FR2910603B1 - PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION - Google Patents

PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION

Info

Publication number
FR2910603B1
FR2910603B1 FR0655775A FR0655775A FR2910603B1 FR 2910603 B1 FR2910603 B1 FR 2910603B1 FR 0655775 A FR0655775 A FR 0655775A FR 0655775 A FR0655775 A FR 0655775A FR 2910603 B1 FR2910603 B1 FR 2910603B1
Authority
FR
France
Prior art keywords
cryogenetic
methane
distillation
possibly
separating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0655775A
Other languages
French (fr)
Other versions
FR2910603A1 (en
Inventor
Beraud Natacha Haik
Guillaume Texeira
Antoine Hernandez
Arthur Darde
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to FR0655775A priority Critical patent/FR2910603B1/en
Priority to FR0755103A priority patent/FR2916264A1/en
Priority to EP07871946.5A priority patent/EP2122282B1/en
Priority to CN2007800477381A priority patent/CN101680713B/en
Priority to US12/519,922 priority patent/US8959952B2/en
Priority to PL07871946T priority patent/PL2122282T3/en
Priority to ES07871946.5T priority patent/ES2683145T3/en
Priority to PCT/FR2007/052530 priority patent/WO2008087318A2/en
Publication of FR2910603A1 publication Critical patent/FR2910603A1/en
Application granted granted Critical
Publication of FR2910603B1 publication Critical patent/FR2910603B1/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0223—H2/CO mixtures, i.e. synthesis gas; Water gas or shifted synthesis gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0252—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of hydrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0261—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of carbon monoxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/40—Features relating to the provision of boil-up in the bottom of a column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/70—Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/30—Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/02—Internal refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/08—Internal refrigeration by flash gas recovery loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/24—Quasi-closed internal or closed external carbon monoxide refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/12—Particular process parameters like pressure, temperature, ratios
FR0655775A 2006-12-21 2006-12-21 PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION Expired - Fee Related FR2910603B1 (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR0655775A FR2910603B1 (en) 2006-12-21 2006-12-21 PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION
FR0755103A FR2916264A1 (en) 2006-12-21 2007-05-16 Mixture separating method, involves separating mixture using carbon monoxide cycle, where cycle assures cooling of methane at washing column, over-cooling of washing column and/or condensation at top of denitrification column
CN2007800477381A CN101680713B (en) 2006-12-21 2007-12-14 Method for separating a mixture of carbon monoxide, methane, hydrogen, and optionally nitrogen by cryogenic distillation
US12/519,922 US8959952B2 (en) 2006-12-21 2007-12-14 Method for separating a mixture of carbon monoxide, methane, hydrogen and optionally nitrogen by cryogenic distillation
EP07871946.5A EP2122282B1 (en) 2006-12-21 2007-12-14 Method for separating a mixture of carbon monoxide, methane, hydrogen and nitrogen by cryogenic distillation
PL07871946T PL2122282T3 (en) 2006-12-21 2007-12-14 Method for separating a mixture of carbon monoxide, methane, hydrogen and nitrogen by cryogenic distillation
ES07871946.5T ES2683145T3 (en) 2006-12-21 2007-12-14 Separation procedure of a mixture of carbon monoxide, methane, hydrogen and nitrogen by cryogenic distillation
PCT/FR2007/052530 WO2008087318A2 (en) 2006-12-21 2007-12-14 Method for separating a mixture of carbon monoxide, methane, hydrogen, and optionally nitrogen by cryogenic distillation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0655775A FR2910603B1 (en) 2006-12-21 2006-12-21 PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION

Publications (2)

Publication Number Publication Date
FR2910603A1 FR2910603A1 (en) 2008-06-27
FR2910603B1 true FR2910603B1 (en) 2009-03-06

Family

ID=38293985

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0655775A Expired - Fee Related FR2910603B1 (en) 2006-12-21 2006-12-21 PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION

Country Status (1)

Country Link
FR (1) FR2910603B1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2953004B1 (en) 2009-11-24 2013-12-20 Air Liquide PROCESS FOR CRYOGENIC SEPARATION OF A NITROGEN MIXTURE AND CARBON MONOXIDE

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1351598A (en) * 1970-03-26 1974-05-01 Air Prod & Chem Separation of gas mixtures
DE3215829A1 (en) * 1982-04-28 1983-11-03 Linde Ag, 6200 Wiesbaden METHOD FOR PRODUCING CARBON MONOXIDE
GB9800693D0 (en) * 1998-01-13 1998-03-11 Air Prod & Chem Separation of carbon monoxide from nitrogen-contaminated gaseous mixtures

Also Published As

Publication number Publication date
FR2910603A1 (en) 2008-06-27

Similar Documents

Publication Publication Date Title
FR2915791B1 (en) METHOD AND APPARATUS FOR SEPARATING A MIXTURE OF HYDROGEN, METHANE AND CARBON MONOXIDE BY CRYOGENIC DISTILLATION
PL2122282T3 (en) Method for separating a mixture of carbon monoxide, methane, hydrogen and nitrogen by cryogenic distillation
EA200800325A1 (en) EXTRACTING MONOXIDE OF CARBON AND HYDROGEN FROM HYDROCARBON FLOWS
MY155414A (en) Cryogenic system for removing acid gases from a hydrocarbon gas stream, and method of removing acid gases
FR2817766B1 (en) PROCESS AND PLANT FOR SEPARATING A GAS MIXTURE CONTAINING METHANE BY DISTILLATION, AND GASES OBTAINED BY THIS SEPARATION
FR2904832B1 (en) PROCESS FOR THE PRODUCTION OF SYNTHESIS GAS WITH CO2 CONVERSION TO HYDROGEN
ZA201003346B (en) Process for producing a purified synthesis gas stream
EP2226598A3 (en) Separation of carbon monoxide from gaseous mixtures containing carbon monoxide
TW200640847A (en) Process for preparing propene from propane
TN2009000480A1 (en) Process for converting hydrocarbon feedstocks with electrolytic recovery of halogen
FR2936864B1 (en) PROCESS FOR THE PRODUCTION OF LIQUID AND GASEOUS NITROGEN CURRENTS, A HELIUM RICH GASEOUS CURRENT AND A DEAZOTE HYDROCARBON CURRENT, AND ASSOCIATED PLANT.
PL2331898T3 (en) Process for generating and separating a hydrogen-carbon monoxide mixture by cryogenic distillation
CL2008001510A1 (en) Process for synthesis of ch3cooh that comprises passing mixture of synthesis gas of recirculation gas and compensation gas through 1st synthesis reactor, obtain gaseous mixture containing ch3cooh, cool mixture, pass through 2nd reactor and form gaseous stream of ch3cooh, cool recover ch3cooh and recirculate gas to 1st reactor.
WO2009004207A3 (en) Method and device for the cryogenic separation of a methane-rich flow
WO2007134716A3 (en) METHOD FOR SEPARATING CHLORINE FROM THE PRODUCT GAS FROM AN HCl OXIDATION PROCESS
FR2910602B1 (en) PROCESS AND APPARATUS FOR SEPARATING A MIXTURE COMPRISING AT LEAST HYDROGEN, NITROGEN AND CARBON MONOXIDE BY CRYOGENIC DISTILLATION
GB2463202A (en) Method and apparatus for recovering and fractionating a mixed hydrocarbon feed stream
FR2893516B1 (en) PROCESS FOR SEPARATING / PURIFYING A GAS MIXTURE
GB201307490D0 (en) Process for improving the hydrogen content of a synthesis gas
FR2934581B1 (en) METHOD AND APPARATUS FOR GENERATING AND PURIFYING GAS SYNTHESIS.
FR2838424B1 (en) PROCESS AND PLANT FOR SEPARATING A MIXTURE OF HYDROGEN AND CARBON MONOXIDE
FR2953004B1 (en) PROCESS FOR CRYOGENIC SEPARATION OF A NITROGEN MIXTURE AND CARBON MONOXIDE
EA201400499A1 (en) METHOD FOR PROCESSING OF FISHER-TROPSHA OUTFLOW GAS SYNTHESIS
TW200626531A (en) Process for the production of methanol
FR2910603B1 (en) PROCESS FOR SEPARATING A MIXTURE OF CARBON MONOXIDE, METHANE, HYDROGEN AND, POSSIBLY, NITROGEN BY CRYOGENETIC DISTILLATION

Legal Events

Date Code Title Description
PLFP Fee payment

Year of fee payment: 10

PLFP Fee payment

Year of fee payment: 11

PLFP Fee payment

Year of fee payment: 12

PLFP Fee payment

Year of fee payment: 13

ST Notification of lapse

Effective date: 20200914