FR3033645B1 - METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS - Google Patents

METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS Download PDF

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Publication number
FR3033645B1
FR3033645B1 FR1552062A FR1552062A FR3033645B1 FR 3033645 B1 FR3033645 B1 FR 3033645B1 FR 1552062 A FR1552062 A FR 1552062A FR 1552062 A FR1552062 A FR 1552062A FR 3033645 B1 FR3033645 B1 FR 3033645B1
Authority
FR
France
Prior art keywords
quantifying
hydrate
slab
identifying
refrigerant fluids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1552062A
Other languages
French (fr)
Other versions
FR3033645A1 (en
Inventor
Mireille Cambert
Anthony Delahaye
Laurence Fournaison
Francois Mariette
Corinne Rondeau
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Institut National de Recherche en Sciences et Technologies Pour Lenvironnement et lAgriculture IRSTEA
Original Assignee
Institut National de Recherche en Sciences et Technologies Pour Lenvironnement et lAgriculture IRSTEA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institut National de Recherche en Sciences et Technologies Pour Lenvironnement et lAgriculture IRSTEA filed Critical Institut National de Recherche en Sciences et Technologies Pour Lenvironnement et lAgriculture IRSTEA
Priority to FR1552062A priority Critical patent/FR3033645B1/en
Priority to PCT/FR2016/050531 priority patent/WO2016142620A1/en
Priority to JP2017546890A priority patent/JP2018515748A/en
Publication of FR3033645A1 publication Critical patent/FR3033645A1/en
Application granted granted Critical
Publication of FR3033645B1 publication Critical patent/FR3033645B1/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/44—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
    • G01R33/448—Relaxometry, i.e. quantification of relaxation times or spin density
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/082—Measurement of solid, liquid or gas content
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/31—Temperature control thereof
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/44—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
    • G01R33/445—MR involving a non-standard magnetic field B0, e.g. of low magnitude as in the earth's magnetic field or in nanoTesla spectroscopy, comprising a polarizing magnetic field for pre-polarisation, B0 with a temporal variation of its magnitude or direction such as field cycling of B0 or rotation of the direction of B0, or spatially inhomogeneous B0 like in fringe-field MR or in stray-field imaging
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/44—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
    • G01R33/46—NMR spectroscopy
    • G01R33/4625—Processing of acquired signals, e.g. elimination of phase errors, baseline fitting, chemometric analysis

Landscapes

  • Physics & Mathematics (AREA)
  • High Energy & Nuclear Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Signal Processing (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR1552062A 2015-03-12 2015-03-12 METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS Expired - Fee Related FR3033645B1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
FR1552062A FR3033645B1 (en) 2015-03-12 2015-03-12 METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS
PCT/FR2016/050531 WO2016142620A1 (en) 2015-03-12 2016-03-08 Nmr method for the identification and quantification of the relative proportions of the different crystallised fractions present in a hydrate slurry, and use thereof for coolants
JP2017546890A JP2018515748A (en) 2015-03-12 2016-03-08 NMR method for identifying and quantifying the relative proportions of different crystallized fractions present in hydrate slurries and its use for coolants

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1552062A FR3033645B1 (en) 2015-03-12 2015-03-12 METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS
FR1552062 2015-03-12

Publications (2)

Publication Number Publication Date
FR3033645A1 FR3033645A1 (en) 2016-09-16
FR3033645B1 true FR3033645B1 (en) 2018-10-12

Family

ID=53404699

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1552062A Expired - Fee Related FR3033645B1 (en) 2015-03-12 2015-03-12 METHOD FOR IDENTIFYING AND QUANTIFYING THE PROPORTIONS RELATING TO THE VARIOUS CRYSTALLIZED FRACTIONS PRESENT IN A HYDRATE SLAB AND ITS USE FOR REFRIGERANT FLUIDS

Country Status (3)

Country Link
JP (1) JP2018515748A (en)
FR (1) FR3033645B1 (en)
WO (1) WO2016142620A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106404610B (en) * 2016-10-20 2019-08-09 中国石油大学(北京) A kind of evaluation method of hydrate dynamic inhibitor and its application in screening
DE102018203434B4 (en) * 2018-03-07 2019-12-05 Bernd Willi Karl-Heinz Diehl Method for heteronuclear quantitative determination by NMR spectroscopy, reference substances therefor and method for determining the degree of deuteration of a deuterated compound
CN108802087A (en) * 2018-05-08 2018-11-13 中国石油大学(华东) The quantitative evaluation method of gas hydrates formation efficiency in a kind of rock based on low-field nuclear magnetic resonance
CN110702722B (en) * 2019-11-06 2021-01-19 大连理工大学 Based on nuclear magnetic resonance T2Method for calculating fractal dimension of porous medium containing hydrate by spectrum
CN111589393B (en) * 2020-05-26 2020-12-29 中国科学院西北生态环境资源研究院 Natural gas hydrate experiment reaction kettle device suitable for low-field nuclear magnetic resonance
CN114114047B (en) * 2020-08-25 2023-04-28 华为技术有限公司 Battery fault detection method and device

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007106810A2 (en) * 2006-03-13 2007-09-20 William Marsh Rice University Nmr method of detecting precipitants in a hydrocarbon stream
WO2013148516A1 (en) * 2012-03-24 2013-10-03 Weatherford/Lamb, Inc. Nuclear magnetic resonance testing for organics and fluids in source and reservoir rock

Also Published As

Publication number Publication date
WO2016142620A1 (en) 2016-09-15
FR3033645A1 (en) 2016-09-16
JP2018515748A (en) 2018-06-14

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