FR2427322A1 - Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise - Google Patents

Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise

Info

Publication number
FR2427322A1
FR2427322A1 FR7915392A FR7915392A FR2427322A1 FR 2427322 A1 FR2427322 A1 FR 2427322A1 FR 7915392 A FR7915392 A FR 7915392A FR 7915392 A FR7915392 A FR 7915392A FR 2427322 A1 FR2427322 A1 FR 2427322A1
Authority
FR
France
Prior art keywords
crystallized sodium
preparation
paraformylphenolate
sodium
parahydroxymandelate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7915392A
Other languages
English (en)
French (fr)
Other versions
FR2427322B1 (US07714131-20100511-C00024.png
Inventor
Alain Schouteeten
Yani Christidis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sanofi Aventis France
Original Assignee
Francaise Hoechst Ste
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Francaise Hoechst Ste filed Critical Francaise Hoechst Ste
Priority to FR7915392A priority Critical patent/FR2427322A1/fr
Publication of FR2427322A1 publication Critical patent/FR2427322A1/fr
Priority to US06/284,835 priority patent/US4408070A/en
Application granted granted Critical
Publication of FR2427322B1 publication Critical patent/FR2427322B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/40—Unsaturated compounds
    • C07C59/42—Unsaturated compounds containing hydroxy or O-metal groups
    • C07C59/52—Unsaturated compounds containing hydroxy or O-metal groups a hydroxy or O-metal group being bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/39—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a secondary hydroxyl group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR7915392A 1979-06-15 1979-06-15 Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise Granted FR2427322A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
FR7915392A FR2427322A1 (fr) 1979-06-15 1979-06-15 Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise
US06/284,835 US4408070A (en) 1979-06-15 1981-07-20 Pure crystalline racemic sodium parahydroxymandelate, process for its preparation and uses thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7915392A FR2427322A1 (fr) 1979-06-15 1979-06-15 Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise

Publications (2)

Publication Number Publication Date
FR2427322A1 true FR2427322A1 (fr) 1979-12-28
FR2427322B1 FR2427322B1 (US07714131-20100511-C00024.png) 1983-12-16

Family

ID=9226680

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7915392A Granted FR2427322A1 (fr) 1979-06-15 1979-06-15 Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise

Country Status (2)

Country Link
US (1) US4408070A (US07714131-20100511-C00024.png)
FR (1) FR2427322A1 (US07714131-20100511-C00024.png)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0023459A1 (fr) * 1979-07-25 1981-02-04 SOCIETE FRANCAISE HOECHST Société anonyme dite: Procédé de préparation d'acides hydroxyarylglycoliques racémiques
WO1981000404A1 (en) * 1979-08-09 1981-02-19 Beecham Group Ltd Process for the isolation of a solid salt of p-hydroxy-mandelic acid;some salts of p-hydroxymandelic acid
FR2638740A1 (fr) * 1988-11-08 1990-05-11 Hoechst France Nouveau procede de fabrication industrielle du parahydroxymandelate de sodium
US5395964A (en) * 1993-05-28 1995-03-07 Societe Francaise Hoechst Preparation process for hydroxyphenylacetic acids

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2760745B1 (fr) * 1997-03-11 1999-05-28 Hoechst France Procede industriel de preparation en continu de l'orthohydroxymandelate de sodium

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR751687A (fr) * 1932-03-21 1933-09-07 J D Riedel E De Haen Ag Procédé pour la préparation d'éthers m-alcoyliques de l'aldéhyde protocatéchique
FR2132364A1 (US07714131-20100511-C00024.png) * 1971-03-31 1972-11-17 Haarmann & Reimer Gmbh
JPS51128934A (en) * 1975-04-30 1976-11-10 Ube Ind Ltd Process for preparing p-hydroxybenzaldehydes
BE867287A (fr) * 1978-05-19 1978-11-20 Ici Ltd Sel de metal alcalin de l'acide p-hydroxy-mandelique
ZA782655B (en) * 1977-05-26 1979-05-30 Ici Ltd Salt

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2062205A (en) * 1932-03-21 1936-11-24 Boedecker Friedrich Process of producing the m-alkylethers of protocatechuic aldehyde
US4163759A (en) * 1971-03-31 1979-08-07 Haarmann & Reimer Gesellschaft Mit Beschrankter Haftung Process for preparing aromatic hydroxyaldehydes
US4165341A (en) * 1977-02-04 1979-08-21 Ube Industries, Ltd. Process for preparing protocatechualdehyde and its derivatives
SE441524B (sv) * 1978-05-19 1985-10-14 Ici Ltd Fast natrium- eller kalium-p-hydroximandelat-monohydrat och sett for dess framstellning
FR2456722A1 (fr) * 1979-05-14 1980-12-12 Hoechst France Parformylphenolate de sodium cristallise, son procede de preparation et son application

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR751687A (fr) * 1932-03-21 1933-09-07 J D Riedel E De Haen Ag Procédé pour la préparation d'éthers m-alcoyliques de l'aldéhyde protocatéchique
FR2132364A1 (US07714131-20100511-C00024.png) * 1971-03-31 1972-11-17 Haarmann & Reimer Gmbh
JPS51128934A (en) * 1975-04-30 1976-11-10 Ube Ind Ltd Process for preparing p-hydroxybenzaldehydes
ZA782655B (en) * 1977-05-26 1979-05-30 Ici Ltd Salt
BE867287A (fr) * 1978-05-19 1978-11-20 Ici Ltd Sel de metal alcalin de l'acide p-hydroxy-mandelique

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
CA1977 *
CA1979 *

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0023459A1 (fr) * 1979-07-25 1981-02-04 SOCIETE FRANCAISE HOECHST Société anonyme dite: Procédé de préparation d'acides hydroxyarylglycoliques racémiques
WO1981000254A1 (fr) * 1979-07-25 1981-02-05 Hoechst France Procede de preparation d'acides hydroxyarylglycoliques racemiques et produits nouveaux en resultant
WO1981000404A1 (en) * 1979-08-09 1981-02-19 Beecham Group Ltd Process for the isolation of a solid salt of p-hydroxy-mandelic acid;some salts of p-hydroxymandelic acid
EP0024181A1 (en) * 1979-08-09 1981-02-25 Beecham Group Plc Process for the isolation of a solid salt of p-hydroxymandelic acid; some salts of p-hydroxymandelic acid
FR2638740A1 (fr) * 1988-11-08 1990-05-11 Hoechst France Nouveau procede de fabrication industrielle du parahydroxymandelate de sodium
EP0368696A1 (fr) * 1988-11-08 1990-05-16 Societe Francaise Hoechst Nouveau procédé de fabrication industrielle du parahydroxymandélate de sodium
US4978784A (en) * 1988-11-08 1990-12-18 Societe Francaise Hoechst Process for industrial manufacture of sodium parahydroxymandelate
US5395964A (en) * 1993-05-28 1995-03-07 Societe Francaise Hoechst Preparation process for hydroxyphenylacetic acids

Also Published As

Publication number Publication date
FR2427322B1 (US07714131-20100511-C00024.png) 1983-12-16
US4408070A (en) 1983-10-04

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