FR2383908A1 - Procede de preparationd'acide vinyllactique et de ses esters - Google Patents
Procede de preparationd'acide vinyllactique et de ses estersInfo
- Publication number
- FR2383908A1 FR2383908A1 FR7807598A FR7807598A FR2383908A1 FR 2383908 A1 FR2383908 A1 FR 2383908A1 FR 7807598 A FR7807598 A FR 7807598A FR 7807598 A FR7807598 A FR 7807598A FR 2383908 A1 FR2383908 A1 FR 2383908A1
- Authority
- FR
- France
- Prior art keywords
- esters
- preparation
- acid
- vinyllactic acid
- vinyllactic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- SXQCPXKZTFJHQI-UHFFFAOYSA-N 2-hydroxy-2-methylbut-3-enoic acid Chemical compound C=CC(O)(C)C(O)=O SXQCPXKZTFJHQI-UHFFFAOYSA-N 0.000 title 1
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 abstract 2
- LBRDQQPGFNRZGV-UHFFFAOYSA-N 1,1-dimethoxy-2-methylbut-3-en-2-ol Chemical compound COC(OC)C(C)(O)C=C LBRDQQPGFNRZGV-UHFFFAOYSA-N 0.000 abstract 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 abstract 1
- 239000005751 Copper oxide Substances 0.000 abstract 1
- 229910000431 copper oxide Inorganic materials 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 239000007800 oxidant agent Substances 0.000 abstract 1
- 229910001923 silver oxide Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/40—Unsaturated compounds
- C07C59/42—Unsaturated compounds containing hydroxy or O-metal groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
- C07C45/515—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups the singly bound functional group being an acetalised, ketalised hemi-acetalised, or hemi-ketalised hydroxyl group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C47/00—Compounds having —CHO groups
- C07C47/20—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms
- C07C47/26—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms containing hydroxy groups
- C07C47/263—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms containing hydroxy groups acyclic
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
L'invention a pour objet un procédé de préparation d'acide vinyllactique et de ses esters, caractérisé par le fait que l'on oxyde de l'aldéhyde vinyllactique avec un oxydant, en présence d'oxyde de cuivre et d'oxyde d'argent, à une température comprise entre 25 degrés et 70 degrés C, à un pH compris entre 8 et 10, et sous une pression de 1 à 26 atm. et l'on estérifie de façon habituelle, le cas échéant, l'acide vinyllactique ainsi obtenu.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19772711381 DE2711381A1 (de) | 1977-03-16 | 1977-03-16 | Verfahren zur herstellung von vinylmilchsaeure und ihren estern |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2383908A1 true FR2383908A1 (fr) | 1978-10-13 |
FR2383908B1 FR2383908B1 (fr) | 1984-02-17 |
Family
ID=6003751
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7807598A Granted FR2383908A1 (fr) | 1977-03-16 | 1978-03-16 | Procede de preparationd'acide vinyllactique et de ses esters |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS53116318A (fr) |
CH (1) | CH640816A5 (fr) |
DE (1) | DE2711381A1 (fr) |
FR (1) | FR2383908A1 (fr) |
HU (1) | HU176748B (fr) |
IT (1) | IT1105168B (fr) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0648735A1 (fr) * | 1993-10-13 | 1995-04-19 | F. Hoffmann-La Roche Ag | Préparation d'un intermédiaire pour l'acétate de la vitamine A |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1017618A (en) * | 1963-05-07 | 1966-01-19 | Snam Spa | Process for the preparation of hydroxyaldehydes and derivatives thereof |
-
1977
- 1977-03-16 DE DE19772711381 patent/DE2711381A1/de not_active Withdrawn
-
1978
- 1978-03-13 JP JP2782378A patent/JPS53116318A/ja active Pending
- 1978-03-13 CH CH270478A patent/CH640816A5/de not_active IP Right Cessation
- 1978-03-14 HU HU78BA3638A patent/HU176748B/hu not_active IP Right Cessation
- 1978-03-14 IT IT48423/78A patent/IT1105168B/it active
- 1978-03-16 FR FR7807598A patent/FR2383908A1/fr active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1017618A (en) * | 1963-05-07 | 1966-01-19 | Snam Spa | Process for the preparation of hydroxyaldehydes and derivatives thereof |
Non-Patent Citations (1)
Title |
---|
EXBK/77 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0648735A1 (fr) * | 1993-10-13 | 1995-04-19 | F. Hoffmann-La Roche Ag | Préparation d'un intermédiaire pour l'acétate de la vitamine A |
US5453547A (en) * | 1993-10-13 | 1995-09-26 | Hoffman-La Roche Inc. | Process for the manufacture of gamma-acetoxytiglic aldehyde |
Also Published As
Publication number | Publication date |
---|---|
DE2711381A1 (de) | 1978-09-21 |
IT7848423A0 (it) | 1978-03-14 |
CH640816A5 (en) | 1984-01-31 |
FR2383908B1 (fr) | 1984-02-17 |
HU176748B (en) | 1981-05-28 |
JPS53116318A (en) | 1978-10-11 |
IT1105168B (it) | 1985-10-28 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |