FR2789929A1 - Light solid sound-proofing and thermo-insulating material, generating no toxic gases on combustion, is obtained from monocotyledones from palmades species and optionally treated to - Google Patents

Light solid sound-proofing and thermo-insulating material, generating no toxic gases on combustion, is obtained from monocotyledones from palmades species and optionally treated to Download PDF

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Publication number
FR2789929A1
FR2789929A1 FR9902300A FR9902300A FR2789929A1 FR 2789929 A1 FR2789929 A1 FR 2789929A1 FR 9902300 A FR9902300 A FR 9902300A FR 9902300 A FR9902300 A FR 9902300A FR 2789929 A1 FR2789929 A1 FR 2789929A1
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Prior art keywords
drying
material according
species
sic
palmades
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FR9902300A
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French (fr)
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Jacques Langer
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Individual
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Priority to FR9902300A priority Critical patent/FR2789929A1/en
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Classifications

    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04BGENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/30Fireproofing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/0207Pretreatment of wood before impregnation
    • B27K3/0214Drying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04BGENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B2001/742Use of special materials; Materials having special structures or shape
    • E04B2001/745Vegetal products, e.g. plant stems, barks

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  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Architecture (AREA)
  • Acoustics & Sound (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)

Abstract

Thermo-insulating sound-proofing material is obtained from monocotyledones (sic) especially of palmades (sic) species and used to produce insulating panels and sandwich-type structures after drying to humidity level up to 25%, preferably 18-19%. Preferred Features: Drying can be preceded or followed by soaking in insecticide and fungicide, and by immersion in bath of running water or in tank where water is periodically changed, or by saturation with vapors or pulverization in solvent, to cause elimination of at least 20% of saccharose originally present in sap. Material can be also treated, after drying, with tetrakis salts, alkali metal citrates, guanyl urea phosphate, ammonium pentaborate, halogen compounds etc., to impart improved fireproofing properties, and can also be rendered waterproof, by impregnation, after drying, with waterproofing agent of methyl siloxane oligomer type or other type, or can be rendered impermeable, after drying, by surface treatment with polyvinylchloride (PVC) copolymer and polyvinyl alcohol resins, or hardened by impregnation, after drying, with for example urea or phenol formol (sic) or diallyl phthalate or methyl methacrylate, and can be used, after drying, in sandwich-type laminated panels between two or more layers of other materials.

Description

-I- A l'inverse des ligneux, bien connus, caractérisés par une partie-I- Unlike woody plants, well known, characterized by a part

externe généralement tendre et un duramen peu imprégnable, les monocotylédones, en particulier les poacées qui ont un chaume ligneux dur et résistant et les palmades dont le stipe est constitué d'un grand nombre de faisceaux libéroligneux. ont une partie interne, souvent méristématique, o des éléments fibro vasculaires ligneux sont entourées d'un tissus de  external generally tender and a little impregnable heartwood, the monocots, in particular the poaceae which have a hard and resistant woody stubble and the palmades whose stipe is made up of a large number of liberous bundles. have an internal part, often meristematic, where woody fibro-vascular elements are surrounded by

cellules peu différenciées dont la consistance est comparable au liège.  poorly differentiated cells whose consistency is comparable to cork.

Il est difficile de trouver sur le marché un matériau naturel qui allie une très grande légèreté et une bonne résistance mécanique, qui soit isolant phonique et thermique, qui soit  It is difficult to find on the market a natural material which combines a very great lightness and a good mechanical resistance, which is sound and thermal insulator, which is

autoextinguible sans émission de fumées toxiques.  self-extinguishing without emission of toxic fumes.

Prenons pour exemple le borassus flabelliformnis. Le délignage du stipe penrmet d'obtenir des planches de couleur très foncée, en bois parfait dans la partie périphérique des planches brun clair de dureté moyenne propres à faire du lambris dans une partie médiane, enfin des planches de teinte beige clair plus tendres et très légères dans le coeur  Take for example the borassus flabelliformnis. The trimming of the stipe makes it possible to obtain very dark planks, of perfect wood in the peripheral part of the light brown planks of medium hardness suitable for making paneling in a middle part, finally planks of light beige color more tender and very light in the heart

du stipe.of the stipe.

Les planches, quelle que soit leur section, issues du coeur du stipe, ont,  The boards, whatever their section, from the heart of the stipe, have,

naturellement, d'excellentes caractéristiques d'isolation phonique, thennique et sont auto-  naturally, excellent sound and thermal insulation characteristics and are self-

extinguibles sans dégagement de funmées toxiques. Leur très grande légèreté, et leur anrmature naturelle permnnet une utilisation nouvelle dans tous les domaines o ces propriétés sont requises, notamment pour constituer des panneaux d'isolation, pour lieux publics ou  extinguishable without release of toxic funmées. Their great lightness, and their natural structure allows new use in all areas where these properties are required, in particular to constitute insulation panels, for public places or

privés, navires, aéronefs, mais aussi, structures en sandwich, par exemple, des skis.  private, ships, aircraft, but also, sandwich structures, for example, skis.

A l'état brut ces planches sont difficilement utilisables car le xylème est imprégné d'une sève à haute teneur en saccharose qui subit en quelques heures, dans le milieu ambiant, une importante pollution microbienne par des levures. des moisissures et des  In the raw state these boards are difficult to use because the xylem is impregnated with a sap with a high sucrose content which undergoes in a few hours, in the ambient environment, a significant microbial pollution by yeasts. mold and

bactéries lactiques.lactic acid bacteria.

Dans tous les cas la matière première doit ètre séchée.  In all cases the raw material must be dried.

Une première solution consiste à introduire les planches dans des séchoirs aussitot après sciage pour ramener leur taux d'humidité au dessous de.%;o idéalement entre. 8 et 19%. Pour une meilleure utilisation, ce traitement peut être complété par trempage préalable dans un insecticide et lfongicide, qu'il s'agisse de pentachlorophénol, d' ammoniums quaternaires de cuivre, fluor, bore, arsenic, de cyperméthrine, de carbamates, etc. Pour éliminer le saccharose il faut pratiquer le dessevage des planches avant séchage aux normes européennes. Ce traitement sera effectué dans une cuve longitudinale Cen tôle galvanisée chaudronnée de 300xO10x100 cm. montée sur une structure de cornières mécano-soudées comprenant une vanne de vidange. On v immerge, dans de l'eau, des planches, écartées par des séparateurs plastiques pour faciliter la dilution; après un premier bain de 2 heures au cours duquel l'eau est brassée par une roue à palettes il est constaté sur des planches d'une section de 15x100 mm. une réduction supérieure à 20% du taux de saccharose; après le premier renouvellement de l'eau de rinçage le taux  A first solution consists in introducing the boards into dryers immediately after sawing to bring their humidity level below.%; O ideally between. 8 and 19%. For better use, this treatment can be completed by pre-soaking in an insecticide and fungicide, whether it be pentachlorophenol, quaternary ammoniums of copper, fluorine, boron, arsenic, cypermethrin, carbamates, etc. To eliminate sucrose it is necessary to practice the drying of the boards before drying to European standards. This treatment will be carried out in a longitudinal Cen galvanized sheet metal tank of 300xO10x100 cm. mounted on a structure of mechanically welded angles including a drain valve. Planks are immersed in water, separated by plastic separators to facilitate dilution; after a first bath of 2 hours during which the water is stirred by a paddle wheel it is found on boards with a section of 15x100 mm. a reduction of more than 20% in the sucrose level; after the first renewal of the rinse water the rate

d'élimination va décroissant; un troisième lavage est suffisant pour éviter le bleuissement.  elimination is decreasing; a third wash is sufficient to prevent blue stain.

-2- Ce dessevage peut également se faire par un lavage à l'eau courante,, ou par entrainement à la vapeur, ou par pulvérisation d'un solvant adéquat, le résultat étant, dans  -2- This drying can also be done by washing with running water, or by steam entrainment, or by spraying with a suitable solvent, the result being, in

tous les cas, I'élimination de 20% au moins, du saccharose contenu dans les planches.  in all cases, the elimination of at least 20% of the sucrose contained in the boards.

Nous avons déja vu que ce dessevage peut être complété, après séchage, par un  We have already seen that this drying can be completed, after drying, by a

traitement fongicide et insecticide.  fungicide and insecticide treatment.

Selon l'utilisation, le traitement peut être complété, après séchage, par un sel tetrakis, par des citrates de métaux alcalins, par un phosphate de guanylurée, par un  Depending on the use, the treatment can be supplemented, after drying, with a tetrakis salt, with alkali metal citrates, with a guanylurea phosphate, with a

pentaborate d'ammonium, par des composés halogénés, etc.. conférant au matériau une meilleure norme d'ignifugation.  ammonium pentaborate, by halogenated compounds, etc. giving the material a better fireproofing standard.

Selon l'utilisation, après séchage, le traitement peut rendre le matériau hydrofuge  Depending on the use, after drying, the treatment can make the material water-repellent

par imprégnation d'un hydrofuge du type oligomère rnméthylsiloxane ou autre.  by impregnating a water repellent of the rnmethylsiloxane or other oligomer type.

Selon l'utilisation, après séchage, le matériau peut recevoir un traitement de surface imperméabilisant et élastique du genre résine de copolymères PVC et alcool polyvinylique. Selon l'utilisation, après séchage, le matériau peut être durci par une imprégnation d'urée formol ou phénol formol ou diallyle phtalate ou métacrylate de méthyle, etc.  According to the use, after drying, the material can receive a waterproofing and elastic surface treatment of the resin type of PVC and polyvinyl alcohol copolymers. Depending on the use, after drying, the material can be hardened by impregnating urea formaldehyde or phenol formaldehyde or diallyl phthalate or methyl methacrylate, etc.

Selon l'utilisation, après séchage, le matériau peut être utilisé en sandwich entre deux ou plusieures autres matières.  Depending on the use, after drying, the material can be used sandwiched between two or more other materials.

0 Le matériau obtenu, d'une densité de 140 Kgim3 environ, convient pour tous les usages o il est requis des caractéristiques d'isolation thermique et phonique, de bonne  0 The material obtained, with a density of approximately 140 Kgim3, is suitable for all uses where thermal and sound insulation characteristics are required, of good

résistance au feu sans dégagement toxique, de légèreté et de solidité ainsi que d'un aspect esthétique intéressant.  fire resistance without toxic release, lightness and solidity as well as an interesting aesthetic aspect.

Claims (9)

REVENDICATIONS Matériau isolant phonique et thermique, autoextinguible sans dégagement de fumées toxiques, alliant une grande légèreté à une bonne résistance mécanique, obtenu à partir de monocotylédones, plus particulièrement de l'espèce des palmades. Ce matériau permet la constitution de panneaux isolants et de structures en sandwich.CLAIMS Sound and heat insulating material, self-extinguishing without release of toxic fumes, combining great lightness with good mechanical resistance, obtained from monocots, more particularly of the palmate species. This material allows the creation of insulating panels and sandwich structures. 1) Matériau caractérisé en ce qu'il n'est utilisable qu'après séchage, aussitot après  1) Material characterized in that it can only be used after drying, immediately after sciage, pour ramener le taux d'humidité au dessous de 25%,; idéalement, entre 18 et 19%.  sawing, to bring the humidity level below 25%; ideally between 18 and 19%. 2) Matériau, selon la revendication 1, caractérisé en ce que le séchage peut être précédé par un trempage préalable dans un insecticide et fongicide, qu'il s'agisse de pentachlorophénol, d'ammoniums quaternaires de cuivre,fluor,bore,arsenic, de  2) Material according to claim 1, characterized in that the drying can be preceded by a prior soaking in an insecticide and fungicide, whether it is pentachlorophenol, quaternary ammoniums of copper, fluorine, boron, arsenic, of cyperméthrine, de carbamates, etc...  cypermethrin, carbamates, etc. 3) Matériau, selon la revendication I, caractérisé en ce que le séchage peut être précédé par un dessevage par immersion dans un bain d'eau courante ou dans une cuve o l'eau serait brassée et renouvelée périodiquement, ou par entrainement à la vapeur, ou par pulvérisation d'un solvant adéquat, le résultat étant, dans tous les cas, l'élimination de 20%  3) Material according to claim I, characterized in that the drying can be preceded by a dessevage by immersion in a running water bath or in a tank where the water would be stirred and renewed periodically, or by steam entrainment , or by spraying with a suitable solvent, the result being, in all cases, the elimination of 20% au moins, du saccharose contenu dans la sève.  at least, sucrose contained in the sap. 4) Matériau, selon la revendication 1, caractérisé en ce qu'un traitement, apres séchage, par des sels tétrakis, par des citrates de métaux alcalins, par un phosphate de guanylurée, par un pentaborate d'ammonium, par des composés halogénés,etc. lui  4) Material according to claim 1, characterized in that a treatment, after drying, with tetrakis salts, with alkali metal citrates, with guanylurea phosphate, with ammonium pentaborate, with halogenated compounds, etc. him conférera une meilleure norme d'ignifugation.  will provide a better standard for fireproofing. 5) Matériau, selon la revendication I, caractérisé en ce que le traitement insecticide et fongicide peut également être exécuté après séchage, qu'il s'agisse d'ammoniurnms quaternaires de cuivre, fluor, bore arsenic, de cyperméthrine,de carbamates, etc.  5) Material according to claim I, characterized in that the insecticide and fungicide treatment can also be carried out after drying, whether it is quaternary ammonium hydroxides of copper, fluorine, boron arsenic, cypermethrin, carbamates, etc. . 6) Matériau, selon la revendication 1, caractérisé en ce qu'il peut être rendu hydrofuge, après séchage, par imprégnation d'un hydrofuge du type oligomère6) Material according to claim 1, characterized in that it can be made water repellent, after drying, by impregnating a water repellent of the oligomer type méthylsiloxane, ou autre.methylsiloxane, or the like. 7) Matériau, selon la revendication 1, caractérisé en ce qu 'il peut être imperméabilisé, après séchage, par un traitement de surface aux résines de copolymères  7) Material according to claim 1, characterized in that it can be waterproofed, after drying, by a surface treatment with copolymer resins PVC et alcool polyvinylique.PVC and polyvinyl alcohol. 8) Matériau, selon la revendication 1, caractérisé en ce qu'il peut être durci, après séchage,par une imprégniation d'urée formol ou phénol formol ou diallyle phtalate ou métacrylate de méthyle, etc.  8) Material according to claim 1, characterized in that it can be hardened, after drying, by an impregnation of urea formaldehyde or phenol formaldehyde or diallyl methyl phthalate or methacrylate, etc. 9) Matériau, selon la revendication 1, caractérisé en ce qu'il peut être utilisé, après9) Material according to claim 1, characterized in that it can be used, after séchage, en panneau sandwich entre deux ou plusieures autres matières.  drying, in sandwich panel between two or more other materials.
FR9902300A 1999-02-24 1999-02-24 Light solid sound-proofing and thermo-insulating material, generating no toxic gases on combustion, is obtained from monocotyledones from palmades species and optionally treated to Pending FR2789929A1 (en)

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FR9902300A FR2789929A1 (en) 1999-02-24 1999-02-24 Light solid sound-proofing and thermo-insulating material, generating no toxic gases on combustion, is obtained from monocotyledones from palmades species and optionally treated to

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FR9902300A FR2789929A1 (en) 1999-02-24 1999-02-24 Light solid sound-proofing and thermo-insulating material, generating no toxic gases on combustion, is obtained from monocotyledones from palmades species and optionally treated to

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116553555A (en) * 2023-07-07 2023-08-08 通威微电子有限公司 Synthesis method of large kilogram silicon carbide powder and silicon carbide powder

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116553555A (en) * 2023-07-07 2023-08-08 通威微电子有限公司 Synthesis method of large kilogram silicon carbide powder and silicon carbide powder
CN116553555B (en) * 2023-07-07 2023-09-26 通威微电子有限公司 Synthesis method of large kilogram of silicon carbide powder

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