FR2353488A1 - Americium dioxide prepn. from americium nitrate - and oxalic acid, with thermal decarboxylation of americium oxalate - Google Patents

Americium dioxide prepn. from americium nitrate - and oxalic acid, with thermal decarboxylation of americium oxalate

Info

Publication number
FR2353488A1
FR2353488A1 FR7716956A FR7716956A FR2353488A1 FR 2353488 A1 FR2353488 A1 FR 2353488A1 FR 7716956 A FR7716956 A FR 7716956A FR 7716956 A FR7716956 A FR 7716956A FR 2353488 A1 FR2353488 A1 FR 2353488A1
Authority
FR
France
Prior art keywords
americium
oxalate
nitrate
oxalic acid
prepn
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7716956A
Other languages
French (fr)
Other versions
FR2353488B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Alkem GmbH
Original Assignee
Alkem GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alkem GmbH filed Critical Alkem GmbH
Publication of FR2353488A1 publication Critical patent/FR2353488A1/en
Application granted granted Critical
Publication of FR2353488B1 publication Critical patent/FR2353488B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G56/00—Compounds of transuranic elements
    • C01G56/007—Compounds of transuranic elements
    • C01G56/009—Compounds of americium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41—Preparation of salts of carboxylic acids
    • C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

AmO2 is prepd. from a soln. of Am nitrate by (1) neutralising the soln. by adding NH3 in a quantity up to 1M HNO3 per litre and then adding oxalic acid pref. as solid, (2) adjusting the Ph to 2.5 by addn. of NH3 or NH4OH to ppte. Am oxalate which is sepd. by filration and (3) calcining the Am oxalate at 450-800 degrees to form AmO2. Before sepn. of the Am oxalate, the reaction liq and suspension obtd are maintained in circulation for about 1 hr.
FR7716956A 1976-06-04 1977-06-03 Americium dioxide prepn. from americium nitrate - and oxalic acid, with thermal decarboxylation of americium oxalate Granted FR2353488A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19762625355 DE2625355C2 (en) 1976-06-04 1976-06-04 Process for the discontinuous production of americium dioxide

Publications (2)

Publication Number Publication Date
FR2353488A1 true FR2353488A1 (en) 1977-12-30
FR2353488B1 FR2353488B1 (en) 1981-08-14

Family

ID=5979911

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7716956A Granted FR2353488A1 (en) 1976-06-04 1977-06-03 Americium dioxide prepn. from americium nitrate - and oxalic acid, with thermal decarboxylation of americium oxalate

Country Status (5)

Country Link
JP (1) JPS52149294A (en)
BE (1) BE855368A (en)
DE (1) DE2625355C2 (en)
ES (1) ES459153A1 (en)
FR (1) FR2353488A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62282832A (en) * 1986-05-30 1987-12-08 Nitto Seiko Co Ltd Parts automatic clamping method and automatic clamping machine therefor

Also Published As

Publication number Publication date
DE2625355C2 (en) 1985-09-19
DE2625355A1 (en) 1977-12-15
JPS611375B2 (en) 1986-01-16
FR2353488B1 (en) 1981-08-14
JPS52149294A (en) 1977-12-12
BE855368A (en) 1977-10-03
ES459153A1 (en) 1978-04-16

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Legal Events

Date Code Title Description
ST Notification of lapse