GB1072816A - Improved dry granular products and method of manufacture thereof - Google Patents

Improved dry granular products and method of manufacture thereof

Info

Publication number
GB1072816A
GB1072816A GB31481/65A GB3148165A GB1072816A GB 1072816 A GB1072816 A GB 1072816A GB 31481/65 A GB31481/65 A GB 31481/65A GB 3148165 A GB3148165 A GB 3148165A GB 1072816 A GB1072816 A GB 1072816A
Authority
GB
United Kingdom
Prior art keywords
lactose
particles
granules
solid particles
liquid medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB31481/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Foremost Dairies Inc
Original Assignee
Foremost Dairies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Foremost Dairies Inc filed Critical Foremost Dairies Inc
Publication of GB1072816A publication Critical patent/GB1072816A/en
Expired legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/40—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
    • A23L3/46—Spray-drying
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08—Concentrating or drying of juices
    • A23L2/10—Concentrating or drying of juices by heating or contact with dry gases
    • A23L2/102—Spray-drying
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/20—Agglomerating; Granulating; Tabletting
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/20—Pills, tablets, discs, rods
    • A61K9/2004—Excipients; Inactive ingredients
    • A61K9/2013—Organic compounds, e.g. phospholipids, fats
    • A61K9/2018—Sugars, or sugar alcohols, e.g. lactose, mannitol; Derivatives thereof, e.g. polysorbates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/28—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using special binding agents
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K5/00—Lactose

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Nutrition Science (AREA)
  • Epidemiology (AREA)
  • Medicinal Chemistry (AREA)
  • Biochemistry (AREA)
  • Biophysics (AREA)
  • Molecular Biology (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Seasonings (AREA)

Abstract

Dry sperical-shaped granules each consist essentially of a plurality of smaller indiivdual solid particles that are dispersible in a liquid medium, the particles are bonded together by a dispersible medium to form the larger spherical granules, the solid particles comprising the major part of each granule, and the granules are free-flowing and relatively rapidly dispersible in the liquid medium. The granules are produced by forming a slurry consisting essentially of small solid particles of material dispersible in a liquid medium together with a liquid medium containing a binding agent, atomizing the slurry to form atomized droplets, the droplets each having a plurality of the particles included therein, and causing the droplets to be dispersed in hot drying gas to convert them to dry spherical-shaped granules, the binding agent serving to bond the solid particles together in the dry spherical-shaped granules. Pressure spray and centrifugal atomizing systems may be employed. For the drying, the inlet gas temperature may range from 300 DEG to 400 DEG F. Particles: lactose, sucrose, dextrose, maltose and corn syrup solids; fumaric, citric, malic, maleic and adipic acids; mannitol; finely-divided cellulose; and sodium silicate. The binding agent in the aqueous medium may be in solution or dispersion and may differ from or be the same material as that forming the solid particles e.g. the native syrup of the material. Binding agents: lactose or glucose, gums, and proteins and starches or their derivatives. The slurry may be formed by crystallization of solid particles from a super-saturated solution in conjunction with agitation to control the size of the particles, or by introducing and inter-mixing ground solid particles with a liquid medium before the atomization. The bulk density of a product may be reduced by introducing small amounts of gas into the slurry being supplied to the atomizer. The slurry may consist essentially of solid lactose particles of 1-100 microns size, the liquid medium being water containing dissolved lactose, and the granules produced by the atomization and drying may have a size of the order 80-400 microns, the bonding consisting of lactose in glass form. If the glass content of the granular particles causes the product to be undesirably hygroscopic, a sufficient portion of the glass lactose may be crystallized, so as to render the product non-hygroscopic, by exposure to warm humidified air and redrying. Examples are directed to producing granules from: (1) crude lactose manufactured from whey and containing 99.25% lactose, 0.4% free moisture, 0.3% ash and 0.05% protein nitrogen, employing a centrifugal atomizer operating at a peripheral speed of 450 feet per second and air at a temperature of 325 DEG F.; fumaric acid with dioctyl sodium sulphosuccinate as a wetting agent and (optionally) lactose or glucose for bonding, employing a centrifugal atomizer operating at a peripheral speed of 7540 r.p.m. and air at a temperature of 310-325 DEG F.
GB31481/65A 1964-09-02 1965-07-23 Improved dry granular products and method of manufacture thereof Expired GB1072816A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US39387764A 1964-09-02 1964-09-02

Publications (1)

Publication Number Publication Date
GB1072816A true GB1072816A (en) 1967-06-21

Family

ID=23556611

Family Applications (1)

Application Number Title Priority Date Filing Date
GB31481/65A Expired GB1072816A (en) 1964-09-02 1965-07-23 Improved dry granular products and method of manufacture thereof

Country Status (5)

Country Link
JP (1) JPS4841539B1 (en)
BE (1) BE668167A (en)
DE (1) DE1542130C3 (en)
GB (1) GB1072816A (en)
NL (2) NL6510689A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1064990A1 (en) * 1999-06-29 2001-01-03 Aeromatic-Fielder AG A process for granulation of a particulate material
CN111643487A (en) * 2020-06-12 2020-09-11 苏州大学 Lactose microsphere and preparation method thereof

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1373167A (en) * 1972-01-26 1974-11-06 Ici Ltd Manufacture of dyestuff powder
DE4119306C2 (en) * 1991-06-12 1996-05-30 Wheli Inter Ag Organic raw materials, intermediate and end products for nutrition and for use for technical purposes that contain vital substances

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1064990A1 (en) * 1999-06-29 2001-01-03 Aeromatic-Fielder AG A process for granulation of a particulate material
CN111643487A (en) * 2020-06-12 2020-09-11 苏州大学 Lactose microsphere and preparation method thereof

Also Published As

Publication number Publication date
BE668167A (en) 1965-12-01
DE1542130B2 (en) 1977-12-15
JPS4841539B1 (en) 1973-12-07
DE1542130A1 (en) 1970-04-23
NL6510689A (en) 1966-03-03
NL136770C (en) 1972-10-16
DE1542130C3 (en) 1980-04-30

Similar Documents

Publication Publication Date Title
JP3682301B2 (en) Soluble coffee beverage products
Bhandari et al. Spray drying of food materials-process and product characteristics
US3042526A (en) Powder agglomerating method and apparatus
BRPI0010636B1 (en) process for preparing an instant enzyme formulation, instant enzyme formulation, feed charge, and use of an instant enzyme formulation
US2016592A (en) Process for stabilizing milk powder and similar colloidal products
US3918986A (en) Composite maltitol powder
GB1168692A (en) Process and Apparatus for Preparing Free-Flowing and Readily Dispersible Products from Finely Powdered Materials.
CA2000827C (en) Method for pregelatinized, spray-dried starch agglomerates
US3262788A (en) Process for aggregating difficult to aggregate particles and the product thereof
CN110478324A (en) A kind of sialic acid particle and preparation method thereof
GB1072816A (en) Improved dry granular products and method of manufacture thereof
WO2002006538A1 (en) Method of spray drying
ES2286608T3 (en) PROCEDURE FOR PREPARATION OF AGLOMERATED PRODUCTS OF ALMIDON HYDROLYSATE DEHYDRATED BY ASPERSION.
US5114726A (en) Process for preparing aspartame coated organic acid
GB1112553A (en) A process for producing crystallized granules
US4517214A (en) Sweetening composition and method
US4622227A (en) Acidulent comprising fumaric acid and dried natural juice solids
JPH0412104B2 (en)
IE44797B1 (en) Sweetening composition and method for the preparation thereof
ES269215A1 (en) Agglomerated sugar mixtures and process for preparing same
JPS59166100A (en) Heating-pressing-expansion method or drying pure sugar or starch hydrolysate for preparing free-flowing powder
US3584617A (en) Production of soft sugar
US2954306A (en) Process for agglomerating dextrose
JPH1025304A (en) Granulation and granule of powder composed of substances taken in body of animal
US3567513A (en) Process for the manufacture of a free-flowing glucose product