifungal agent
US6884797B2 (en) * 2001-03-30 2005-04-26 Robert F. Hofmann Targeted oxidative therapeutic formulation
CN111393345A (en) * 2020-04-09 2020-07-10 福州大学 Preparation method of limonene hydroperoxide

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2387304A (en) * 1941-10-02 1945-10-23 Hercules Powder Co Ltd Stabilization of terpene products
DE933925C (en) * 1943-12-24 1955-10-06 Guenther O Dr Phil Schenck Process for the production of pinocarveyl hydroperoxide
US2950237A (en) * 1957-11-13 1960-08-23 Monsanto Chemicals Photoxidation processes utilizing novel catalysts
FR1319202A (en) * 1961-04-07 1963-02-22 Studiengesellschaft Kohle Mbh Process for preparing oxidation products from unsaturated compounds

Also Published As

Publication number Publication date
CH453344A (en) 1968-06-14
DE1235306B (en) 1967-03-02
NL6515048A (en) 1967-05-16
FR1456297A (en) 1966-10-21
US3505412A (en) 1970-04-07

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