FR2839554A1 - Immersion sampler for water or other liquid has sample collection container with siphon on inlet side and washing flask on outlet side - Google Patents

Immersion sampler for water or other liquid has sample collection container with siphon on inlet side and washing flask on outlet side Download PDF

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Publication number
FR2839554A1
FR2839554A1 FR0205823A FR0205823A FR2839554A1 FR 2839554 A1 FR2839554 A1 FR 2839554A1 FR 0205823 A FR0205823 A FR 0205823A FR 0205823 A FR0205823 A FR 0205823A FR 2839554 A1 FR2839554 A1 FR 2839554A1
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France
Prior art keywords
siphon
water
sample
container
liquid
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Granted
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FR0205823A
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French (fr)
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FR2839554B1 (en
Inventor
Medec Yves Le
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Individual
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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/18Water
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/18Water
    • G01N33/1826Water organic contamination in water
    • G01N2033/184Water organic contamination in water herbicides, pesticides, fungicides, insecticides, or the like

Abstract

Liquid sampler consists of sample collection container (1) with siphon (2) on its inlet side that controls the intake of liquid by high point (5) on its inlet (4) while retaining trap and flask (3) on its outlet side for when liquid level reaches the bottom of its air outlet tube (9). The sample container can be separated from the siphon and the washing flask, and the base (10) is detachable to air to be removed before recovering the sample. Liquid sampler consists of sample collection container (1) with a swan-neck siphon (2) on its inlet side that controls the intake of liquid by a high point (5) on its inlet (4) while retaining a trap, and a washing flask (3) on its outlet side that stops the siphoning when the liquid level reaches the bottom of its air outlet tube (9). The sample container can be separated from the siphon and the washing flask for removal and transport of the sample, and the base (10) of the siphon is detachable to air to be removed before recovering the sample and for easier cleaning. The inlet of the siphon can also have a float-controlled shutter, and plugs can be used to seal the inlet and outlet tubes before the required depth is reached for sampling.

Description

du vehicule automobile.of the motor vehicle.

À 1 2839554At 1 2839554

DESCRIPTIONDESCRIPTION

L'invention concerne un dispositif autonome pour un prelevement unique d'eau (ou tout liquide analogue) lors de sa plongee dans ['element liquide. Le dispositif est particulierement destine au suivi de la qualite d'eau des cours d'eau en periode de crues. Porte au bout d'une perche, par exemple, et regle a un niveau predetermine, l'appareil realisera automatiquement et dans le respect des normes en vigueur un echantillonnage lorsque la montee des eaux apportera le  The invention relates to an autonomous device for a single sampling of water (or any similar liquid) when it is immersed in the liquid element. The device is particularly intended for monitoring the water quality of rivers during flood periods. Worn at the end of a pole, for example, and adjusted to a predetermined level, the device will automatically carry out and in compliance with the standards in force a sampling when the rise in water will bring the

liquide jusqu'au niveau du siphon d'entree.  liquid up to the level of the inlet siphon.

En ltoccurrence, la plupart des crues vent suivies par des technicians realisant au cas par cas des prelevements ponctuels et manuels. Rapidement, ils vent debordes par la surcharge de travail: les crues apparaissaient soudainement et s'etalent un laps de temps assez court. Par ailleurs, realiser un prelevement dans un cours d'eau peut alors presenter des risques (courant  In this case, most of the floods are monitored by technicians carrying out punctual and manual samples on a case-by-case basis. Quickly, they were overwhelmed by the overload of work: the floods appeared suddenly and spread over a fairly short period of time. In addition, taking a sample from a watercourse can then present risks (current

puissant, berges instables).powerful, unstable banks).

En fait, il existe sur le marche des preleveurs automatiques capables via une pompe et un detecteur du niveau de l'eau de prelever l'eau de surface lors la montee des crues. Si leur fiabilite est prouvee, des ecueils techniques (manipulation par des inities, genie civil, amenee  In fact, there are automatic samplers on the market capable of withdrawing surface water when the floods rise, via a pump and a water level detector. If their reliability is proven, technical pitfalls (manipulation by insiders, civil engineering,

d'energie electrique) et surtout financiers reservent leur emploi a quelques etudes particulieres.  of electrical energy) and especially financial reserve their employment for some particular studies.

Pourtant, ['etude a grande echelle et complete des crues suite a des evenements pluvieux vent de toute premiere importance: les flux les plus importants en nitrates, en phosphore et en  However, the large-scale and complete study of floods following very important wind rain events: the most important fluxes of nitrates, phosphorus and

pesticides vent observes durant ces episodes hydrologiques.  wind pesticides observed during these hydrological episodes.

Le dispositif selon ['invention est le maillon manquant entre le prelevement manuel et le  The device according to the invention is the missing link between the manual sampling and the

prelevement automatise.automated collection.

L'appareil se caracterise par ces elements: tout d'abord, un contenant qui recueillera l' echantillo n. A l'amont de ce co ntentant se trouve un siphon en c o l de cygne qui c ommande par son point haut ['entree de lteau et retient un bouchon d'eau lors de la remontee du dispositif et a l'aval le contenant se termine par un flacon laveur responsable de l'arret du siphonage  The device is characterized by these elements: first of all, a container which will collect the sample n. Upstream of this co ntentant is a swan neck siphon which controls by its high point [lteau entry and retains a water cap during the ascent of the device and downstream the container ends by a washing bottle responsible for stopping the siphoning

lorsque le niveau de l'eau atteint la base du tube qui permet a l'air de s'echapper.  when the water level reaches the base of the tube which allows air to escape.

Le dessin annexe illustre ['invention: la figure represente en coupe, le dispositif de ['invention.  The accompanying drawing illustrates the invention: the figure shows in section the device of the invention.

En reference a ce dessin, nous pouvons done imaginer que l'appareil est fixe en surplomb et a ['horizontal de la surface de l'eau dans le cas d'un suivi des crues. Lorsque la montee de l'eau sera effective, lteau va penetrer par ['orifice du siphon (4) puis au fur a mesure de ltengloutissement de l'appareil va atteindre le point haut du siphon (5). C'est senlement a partir de ce seuil que le prelevement va etre realise (a la condition que ce point 5 est plus eleve que le point 6 sinon ctest le dernier point 6 qui commande l'echantillonnage). Rapidement, l'eau  With reference to this drawing, we can therefore imagine that the device is fixed overhanging and horizontal to the surface of the water in the case of flood monitoring. When the water rise is effective, the water will penetrate by the orifice of the siphon (4) then, as the device drips, will reach the high point of the siphon (5). It is only from this threshold that the sample will be taken (on the condition that this point 5 is higher than point 6 otherwise it is the last point 6 which controls the sampling). Water quickly

stengouffre dans le siphon, remplit le conduit (6) puis se jette dans le flacon echantillonneur (1).  stewards in the siphon, fills the conduit (6) then empties into the sampler bottle (1).

Lorsque le remplissage sera effectif, l'eau va alors atteindre par surverse (8) le flacon laveur (3) ou une tige de verre dont ['orifice superieur depasse le niveau haut du siphon permet a l'air atmospherique de s'echapper et done d'etre remplace par un volume d'eau equivalent. Peu a peu, l'eau occupe le fond du flacon et atteint la base inferieure de ce tube en verre (9). L'air ne  When the filling is effective, the water will then reach by overflow (8) the washing bottle (3) or a glass rod whose [orifice above the upper level of the siphon allows atmospheric air to escape and therefore to be replaced by an equivalent volume of water. Little by little, water occupies the bottom of the bottle and reaches the lower base of this glass tube (9). The air does

peut plus 8tre evacue vers l'exterieur. Aussi, l'eau ne peut plus penetrer dans ltechantillonneur.  can no longer be evacuated to the outside. Also, water can no longer enter the sampler.

Si lteau continue a monter et depasse le niveau de ['orifice aval du flacon laveur, elle ne peut neanmoins penetrer dans l'echantillonneur, la pression de l'eau etant superieur a ['orifice amont  If the water continues to rise and exceeds the level of the downstream orifice of the washing bottle, it cannot nevertheless enter the sampler, the water pressure being greater than the upstream orifice

du siphon.siphon.

L'echantillonnage est done unique et s'effectue en sens unique.  Sampling is therefore unique and is carried out in one direction.

2 28395542 2839554

Lorsque l'echantillonneur est retire de l'eau ou si le niveau de l'eau redescend sous ['orifice d'entree du siphon (4), l'eau excedentaire est refoulee par siphonage. Un tube coude dont ['orifice se trouve sous le niveau du bord superieur du contenant evacue une partie de l'eau qui aurait empeche la pose d'un bouchon sur ce flacon lors du transport ulterieur. Il convient que ['orifice amont du siphon soit legerement inferieur au niveau teas de ce tube coude. Dans le cas contraire (niveau 4 = niveau 7), un phenomene de capillarite peut empecher une bonne vidange  When the sampler is removed from the water or if the water level drops below the siphon inlet (4), the excess water is discharged by siphoning. An elbow tube whose orifice is below the level of the upper edge of the container discharges part of the water which would have prevented the fitting of a stopper on this bottle during subsequent transport. The upstream opening of the siphon should be slightly lower than the teas level of this elbow tube. Otherwise (level 4 = level 7), a phenomenon of capillarity can prevent good drainage

du siphon.siphon.

Dans cette configuration optimale, un volume suffisant pour des analyses ulterieures est lo conserve dans le contenant principal (1). Deux bouchons d'eau (pieges respectivement dans le col de cygne et au fond du flacon laveur) separes de l'echantillon par un volume d'air le  In this optimal configuration, a sufficient volume for subsequent analyzes is kept in the main container (1). Two water plugs (traps respectively in the swan neck and at the bottom of the washing bottle) separated from the sample by a volume of air

protegent de toute pollution ulterieure (par l'air exterieur ou lors d'une remontee des eaux).  protect from any subsequent pollution (by outside air or during upwelling).

Pour recuperer ltechantillon, il convient d'escamoter les bouchons d'eau du siphon (10) et du flacon laveur (11) en devissant leurs bases amovibles afin d'eviter l'entra^nement de ces eaux souillees vers l'echantillon destine a l'analyse (ltenlevement du contenant (12) sans cette precaution peut amener une partie de l'eau du siphon vers le contentant car ce volume d'eau  To recover the sample, it is necessary to retract the water plugs from the siphon (10) and the washing bottle (11) by unscrewing their removable bases in order to avoid entrainment of these contaminated water towards the sample intended for analysis (raising the container (12) without this precaution can bring part of the water from the siphon to the container because this volume of water

tense de remplacer le volume occupe par la paroi du contenant).  tense to replace the volume occupied by the wall of the container).

Dans une variante non illustree, un bras relic a des flotteurs peut reposer hermetiquement sur ['entree du siphon (4). Cette etancheite est brisee lorsque la montee de lteau souleve les  In a variant not illustrated, an arm connected to floats can rest hermetically on the inlet of the siphon (4). This seal is broken when the rise in water lifts the

flotteurs (protection optimisee du conduit d'amenee de l'echantillon).  floats (optimized protection of the sample supply pipe).

L'echantillonneur (flacons 1, 2, 3 vices) peut prelever une nouvelle crue (avec la possibilite  The sampler (bottles 1, 2, 3 vices) can take a new flood (with the possibility

d'une autre hauteur de prelevement par un deplacement vertical de ['ensemble du dispositif).  from another sampling height by a vertical displacement of the whole device.

A titre indicatif, ce dispositif est constitue dans le respect des normes en vigueur exclusivement de materiaux inertes (verre, inox, teflon,...) propres a l'analyse de composees diverges dans  As an indication, this device is made in compliance with the standards in force exclusively of inert materials (glass, stainless steel, Teflon, ...) suitable for the analysis of diverging compounds in

l'eau ou dans toute autre liquide.water or any other liquid.

L'utilisation de verre peut le rendre fragile. Aussi, ce dispositif peut etre protege par une coque. Cet appareil peut conserver a titre d'exemple un litre d'echantillon (le volume du contenant n'a d'ailleurs pas d'influence sur la bonne marche du dispositif), peser deux a trots kilos et se caracterise par une largeur de quinze centimetres environ pour une hauteur et longueur de  The use of glass can make it fragile. Also, this device can be protected by a shell. This device can keep by way of example a liter of sample (the volume of the container does not have any influence on the good functioning of the device), weigh two to three pounds and is characterized by a width of fifteen about centimeters for a height and length of

trente centimetres.thirty centimeters.

I1 est envisageable d'utiliser un siphon modifiable dans sa courbure et son diametre afin  It is conceivable to use a siphon which can be modified in its curvature and its diameter in order to

d'adapter le dispositif a la viscosite du liquide preleve.  to adapt the device to the viscosity of the withdrawn liquid.

Dans une variante non illustree et pour un prelevement en profondeur un bouchon escamotable  In a variant not illustrated and for a deep sampling a retractable plug

peut interdire le remplissage du dispositif avant que ce dispositif atteigne la profondeur desiree.  can prohibit the filling of the device before this device reaches the desired depth.

Ce bouchon peut se poser a ['orifice amont (4) ou aval (12) du dispositif.  This plug can be placed at the upstream (4) or downstream (12) orifice of the device.

De meme, cet dispositif couple ou non a un regulateur de vitesse peut realiser lors de sa  Likewise, this device, whether or not coupled to a speed regulator, can be carried out during its

plongee dans ['element liquide un prelevement sur toute la hauteur parcourue.  immersed in the liquid element a sample over the entire height traveled.

3 28395543 2839554

Claims (1)

REVENDICATIONS l) Dispositif autonome pour un prelevement unique d'eau (ou tout liquide analogue) lors de sa plongee dans ['element liquide, caracterise en ce qu'il se compose d'un contenant (1) qui recueillera l'echantillon, a l'amont de ce contenant se trouve un siphon en col de cygne (2) qui comrnande par son point haut ['entree de l'eau (5) et retient un bouchon d'eau lors de la remontee du dispositif et a l'aval le contenant se termine par un flacon laveur (3) responsable de l'arret du siphonage lorsque le niveau de l'eau atteint la base  l) Autonomous device for a single sampling of water (or any similar liquid) when it is immersed in the liquid element, characterized in that it consists of a container (1) which will collect the sample, a 'upstream of this container is a swan neck siphon (2) which commands by its high point [' water inlet (5) and retains a water cap when raising the device and downstream the container ends with a washing bottle (3) responsible for stopping the siphoning when the water level reaches the base du tube (9) qui permet a l'air de stechapper.  of the tube (9) which allows the air to escape. 2) Dispositif selon la revendication l carcaterise en ce que le contenant (1) se desolidarise du siphon en col de cygne (2) et du fiacon lavour (3) afin de permettre la recuperation  2) Device according to claim l carcaterise in that the container (1) is detached from the swan neck siphon (2) and the lavour bottle (3) in order to allow recovery et le transport de l'echantillon.and transport of the sample. 3) Dispositif selon l'une ou l'autre des revendications caracterise en ce que la base du  3) Device according to either of the claims characterized in that the base of the siphon (10) est escamotable afin de permettre de chasser l'air avant la recuperation de ltechantillon et un nettoyage optimal. I1 en est de meme pour la base du flacon laveur  siphon (10) is retractable in order to allow the air to be expelled before the sample is collected and optimal cleaning. It is the same for the base of the washing bottle (11) afin de faciliter le nettoyage et le reamorcage du dispositif.  (11) to facilitate cleaning and re-priming of the device. 4) Dispositif selon l'une quelconque des revendications precedentes caracterise en ce que  4) Device according to any one of the preceding claims, characterized in that une tige coudee plongee (7) dans le contenant et reliee au siphon evacue l'excedent  a bent rod immersed (7) in the container and connected to the siphon discharges the excess d'eau lors de la remontee du dispositif.  of water when raising the device. 5) Dispositif selon l'une quelconque des revendications precedentes caracterise en ce qutun  5) Device according to any one of the preceding claims, characterized in that bras relic a des flotteurs peut reposer hermetiquement sur ['entree du siphon (4). Cette  arm connected to floats can rest hermetically on the inlet of the siphon (4). This etancheite est brisee lorsque la montee de l'eau souleve les flotteurs.  sealing is broken when the rise in water lifts the floats. 6) Dispositif selon les revendications precedentes 1, 2, 3 et 4 caracterise en ce qu'un  6) Device according to the preceding claims 1, 2, 3 and 4 characterized in that a bouchon escamotable peut rendre etanche l'extremite amont (4) ou aval (9) pour  retractable plug can seal the upstream (4) or downstream (9) end for
FR0205823A 2002-05-13 2002-05-13 AUTONOMOUS DEVICE FOR A SINGLE COLLECTION OF WATER (OR ANY LIQUID ANALOGUE) DURING ITS DIVE IN THE LIQUID ELEMENT Expired - Fee Related FR2839554B1 (en)

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FR0205823A FR2839554B1 (en) 2002-05-13 2002-05-13 AUTONOMOUS DEVICE FOR A SINGLE COLLECTION OF WATER (OR ANY LIQUID ANALOGUE) DURING ITS DIVE IN THE LIQUID ELEMENT

Applications Claiming Priority (1)

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FR0205823A FR2839554B1 (en) 2002-05-13 2002-05-13 AUTONOMOUS DEVICE FOR A SINGLE COLLECTION OF WATER (OR ANY LIQUID ANALOGUE) DURING ITS DIVE IN THE LIQUID ELEMENT

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3554037A (en) * 1968-05-09 1971-01-12 Robert H Berg Continuous flow pipeline sampling orifice arrangement
US4095471A (en) * 1977-04-04 1978-06-20 The United States Of America As Represented By The United States Department Of Energy Tidal sampler
GB2203406A (en) * 1987-04-14 1988-10-19 Shell Int Research Device for taking a fluid sample near the bottom of a tank
US5524495A (en) * 1992-06-22 1996-06-11 Vortox Company Liquid sampling devices and method
US5783758A (en) * 1996-02-12 1998-07-21 Vortox Company Liquid sampling apparatus for conduit liquid flow
US5821437A (en) * 1997-01-03 1998-10-13 Budin; Timothy M. Environmental liquid collection apparatus

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3554037A (en) * 1968-05-09 1971-01-12 Robert H Berg Continuous flow pipeline sampling orifice arrangement
US4095471A (en) * 1977-04-04 1978-06-20 The United States Of America As Represented By The United States Department Of Energy Tidal sampler
GB2203406A (en) * 1987-04-14 1988-10-19 Shell Int Research Device for taking a fluid sample near the bottom of a tank
US5524495A (en) * 1992-06-22 1996-06-11 Vortox Company Liquid sampling devices and method
US5783758A (en) * 1996-02-12 1998-07-21 Vortox Company Liquid sampling apparatus for conduit liquid flow
US5821437A (en) * 1997-01-03 1998-10-13 Budin; Timothy M. Environmental liquid collection apparatus

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