FR2119624A5 - Defluorescence of cresol - for tricresyl phosphate prepn by treatment with acid and distillation - Google Patents
Defluorescence of cresol - for tricresyl phosphate prepn by treatment with acid and distillationInfo
- Publication number
- FR2119624A5 FR2119624A5 FR7146162A FR7146162A FR2119624A5 FR 2119624 A5 FR2119624 A5 FR 2119624A5 FR 7146162 A FR7146162 A FR 7146162A FR 7146162 A FR7146162 A FR 7146162A FR 2119624 A5 FR2119624 A5 FR 2119624A5
- Authority
- FR
- France
- Prior art keywords
- acid
- treatment
- cresol
- defluorescence
- prepn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/82—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/86—Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Cresol (I) is purified by treatment with an acid to free it from fluorescent materials. Pref. 0.01-10 pts. of acid/100 pts. (I) is used where the acid is pref. mineral (HCl), Friedel-Crafts catalyst (AlCl3), oxide (alumina) or cation exchange resin. Treatment temp. is 30-600 degrees C for 5 min-10 hrs. Fluorescence is undesirable where (I) is used as plasticiser for PVC, and this treatment eliminates it.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11833870 | 1970-12-23 | ||
JP12997370A JPS541289B1 (en) | 1970-12-28 | 1970-12-28 |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2119624A5 true FR2119624A5 (en) | 1972-08-04 |
Family
ID=26456296
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7146162A Expired FR2119624A5 (en) | 1970-12-23 | 1971-12-22 | Defluorescence of cresol - for tricresyl phosphate prepn by treatment with acid and distillation |
Country Status (5)
Country | Link |
---|---|
BE (1) | BE777196A (en) |
DE (1) | DE2164266A1 (en) |
FR (1) | FR2119624A5 (en) |
IT (1) | IT943342B (en) |
NL (1) | NL7117738A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2365544A1 (en) * | 1976-09-24 | 1978-04-21 | Stamicarbon | PROCESS FOR THE PURIFICATION OF A PHENOL PREPARED BY OXIDATION OF AN ALKYLBENZENIC COMPOUND |
-
1971
- 1971-12-22 IT IT7120071A patent/IT943342B/en active
- 1971-12-22 FR FR7146162A patent/FR2119624A5/en not_active Expired
- 1971-12-23 DE DE19712164266 patent/DE2164266A1/en active Pending
- 1971-12-23 BE BE777196A patent/BE777196A/en unknown
- 1971-12-23 NL NL7117738A patent/NL7117738A/xx unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2365544A1 (en) * | 1976-09-24 | 1978-04-21 | Stamicarbon | PROCESS FOR THE PURIFICATION OF A PHENOL PREPARED BY OXIDATION OF AN ALKYLBENZENIC COMPOUND |
Also Published As
Publication number | Publication date |
---|---|
NL7117738A (en) | 1972-06-27 |
DE2164266A1 (en) | 1972-07-13 |
BE777196A (en) | 1972-06-23 |
IT943342B (en) | 1973-04-02 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |