FR3032707B1 - Procede d'esterification d'un diol mettant en œuvre une distillation reactive - Google Patents

Procede d'esterification d'un diol mettant en œuvre une distillation reactive

Info

Publication number
FR3032707B1
FR3032707B1 FR1551354A FR1551354A FR3032707B1 FR 3032707 B1 FR3032707 B1 FR 3032707B1 FR 1551354 A FR1551354 A FR 1551354A FR 1551354 A FR1551354 A FR 1551354A FR 3032707 B1 FR3032707 B1 FR 3032707B1
Authority
FR
France
Prior art keywords
esterifying
diol
implementing
reactive distillation
distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1551354A
Other languages
English (en)
Other versions
FR3032707A1 (fr
Inventor
Romain Richard
Le Cocq Damien Leinekugel
Marc Jacquin
Margarita Dorato
Nuno Pacheco
Claire Rannoux
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Michelin Recherche et Technique SA Switzerland
Compagnie Generale des Etablissements Michelin SCA
IFP Energies Nouvelles IFPEN
Michelin Recherche et Technique SA France
Original Assignee
Michelin Recherche et Technique SA Switzerland
Compagnie Generale des Etablissements Michelin SCA
IFP Energies Nouvelles IFPEN
Michelin Recherche et Technique SA France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Michelin Recherche et Technique SA Switzerland, Compagnie Generale des Etablissements Michelin SCA, IFP Energies Nouvelles IFPEN, Michelin Recherche et Technique SA France filed Critical Michelin Recherche et Technique SA Switzerland
Priority to FR1551354A priority Critical patent/FR3032707B1/fr
Priority to US15/551,754 priority patent/US10421706B2/en
Priority to BR112017017640-8A priority patent/BR112017017640B1/pt
Priority to PCT/EP2016/053300 priority patent/WO2016131845A1/fr
Publication of FR3032707A1 publication Critical patent/FR3032707A1/fr
Application granted granted Critical
Publication of FR3032707B1 publication Critical patent/FR3032707B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/207—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms from carbonyl compounds
    • C07C1/213—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms from carbonyl compounds by splitting of esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/04—Formic acid esters
    • C07C69/08—Formic acid esters of dihydroxylic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12—Acetic acid esters
    • C07C69/16—Acetic acid esters of dihydroxylic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/22—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen having three or more carbon atoms in the acid moiety
    • C07C69/28—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen having three or more carbon atoms in the acid moiety esterified with dihydroxylic compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR1551354A 2015-02-18 2015-02-18 Procede d'esterification d'un diol mettant en œuvre une distillation reactive Active FR3032707B1 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
FR1551354A FR3032707B1 (fr) 2015-02-18 2015-02-18 Procede d'esterification d'un diol mettant en œuvre une distillation reactive
US15/551,754 US10421706B2 (en) 2015-02-18 2016-02-17 Method for esterification of a diol using a reactive distillation
BR112017017640-8A BR112017017640B1 (pt) 2015-02-18 2016-02-17 Processo de conversão alimentado por uma carga de diol compreendendo pelo menos 90% em peso de diol e uma carga de ácido carboxilíco compreendendo pelo menos 80% em peso de ácido carboxílico
PCT/EP2016/053300 WO2016131845A1 (fr) 2015-02-18 2016-02-17 Procede d'esterification d'un diol mettant en oeuvre une distillation reactive

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1551354A FR3032707B1 (fr) 2015-02-18 2015-02-18 Procede d'esterification d'un diol mettant en œuvre une distillation reactive

Publications (2)

Publication Number Publication Date
FR3032707A1 FR3032707A1 (fr) 2016-08-19
FR3032707B1 true FR3032707B1 (fr) 2017-03-10

Family

ID=53514280

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1551354A Active FR3032707B1 (fr) 2015-02-18 2015-02-18 Procede d'esterification d'un diol mettant en œuvre une distillation reactive

Country Status (4)

Country Link
US (1) US10421706B2 (fr)
BR (1) BR112017017640B1 (fr)
FR (1) FR3032707B1 (fr)
WO (1) WO2016131845A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3051467B1 (fr) * 2016-05-17 2018-06-01 IFP Energies Nouvelles Conversion du butanediol en butadiene avec lavage aux diesters
FR3057568B1 (fr) * 2016-10-14 2018-12-07 IFP Energies Nouvelles Procede de production de 1,3-butadiene et purification
CN107245035B (zh) * 2017-05-31 2020-07-07 南京威尔药业股份有限公司 一种低碳酸高沸点醇酯的清洁生产装置及使用工艺

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2224912A (en) * 1936-07-28 1940-12-17 Ici Ltd Manufacture of butadiene
FR859902A (fr) 1939-06-03 1941-01-02 Cie Nat Matieres Colorantes Procédé de préparation de butadiène
US2383205A (en) 1942-11-16 1945-08-21 Universal Oil Prod Co Manufacture of butadiene
US2372221A (en) 1943-09-14 1945-03-27 Samuel A Morell Process of acetylating 2,3-butylene glycol with the impure acetic acid obtained from the pyrolytic decomposition of 2,3-butylene glycol diacetate to butadiene
FR2044085A5 (fr) * 1969-05-08 1971-02-19 Raffinage Cie Francaise
FR2737131B3 (fr) 1995-07-24 1997-09-05 Inst Francais Du Petrole Procede et dispositif de distillation reactive avec distribution particuliere des phases liquide et vapeur
TW575557B (en) * 2001-12-05 2004-02-11 Ind Tech Res Inst Preparation method for carboxylate
CN102459138A (zh) 2009-06-04 2012-05-16 基因组股份公司 分离发酵液成分的方法
FR2957918B1 (fr) * 2010-03-25 2012-07-13 Rhodia Poliamida E Especialidades Ltda Procede d'obtention d'un ester d'acide carboxylique
AU2011320544B2 (en) 2010-10-29 2014-05-01 Lanzatech Nz, Inc. Methods and systems for the production of hydrocarbon products

Also Published As

Publication number Publication date
FR3032707A1 (fr) 2016-08-19
US10421706B2 (en) 2019-09-24
BR112017017640B1 (pt) 2021-10-26
BR112017017640A2 (pt) 2018-05-08
WO2016131845A1 (fr) 2016-08-25
US20180022682A1 (en) 2018-01-25

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