FR2318156A1 - Procede de purification de l'a-amino-e-caprolactame - Google Patents
Procede de purification de l'a-amino-e-caprolactameInfo
- Publication number
- FR2318156A1 FR2318156A1 FR7621690A FR7621690A FR2318156A1 FR 2318156 A1 FR2318156 A1 FR 2318156A1 FR 7621690 A FR7621690 A FR 7621690A FR 7621690 A FR7621690 A FR 7621690A FR 2318156 A1 FR2318156 A1 FR 2318156A1
- Authority
- FR
- France
- Prior art keywords
- caprolactam
- purificn
- crystallisation
- traces
- alpha
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title abstract 4
- 239000011358 absorbing material Substances 0.000 title 1
- 238000002425 crystallisation Methods 0.000 title 1
- 239000000463 material Substances 0.000 title 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- 239000002904 solvent Substances 0.000 abstract 2
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 abstract 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 abstract 1
- 125000005907 alkyl ester group Chemical group 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D223/12—Nitrogen atoms not forming part of a nitro radical
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8669275A JPS5212187A (en) | 1975-07-17 | 1975-07-17 | Method of purifying alpha-amino-epsilon- caprolactam |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2318156A1 true FR2318156A1 (fr) | 1977-02-11 |
| FR2318156B1 FR2318156B1 (https=) | 1980-09-26 |
Family
ID=13894007
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7621690A Granted FR2318156A1 (fr) | 1975-07-17 | 1976-07-15 | Procede de purification de l'a-amino-e-caprolactame |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JPS5212187A (https=) |
| FR (1) | FR2318156A1 (https=) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1490312A (fr) * | 1965-09-11 | 1967-07-28 | Zimmer Ag Hans J | Procédé perfectionné de purification de l'epsilon-caprolactame |
| FR2185623A1 (https=) * | 1972-05-19 | 1974-01-04 | Bayer Ag | |
| US3898213A (en) * | 1974-06-06 | 1975-08-05 | Allied Chem | Separation of {60 -amino-{107 -lactams |
-
1975
- 1975-07-17 JP JP8669275A patent/JPS5212187A/ja active Pending
-
1976
- 1976-07-15 FR FR7621690A patent/FR2318156A1/fr active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1490312A (fr) * | 1965-09-11 | 1967-07-28 | Zimmer Ag Hans J | Procédé perfectionné de purification de l'epsilon-caprolactame |
| FR2185623A1 (https=) * | 1972-05-19 | 1974-01-04 | Bayer Ag | |
| US3898213A (en) * | 1974-06-06 | 1975-08-05 | Allied Chem | Separation of {60 -amino-{107 -lactams |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5212187A (en) | 1977-01-29 |
| FR2318156B1 (https=) | 1980-09-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |