FR3131310B1 - Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée - Google Patents

Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée Download PDF

Info

Publication number
FR3131310B1
FR3131310B1 FR2114337A FR2114337A FR3131310B1 FR 3131310 B1 FR3131310 B1 FR 3131310B1 FR 2114337 A FR2114337 A FR 2114337A FR 2114337 A FR2114337 A FR 2114337A FR 3131310 B1 FR3131310 B1 FR 3131310B1
Authority
FR
France
Prior art keywords
aqueous
hmf
counter
extract
hydroxymethylfurfural
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2114337A
Other languages
English (en)
French (fr)
Other versions
FR3131310A1 (fr
Inventor
Marc Jacquin
Espada Pastor Maria Fernandez
Kim Larmier
Hélène Lorcet
Thi Bich Ngoc Dang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR2114337A priority Critical patent/FR3131310B1/fr
Priority to JP2024537842A priority patent/JP2024547102A/ja
Priority to PCT/EP2022/084588 priority patent/WO2023117407A1/fr
Priority to CN202280085330.8A priority patent/CN118475564A/zh
Priority to US18/723,000 priority patent/US20250051297A1/en
Priority to EP22830746.8A priority patent/EP4452960A1/fr
Publication of FR3131310A1 publication Critical patent/FR3131310A1/fr
Application granted granted Critical
Publication of FR3131310B1 publication Critical patent/FR3131310B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Furan Compounds (AREA)
FR2114337A 2021-12-23 2021-12-23 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée Active FR3131310B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR2114337A FR3131310B1 (fr) 2021-12-23 2021-12-23 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée
JP2024537842A JP2024547102A (ja) 2021-12-23 2022-12-06 高純度の5-ヒドロキシメチルフルフラール(5-hmf)水溶液の製造方法
PCT/EP2022/084588 WO2023117407A1 (fr) 2021-12-23 2022-12-06 Procédé de production d'une solution aqueuse de 5-hydroxyméthylfurfural (5-hmf) de pureté élevée
CN202280085330.8A CN118475564A (zh) 2021-12-23 2022-12-06 生产高纯度5-羟甲基糠醛(5-hmf)水溶液的方法
US18/723,000 US20250051297A1 (en) 2021-12-23 2022-12-06 Method for producing a high-purity aqueous 5-hydroxymethylfurfural (5-hmf) solution
EP22830746.8A EP4452960A1 (fr) 2021-12-23 2022-12-06 Procédé de production d'une solution aqueuse de 5-hydroxyméthylfurfural (5-hmf) de pureté élevée

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2114337 2021-12-23
FR2114337A FR3131310B1 (fr) 2021-12-23 2021-12-23 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée

Publications (2)

Publication Number Publication Date
FR3131310A1 FR3131310A1 (fr) 2023-06-30
FR3131310B1 true FR3131310B1 (fr) 2023-12-01

Family

ID=80786623

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2114337A Active FR3131310B1 (fr) 2021-12-23 2021-12-23 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée

Country Status (6)

Country Link
US (1) US20250051297A1 (https=)
EP (1) EP4452960A1 (https=)
JP (1) JP2024547102A (https=)
CN (1) CN118475564A (https=)
FR (1) FR3131310B1 (https=)
WO (1) WO2023117407A1 (https=)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2669635B1 (fr) 1990-11-22 1994-06-10 Furchim Procede de fabrication d'hydroxymethylfurfural (hmf) du purete elevee.
EP1834950A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
FR3071172B1 (fr) * 2017-09-18 2019-10-04 IFP Energies Nouvelles Procede de separation des composes furaniques, en particulier le 5- hydroxymethylfurfural, du dimethoxysulfoxyde par des extractions liquide-liquide

Also Published As

Publication number Publication date
US20250051297A1 (en) 2025-02-13
CN118475564A (zh) 2024-08-09
JP2024547102A (ja) 2024-12-26
FR3131310A1 (fr) 2023-06-30
WO2023117407A1 (fr) 2023-06-29
EP4452960A1 (fr) 2024-10-30

Similar Documents

Publication Publication Date Title
Winkler et al. A highly efficient synthesis of taxanes via the tandem Diels-Alder reaction
Xu et al. Interception of benzyne with thioethers: a facile access to sulfur ylides under mild conditions
Frankowski et al. Inverting the reactivity of troponoid systems in enantioselective higher-order cycloaddition
FR3131310B1 (fr) Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF) de pureté élevée
Peng et al. Direct transition-metal-free intramolecular C–O bond formation: Synthesis of benzoxazole derivatives
MX2018006741A (es) Proceso para produccion de acido 2,5-furandicarboxilico (fdca).
Borrel et al. Azido-alkynylation of alkenes through radical-polar crossover
EA201991342A1 (ru) Способ получения hmf
US10508112B2 (en) Intermediate compounds for preparation of praziquantel and processes for preparing the intermediate compounds
CA3156015A1 (en) METHOD FOR OBTAINING A LIGNIN OIL COMPOSITION USING A COMPRESSED GAS AND ACID-ASSISTED METHOD
MY208992A (en) Recovery of water-free methanesulfonic acid from the bottom stream of a distillation column
Wu et al. A versatile and practical method for regioselective synthesis of polysubstituted furanonaphthoquinones
AR098053A1 (es) Proceso para la síntesis industrial de lurasidona
Rodrigues Jr et al. 1, 1′-Carbonyldiimidazole mediates the synthesis of N-substituted imidazole derivatives from Morita–Baylis–Hillman adducts
Liu et al. 2-Chlorotetrafluoroethanesulfinamide induced asymmetric vinylogous Mannich reaction
Ghorai et al. Intramolecular 1, 3-dipolar nitrone and nitrile oxide cycloaddition of 2-and 4-O-allyl and propargyl glucose derivatives: a versatile approach to chiral cyclic ether fused isoxazolidines, isoxazolines and isoxazoles
FR3086548B1 (fr) Procede de purification d'une charge hydroalcoolique comprenant de l'ethanol, de l'acetaldehyde et des impuretes
Fei et al. BINOL-phosphoric acids-catalyzed furylogous pinacol rearrangement of 1-[5-(hydroxy-diaryl-methyl)-furan-2-yl]-cyclobutanols into spiro cyclopentanones
Wang et al. Diastereoselectivity in the triethylamine-catalyzed sulfa-Michael addition of thiols to nitroalkenes: kinetic and thermodynamic control
Zhou et al. Catalyst-and additive-free Baeyer–Villiger-type oxidation of α-iodocyclopentenones to α-pyrones: using air as the oxidant
FR3143379B1 (fr) Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration
Duran-Lara et al. Studies towards the construction of quaternary indolizidines by [2, 3]-sigmatropic rearrangement cocatalyzed by ionic liquid
Dolna et al. Remotely controlled flow photo-Fries-type rearrangement of N-vinylazetidinones: an efficient route to structurally diverse 2, 3-dihydro-4-pyridones
WO2022088306A1 (zh) 一种中间体4,4-二甲基异恶唑-3-酮的制备方法
SA520412074B1 (ar) طريقة ونظام لإنتاج إيبوكسي ألكان

Legal Events

Date Code Title Description
PLFP Fee payment

Year of fee payment: 2

PLSC Publication of the preliminary search report

Effective date: 20230630

PLFP Fee payment

Year of fee payment: 3

PLFP Fee payment

Year of fee payment: 4

PLFP Fee payment

Year of fee payment: 5