FR2234037A1 - Growing single crystals - by seeding of agitated, temp-controlled supersaturated soln - Google Patents
Growing single crystals - by seeding of agitated, temp-controlled supersaturated solnInfo
- Publication number
- FR2234037A1 FR2234037A1 FR7323051A FR7323051A FR2234037A1 FR 2234037 A1 FR2234037 A1 FR 2234037A1 FR 7323051 A FR7323051 A FR 7323051A FR 7323051 A FR7323051 A FR 7323051A FR 2234037 A1 FR2234037 A1 FR 2234037A1
- Authority
- FR
- France
- Prior art keywords
- crystal
- agitators
- supersaturated
- soln
- rising currents
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
Supersaturated soln. of chemical to be crystallised is agitated sufficiently to ensure homogeneity, thereby promoting perfect crystal morphology, without producing excessive velocity past the crystal which could affect the crystal form. The agitators used form rising currents of small cross-sectional area in locations away from the growing crystal; the resulting downflow occurs across the rest of the cross-sectional area of containing vessel and is of low velocity. A pref. configuration is of three rising currents forming, in plan, the points of an equilateral triangle with the crystal at the point of intersection of the three axes of symmetry. An alternative configuration is of several rising currents forming, in plan, the centre and points of a regular polygon with several crystals each on an axis of symmetry of the equilateral triangles constituting the polygon. Agitators need only be immersed superficially in the fluid, and regular disposition of the agitators permits homogenisation of large free columns of fluid.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7323051A FR2234037A1 (en) | 1973-06-25 | 1973-06-25 | Growing single crystals - by seeding of agitated, temp-controlled supersaturated soln |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7323051A FR2234037A1 (en) | 1973-06-25 | 1973-06-25 | Growing single crystals - by seeding of agitated, temp-controlled supersaturated soln |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2234037A1 true FR2234037A1 (en) | 1975-01-17 |
FR2234037B1 FR2234037B1 (en) | 1976-09-17 |
Family
ID=9121486
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7323051A Granted FR2234037A1 (en) | 1973-06-25 | 1973-06-25 | Growing single crystals - by seeding of agitated, temp-controlled supersaturated soln |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2234037A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2531635A1 (en) * | 2010-02-01 | 2012-12-12 | Michael Krautter | Device for crystal growth at intermediate temperatures using controlled semi-active cooling |
-
1973
- 1973-06-25 FR FR7323051A patent/FR2234037A1/en active Granted
Non-Patent Citations (1)
Title |
---|
NEANT * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2531635A1 (en) * | 2010-02-01 | 2012-12-12 | Michael Krautter | Device for crystal growth at intermediate temperatures using controlled semi-active cooling |
EP2531635A4 (en) * | 2010-02-01 | 2014-01-01 | Michael Krautter | Device for crystal growth at intermediate temperatures using controlled semi-active cooling |
Also Published As
Publication number | Publication date |
---|---|
FR2234037B1 (en) | 1976-09-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
CD | Change of name or company name | ||
ST | Notification of lapse |