FR2970251B1 - PROCESS FOR THE PRODUCTION OF METHYLIMINOBISDIALKYLACETAMIDE - Google Patents

PROCESS FOR THE PRODUCTION OF METHYLIMINOBISDIALKYLACETAMIDE

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Publication number
FR2970251B1
FR2970251B1 FR1250176A FR1250176A FR2970251B1 FR 2970251 B1 FR2970251 B1 FR 2970251B1 FR 1250176 A FR1250176 A FR 1250176A FR 1250176 A FR1250176 A FR 1250176A FR 2970251 B1 FR2970251 B1 FR 2970251B1
Authority
FR
France
Prior art keywords
compound
methyliminodiacetic acid
dialkylacetamide
methylimino
methylimidazole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1250176A
Other languages
French (fr)
Other versions
FR2970251A1 (en
Inventor
Yuji Sasaki
Takeshi Oriyama
Akira Ohashi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Japan Atomic Energy Agency
Original Assignee
Japan Atomic Energy Agency
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Japan Atomic Energy Agency filed Critical Japan Atomic Energy Agency
Publication of FR2970251A1 publication Critical patent/FR2970251A1/en
Application granted granted Critical
Publication of FR2970251B1 publication Critical patent/FR2970251B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Producing methylimino-N,N-dialkylacetamide compound (I) comprises mixing methyliminodiacetic acid and methylimidazole in anhydrous dichloromethane, adding p-toluenesulfonyl chloride in an ice bath to obtain an imidazole compound reacted with the methyliminodiacetic acid, as an intermediate, and adding a secondary amine to the intermediate compound. Producing methylimino-N,N-dialkylacetamide compound of formula (I) (CH 3-N(CH 2CON(R) 2) 2) (I) comprises mixing methyliminodiacetic acid and methylimidazole in anhydrous dichloromethane, adding p-toluenesulfonyl chloride in an ice bath to obtain an imidazole compound reacted with the methyliminodiacetic acid, as an intermediate, and adding a secondary amine to the intermediate compound. R : 2-12C-alkyl.
FR1250176A 2011-01-07 2012-01-06 PROCESS FOR THE PRODUCTION OF METHYLIMINOBISDIALKYLACETAMIDE Active FR2970251B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2011001809A JP5682889B2 (en) 2011-01-07 2011-01-07 Method for producing methyliminobisdialkylacetamide

Publications (2)

Publication Number Publication Date
FR2970251A1 FR2970251A1 (en) 2012-07-13
FR2970251B1 true FR2970251B1 (en) 2013-02-08

Family

ID=46330804

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1250176A Active FR2970251B1 (en) 2011-01-07 2012-01-06 PROCESS FOR THE PRODUCTION OF METHYLIMINOBISDIALKYLACETAMIDE

Country Status (2)

Country Link
JP (1) JP5682889B2 (en)
FR (1) FR2970251B1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6061335B2 (en) * 2012-06-18 2017-01-18 国立研究開発法人日本原子力研究開発機構 Solvent extraction separation of osmium, iridium, platinum, gold or mercury from hydrochloric acid solution

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009062296A (en) * 2007-09-05 2009-03-26 Fujifilm Corp Method for producing carboxylic acid ester compound
JP2009091267A (en) * 2007-10-04 2009-04-30 Kyorin Pharmaceut Co Ltd Amide derivative, and selective agonist for sphingosine-1-phosphoric acid-1 (s1p1) receptor comprising the same as effective component
JP2009114129A (en) * 2007-11-07 2009-05-28 Japan Atomic Energy Agency N,n,n',n'-tetraoctyl-3-methyliminodiglycol amide compound and complexing extractant of specific metal comprising the compound
JP5284735B2 (en) * 2008-09-18 2013-09-11 株式会社Ａｄｅｋａ Polymerizable optically active imide compound and polymerizable composition containing the compound
JP2010101641A (en) * 2008-10-21 2010-05-06 Japan Atomic Energy Agency Method for extracting and separating solvent of metals using methyliminobisdialkyl acetamide is used as extractant

Also Published As

Publication number Publication date
JP5682889B2 (en) 2015-03-11
FR2970251A1 (en) 2012-07-13
JP2012144448A (en) 2012-08-02

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