FR3060558B1 - PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS - Google Patents

PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS Download PDF

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Publication number
FR3060558B1
FR3060558B1 FR1662968A FR1662968A FR3060558B1 FR 3060558 B1 FR3060558 B1 FR 3060558B1 FR 1662968 A FR1662968 A FR 1662968A FR 1662968 A FR1662968 A FR 1662968A FR 3060558 B1 FR3060558 B1 FR 3060558B1
Authority
FR
France
Prior art keywords
separation steps
improved separation
producing butadiene
butadiene
ethanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1662968A
Other languages
French (fr)
Other versions
FR3060558A1 (en
Inventor
Beatrice Fischer
Rejane Dastillung
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Michelin Recherche et Technique SA Switzerland
Compagnie Generale des Etablissements Michelin SCA
IFP Energies Nouvelles IFPEN
Michelin Recherche et Technique SA France
Original Assignee
Michelin Recherche et Technique SA Switzerland
Compagnie Generale des Etablissements Michelin SCA
IFP Energies Nouvelles IFPEN
Michelin Recherche et Technique SA France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Michelin Recherche et Technique SA Switzerland, Compagnie Generale des Etablissements Michelin SCA, IFP Energies Nouvelles IFPEN, Michelin Recherche et Technique SA France filed Critical Michelin Recherche et Technique SA Switzerland
Priority to FR1662968A priority Critical patent/FR3060558B1/en
Priority to PCT/EP2017/083070 priority patent/WO2018114694A1/en
Publication of FR3060558A1 publication Critical patent/FR3060558A1/en
Application granted granted Critical
Publication of FR3060558B1 publication Critical patent/FR3060558B1/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C07C45/292—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups with chromium derivatives
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/22—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by decomposition of gaseous or liquid organic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/52—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with liquids; Regeneration of used liquids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/207—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms from carbonyl compounds
    • C07C1/2072—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms from carbonyl compounds by condensation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/10—Purification; Separation; Use of additives by extraction, i.e. purification or separation of liquid hydrocarbons with the aid of liquids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0415—Purification by absorption in liquids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C01B2203/1076—Copper or zinc-based catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1217—Alcohols
    • C01B2203/1229—Ethanol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2523/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
    • C07C2523/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals
    • C07C2523/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals combined with metals, oxides or hydroxides provided for in groups C07C2523/02 - C07C2523/36
    • C07C2523/56—Platinum group metals
    • C07C2523/64—Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tatalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • C07C2523/648—Vanadium, niobium or tantalum
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne l'utilisation d'une colonne à cloison pour séparer une charge comprenant de l'éthanol, de l'acétaldéhyde, du butadiène et de l'eau ainsi qu'un procédé de production de butadiène à partir d'éthanol mettant en œuvre des étapes de séparation comprenant des colonnes à cloison.The invention relates to the use of a bulkhead column for separating a feedstock comprising ethanol, acetaldehyde, butadiene and water and a process for the production of butadiene from ethanol implementing separation steps comprising partition columns.

FR1662968A 2016-12-21 2016-12-21 PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS Expired - Fee Related FR3060558B1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
FR1662968A FR3060558B1 (en) 2016-12-21 2016-12-21 PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS
PCT/EP2017/083070 WO2018114694A1 (en) 2016-12-21 2017-12-15 Butadiene production method comprising improved separation steps

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1662968 2016-12-21
FR1662968A FR3060558B1 (en) 2016-12-21 2016-12-21 PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS

Publications (2)

Publication Number Publication Date
FR3060558A1 FR3060558A1 (en) 2018-06-22
FR3060558B1 true FR3060558B1 (en) 2019-05-24

Family

ID=58645159

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1662968A Expired - Fee Related FR3060558B1 (en) 2016-12-21 2016-12-21 PROCESS FOR PRODUCING BUTADIENE COMPRISING IMPROVED SEPARATION STEPS

Country Status (2)

Country Link
FR (1) FR3060558B1 (en)
WO (1) WO2018114694A1 (en)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19617210A1 (en) 1996-04-30 1997-11-06 Basf Ag Partition wall column for the continuous separation of multi-component mixtures by distillation
DE10056841A1 (en) * 2000-11-16 2002-05-23 Basf Ag Distillation purification of butadiene comprises using single partitioned column
US20150166445A1 (en) * 2012-06-05 2015-06-18 Akzo Nobel Chemicals International B.V. Dehydration of dilutions of compounds forming an azeotrope with water
RU2678100C2 (en) * 2013-06-21 2019-01-23 Карджилл, Инкорпорейтед Dividing wall in ethanol purification process
FR3026100B1 (en) * 2014-09-19 2016-12-09 Ifp Energies Now PROCESS FOR PRODUCING BUTADIENE AND HYDROGEN FROM ETHANOL IN TWO REACTIONAL STEPS WITH LOW WATER AND ENERGY CONSUMPTION

Also Published As

Publication number Publication date
FR3060558A1 (en) 2018-06-22
WO2018114694A1 (en) 2018-06-28

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Year of fee payment: 2

PLSC Publication of the preliminary search report

Effective date: 20180622

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Year of fee payment: 3

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Effective date: 20200910