FR2903337A1 - Producing a motor vehicle component containing fragments of agglomerated flexible foam, comprises mixing the foam, prepolymer resin and catalyst in an aqueous solution in a mixing unit to produce the mixture - Google Patents
Producing a motor vehicle component containing fragments of agglomerated flexible foam, comprises mixing the foam, prepolymer resin and catalyst in an aqueous solution in a mixing unit to produce the mixture Download PDFInfo
- Publication number
- FR2903337A1 FR2903337A1 FR0606267A FR0606267A FR2903337A1 FR 2903337 A1 FR2903337 A1 FR 2903337A1 FR 0606267 A FR0606267 A FR 0606267A FR 0606267 A FR0606267 A FR 0606267A FR 2903337 A1 FR2903337 A1 FR 2903337A1
- Authority
- FR
- France
- Prior art keywords
- mixture
- catalyst
- prepolymer
- resin
- foam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C67/00—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00
- B29C67/20—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00 for porous or cellular articles, e.g. of foam plastics, coarse-pored
- B29C67/207—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00 for porous or cellular articles, e.g. of foam plastics, coarse-pored comprising impregnating expanded particles or fragments with a binder
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C44/00—Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
- B29C44/34—Auxiliary operations
- B29C44/3442—Mixing, kneading or conveying the foamable material
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/22—After-treatment of expandable particles; Forming foamed products
- C08J9/228—Forming foamed products
- C08J9/236—Forming foamed products using binding agents
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/35—Composite foams, i.e. continuous macromolecular foams containing discontinuous cellular particles or fragments
Abstract
Description
1 L'invention concerne un procédé de réalisation d'un composant, notammentThe invention relates to a method for producing a component, in particular
de véhicule automobile, à base de flocons de mousse souple agglomérés, et un composant réalisé par un tel procédé. motor vehicle, based agglomerated soft foam flakes, and a component made by such a method.
II est connu de réaliser un composant à base de flocons de mousse souple agglomérés, notamment issus du recyclage, par exemple un composant d'insonorisation, par un procédé comprenant les étapes suivantes : • mélanger dans une unité de mélange de grande taille la quantité nécessaire à la réalisation d'une pluralité de composants d'un mélange 1 o de flocons de mousse souple et de résine prépolymère à base polyuréthanne, • disposer ledit mélange dans une unité de stockage, • disposer la quantité dudit mélange nécessaire à la réalisation d'un composant dans un moule, généralement fermé, 15 • injecter dans ledit moule de la vapeur d'eau, notamment à température voisine de 110 C, de sorte à réaliser la polymérisation dudit prépolymère et à obtenir un liant polymérique expansé, • démouler le composant obtenu • le faire sécher en étuve, notamment à une température comprise entre 20 100 et 130 C. Un tel procédé requiert des équipements complexes et encombrants, de grandes quantités d'énergie et une grande surface de réception des équipements. L'invention a pour but de pallier ces inconvénients. A cet effet, et selon un premier aspect, l'invention propose un procédé de réalisation d'un composant, notamment de véhicule automobile, à base de 30 flocons de mousse souple agglomérés, ledit procédé comprenant les étapes suivantes : 25 2903337 2 • mélanger dans une unité de mélange la quantité nécessaire à la réalisation du composant d'un mélange de flocons de mousse souple, de résine prépolymère, et de catalyseur en solution aqueuse, de sorte à réaliser ledit mélange dans un temps inférieur au temps de démarrage 5 de la réaction de ladite résine avec ledit catalyseur, • disposer ledit mélange dans un moule ouvert et le répartir dans ledit moule, • fermer ledit moule et laisser agir ledit catalyseur sur ladite résine à température modérée et pression ambiante, de sorte à réaliser la polymérisation dudit prépolymère et à obtenir un liant polymérique, • démouler le composant obtenu. De la sorte, le mélange est préparé juste avant réalisation du composant, et ce dans la quantité nécessaire à sa fabrication. II en résulte que l'on s'affranchit de l'utilisation d'une unité de stockage et que l'unité de mélange est de taille très réduite. En outre, la présence de catalyseur permet d'éviter l'injection de vapeur d'eau dans le moule. Les moules sont donc simplifiés. Par ailleurs, il n'est plus nécessaire de réaliser un séchage des composants après moulage. Enfin, on économise l'énergie liée à la production de vapeur et au séchage. On notera que la polymérisation étant réalisée en l'absence d'eau, hormis celle résiduelle servant de solvant au catalyseur, le liant présente une forme compacte, c'est à dire non expansée. Selon un deuxième aspect, l'invention propose un composant réalisé par un tel procédé, le liant étant sous forme compacte. It is known to produce a component based on agglomerated soft foam flakes, in particular derived from recycling, for example a soundproofing component, by a process comprising the following steps: • mixing in a large mixing unit the necessary quantity producing a plurality of components of a mixture of soft foam flakes and polyurethane-based prepolymer resin, arranging said mixture in a storage unit, arranging the quantity of said mixture necessary for the production of a component in a mold, generally closed, • injecting into said mold water vapor, especially at a temperature of about 110 [deg.] C., so as to carry out the polymerization of said prepolymer and to obtain an expanded polymeric binder, • demold the component obtained • drying in an oven, especially at a temperature between 100 and 130 C. Such a process requires equipment ts complex and bulky, large amounts of energy and a large surface receiving equipment. The invention aims to overcome these disadvantages. For this purpose, and according to a first aspect, the invention provides a method of producing a component, especially a motor vehicle, based on agglomerated soft foam flakes, said process comprising the following steps: in a mixing unit the amount necessary to produce the component of a mixture of soft foam flakes, prepolymer resin, and catalyst in aqueous solution, so as to achieve said mixture in a time less than the start time 5 of reacting said resin with said catalyst, • disposing said mixture in an open mold and distributing it in said mold, • closing said mold and allowing said catalyst to act on said resin at moderate temperature and ambient pressure, so as to carry out the polymerization of said prepolymer and to obtain a polymeric binder, • demold the component obtained. In this way, the mixture is prepared just before production of the component, and in the amount necessary for its manufacture. As a result, the use of a storage unit is dispensed with and the mixing unit is very small in size. In addition, the presence of catalyst makes it possible to avoid the injection of water vapor into the mold. The molds are simplified. Moreover, it is no longer necessary to perform a drying of the components after molding. Finally, we save energy related to steam production and drying. It should be noted that the polymerization being carried out in the absence of water, apart from the residual one serving as solvent for the catalyst, the binder has a compact form, ie not expanded. According to a second aspect, the invention proposes a component produced by such a method, the binder being in compact form.
On décrit à présent un procédé de réalisation d'un composant notamment de véhicule automobile, à base de flocons de mousse souple agglomérés, ledit procédé comprenant les étapes suivantes : 2903337 3 • mélanger énergiquement dans une unité de mélange de petite taille la quantité nécessaire à la réalisation du composant d'un mélange de flocons de mousse souple, de résine prépolymère, et de catalyseur en solution aqueuse, de sorte à réaliser ledit mélange dans un temps 5 inférieur au temps de démarrage de la réaction de ladite résine avec ledit catalyseur, • disposer ledit mélange dans un moule ouvert et le répartir dans ledit moule, • fermer ledit moule et laisser agir, par exemple pendant une durée de 4 à 10 5 minutes environ, ledit catalyseur sur ladite résine à température modérée et pression ambiante, de sorte à réaliser la polymérisation dudit prépolymère et à obtenir un liant polymérique, • démouler le composant obtenu. A method of producing a component, especially a motor vehicle component, based on agglomerated flexible foam flakes, said method comprising the following steps: • mixing vigorously in a small mixing unit the quantity necessary for producing the component of a mixture of soft foam flakes, prepolymer resin, and catalyst in aqueous solution, so as to make said mixture in a time less than the starting time of the reaction of said resin with said catalyst, Disposing said mixture in an open mold and distributing it in said mold, closing said mold and allowing said catalyst to act on said resin at moderate temperature and ambient pressure, for example for a period of about 4 to 10 minutes, so that performing the polymerization of said prepolymer and obtaining a polymeric binder, • demolding the component obtained.
15 Selon une réalisation, le prépolymère est choisi de sorte à produire un liant à base de polyuréthanne. La température modérée peut être de l'ordre de 50 C, les moules pouvant être maintenus à cette température par circulation d'eau dans leur corps. Selon une réalisation, le temps de mélange est compris entre 30 et 120 secondes, et notamment inférieur à 60 secondes et inférieur au temps de démarrage de la réaction de la résine avec le catalyseur.In one embodiment, the prepolymer is selected to produce a polyurethane binder. The moderate temperature can be of the order of 50 C, the molds can be maintained at this temperature by circulating water in their body. According to one embodiment, the mixing time is between 30 and 120 seconds, and in particular less than 60 seconds and less than the start time of the reaction of the resin with the catalyst.
25 Selon une réalisation, le mélange est réalisé par une hélice disposée au fond de l'unité de mélange, ladite hélice tournant à une vitesse comprise entre 800 et 1600 tours/minute, par exemple à une vitesse de 1000 tours/minute environ, ce qui permet d'assurer le mélange dans le temps susmentionné, avec imprégnation de surface des flocons par le prépolymère et le catalyseur.According to one embodiment, the mixing is carried out by a propeller disposed at the bottom of the mixing unit, said propeller rotating at a speed of between 800 and 1600 revolutions / minute, for example at a speed of approximately 1000 revolutions / minute. which makes it possible to ensure the mixing in the aforementioned time, with surface impregnation of the flakes with the prepolymer and the catalyst.
30 Selon une réalisation, la répartition du mélange dans le moule est réalisée manuellement, l'opérateur effectuant cette répartition en tenant compte des fluctuations d'épaisseur éventuelles du composant.According to one embodiment, the distribution of the mixture in the mold is performed manually, the operator performing this distribution taking into account possible thickness fluctuations of the component.
20 2903337 4 Selon une réalisation, les flocons de mousse sont issus du recyclage. Un composant réalisé par un tel procédé présente la particularité que le liant est 5 sous forme compacte, c'est à dire non expansée.In one embodiment, the foam flakes are derived from recycling. A component made by such a process has the particularity that the binder is in compact form, ie unexpanded.
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0606267A FR2903337B1 (en) | 2006-07-10 | 2006-07-10 | METHOD OF MAKING A COMPONENT BASED ON AGGLOMERATED SOFT FOAM FLAKES USING A RESIN AND A CATALYST |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0606267A FR2903337B1 (en) | 2006-07-10 | 2006-07-10 | METHOD OF MAKING A COMPONENT BASED ON AGGLOMERATED SOFT FOAM FLAKES USING A RESIN AND A CATALYST |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2903337A1 true FR2903337A1 (en) | 2008-01-11 |
FR2903337B1 FR2903337B1 (en) | 2010-10-22 |
Family
ID=37075274
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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FR0606267A Active FR2903337B1 (en) | 2006-07-10 | 2006-07-10 | METHOD OF MAKING A COMPONENT BASED ON AGGLOMERATED SOFT FOAM FLAKES USING A RESIN AND A CATALYST |
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FR (1) | FR2903337B1 (en) |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4666646A (en) * | 1985-07-24 | 1987-05-19 | Chang Kun H | Method of producing high-density PU foam material |
DE4306626A1 (en) * | 1992-03-30 | 1994-09-08 | Hecker & Krosch Gmbh & Co Kg | Process for recycling rigid polyurethane foam |
WO1998014508A1 (en) * | 1996-09-30 | 1998-04-09 | Woodbridge Foam Corporation | Agglomerated superabsorbant foam |
US20040053032A1 (en) * | 2000-07-11 | 2004-03-18 | Rudolf Weingartner | Method for producing foam products |
US20040082676A1 (en) * | 2002-03-07 | 2004-04-29 | Douglas Bruce F. | Method for mixing blowing agents with polyurethane reagents for the production of polyurethane foam boards |
-
2006
- 2006-07-10 FR FR0606267A patent/FR2903337B1/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4666646A (en) * | 1985-07-24 | 1987-05-19 | Chang Kun H | Method of producing high-density PU foam material |
DE4306626A1 (en) * | 1992-03-30 | 1994-09-08 | Hecker & Krosch Gmbh & Co Kg | Process for recycling rigid polyurethane foam |
WO1998014508A1 (en) * | 1996-09-30 | 1998-04-09 | Woodbridge Foam Corporation | Agglomerated superabsorbant foam |
US20040053032A1 (en) * | 2000-07-11 | 2004-03-18 | Rudolf Weingartner | Method for producing foam products |
US20040082676A1 (en) * | 2002-03-07 | 2004-04-29 | Douglas Bruce F. | Method for mixing blowing agents with polyurethane reagents for the production of polyurethane foam boards |
Also Published As
Publication number | Publication date |
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FR2903337B1 (en) | 2010-10-22 |
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