FR3021654B1 - PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID - Google Patents

PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID

Info

Publication number
FR3021654B1
FR3021654B1 FR1454830A FR1454830A FR3021654B1 FR 3021654 B1 FR3021654 B1 FR 3021654B1 FR 1454830 A FR1454830 A FR 1454830A FR 1454830 A FR1454830 A FR 1454830A FR 3021654 B1 FR3021654 B1 FR 3021654B1
Authority
FR
France
Prior art keywords
preparation
basic amino
amino acid
acid salt
acetylsalicylic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1454830A
Other languages
French (fr)
Other versions
FR3021654A1 (en
Inventor
Thierry Arnal
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unither Pharmaceuticals
Original Assignee
Unither Pharmaceuticals
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unither Pharmaceuticals filed Critical Unither Pharmaceuticals
Priority to FR1454830A priority Critical patent/FR3021654B1/en
Priority to US15/312,262 priority patent/US9745246B2/en
Priority to EP15724710.7A priority patent/EP3148961B1/en
Priority to PT15724710T priority patent/PT3148961T/en
Priority to ES15724710.7T priority patent/ES2690066T3/en
Priority to PCT/EP2015/061864 priority patent/WO2015181304A1/en
Publication of FR3021654A1 publication Critical patent/FR3021654A1/en
Application granted granted Critical
Publication of FR3021654B1 publication Critical patent/FR3021654B1/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12—Acetic acid esters
    • C07C69/14—Acetic acid esters of monohydroxylic compounds
    • C07C69/145—Acetic acid esters of monohydroxylic compounds of unsaturated alcohols
    • C07C69/157—Acetic acid esters of monohydroxylic compounds of unsaturated alcohols containing six-membered aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
FR1454830A 2014-05-28 2014-05-28 PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID Expired - Fee Related FR3021654B1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1454830A FR3021654B1 (en) 2014-05-28 2014-05-28 PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID
US15/312,262 US9745246B2 (en) 2014-05-28 2015-05-28 Method for preparing a salt of acetylsalicylic acid and a basic amino acid
EP15724710.7A EP3148961B1 (en) 2014-05-28 2015-05-28 Method for preparing a salt of acetylsalicylic acid and a basic amino acid
PT15724710T PT3148961T (en) 2014-05-28 2015-05-28 Method for preparing a salt of acetylsalicylic acid and a basic amino acid
ES15724710.7T ES2690066T3 (en) 2014-05-28 2015-05-28 Procedure for preparing an acetylsalicylic acid salt and a basic amino acid
PCT/EP2015/061864 WO2015181304A1 (en) 2014-05-28 2015-05-28 Method for preparing a salt of acetylsalicylic acid and a basic amino acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1454830A FR3021654B1 (en) 2014-05-28 2014-05-28 PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID

Publications (2)

Publication Number Publication Date
FR3021654A1 FR3021654A1 (en) 2015-12-04
FR3021654B1 true FR3021654B1 (en) 2016-06-24

Family

ID=51570555

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1454830A Expired - Fee Related FR3021654B1 (en) 2014-05-28 2014-05-28 PROCESS FOR THE PREPARATION OF AN ACETYLSALICYLIC ACID SALT AND A BASIC AMINO ACID

Country Status (6)

Country Link
US (1) US9745246B2 (en)
EP (1) EP3148961B1 (en)
ES (1) ES2690066T3 (en)
FR (1) FR3021654B1 (en)
PT (1) PT3148961T (en)
WO (1) WO2015181304A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106674036B (en) * 2016-12-22 2018-08-14 河南中医学院 The method that non-organic solvent method synthesizes di-lysine-aspirin
CA3044137C (en) 2016-12-23 2021-06-15 Ventaleon Gmbh Improved synthesis of lysine acetylsalicylate · glycine particles

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10034802A1 (en) * 2000-07-18 2002-01-31 Bayer Ag Stable salts of O-acetylsalicylic acid with basic amino acids
FR2950625B1 (en) * 2009-09-30 2016-12-02 Holis Tech PROCESS FOR PREPARING AN O-ACETYLSALICYL ACID SALT OF A BASIC AMINO ACID AND COMPOSITION OBTAINED
FR2965261B1 (en) * 2009-09-30 2012-10-26 Holis Technologies PROCESS FOR THE PREPARATION OF AN O-ACETYLSALICYLIC ACID SALT OF A BASIC AMINO ACID AND COMPOSITION OBTAINED THEREBY
FR2973370B1 (en) * 2011-03-29 2013-05-03 Holis Technologies LOW COST PROCESS FOR THE PREPARATION OF O-ACETYLSALICYCLIC ACID AND BASIC AMINO ACID
CN102503845A (en) * 2011-09-28 2012-06-20 广州普星药业有限公司 Preparation method of DL-lysine aspirin salt and application thereof
ITMI20121144A1 (en) * 2012-06-28 2013-12-29 Dipharma Francis Srl PROCEDURE FOR THE PREPARATION OF A SALT OF A NON STEROIDOUS ANTI-INFLAMMATORY MEDICINE

Also Published As

Publication number Publication date
US20170081270A1 (en) 2017-03-23
FR3021654A1 (en) 2015-12-04
ES2690066T3 (en) 2018-11-19
WO2015181304A1 (en) 2015-12-03
US9745246B2 (en) 2017-08-29
EP3148961A1 (en) 2017-04-05
EP3148961B1 (en) 2018-08-22
PT3148961T (en) 2018-11-05

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