FR2102540A5 - Sepn of sulphonic acids - from solns also contg sulphuric water and unsulphonated hydrocarbons - Google Patents
Sepn of sulphonic acids - from solns also contg sulphuric water and unsulphonated hydrocarbonsInfo
- Publication number
- FR2102540A5 FR2102540A5 FR7029211A FR7029211A FR2102540A5 FR 2102540 A5 FR2102540 A5 FR 2102540A5 FR 7029211 A FR7029211 A FR 7029211A FR 7029211 A FR7029211 A FR 7029211A FR 2102540 A5 FR2102540 A5 FR 2102540A5
- Authority
- FR
- France
- Prior art keywords
- contg
- solns
- sulphonic acids
- unsulphonated
- sepn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
- C07C303/44—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Sulphonic acid soln. is degassed soln. and one or more weakly polar alcohols contg. at least 5C atoms, in the molecule, are added to separate the mixture into an org. phase contg. all of the sulphonic acids, and an aqs. phase contg. almost all of the H2SO4. The aqs. phase is separated and the organic phase is treated to separate the sulphonic acids in the form of the free acids on their acetal, salts. This procedure is esp. suitable for treating crude sulphonic solns. produced by the sulphoxidation of n-paraffins contg. 7-30 pref. 10-20C atoms.
Priority Applications (21)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7029211A FR2102540A5 (en) | 1970-08-07 | 1970-08-07 | Sepn of sulphonic acids - from solns also contg sulphuric water and unsulphonated hydrocarbons |
IT27087/71A IT941650B (en) | 1970-08-07 | 1971-08-03 | PROCEDURE FOR THE PREPARATION OF SULFONIC ACIDS AND SULPHONATES |
YU2016/71A YU35756B (en) | 1970-08-07 | 1971-08-03 | Process for the separation of sulfonic acids |
BG018229A BG20344A3 (en) | 1970-08-07 | 1971-08-03 | METHOD FOR SEPARATION OF SULFONIC ACIDS AND SULFONATES |
CH1142271A CH534670A (en) | 1970-08-07 | 1971-08-03 | Process for the separation of sulfonic acids contained in a crude sulfonic solution |
LU63662D LU63662A1 (en) | 1970-08-07 | 1971-08-04 | |
HUPE788A HU166904B (en) | 1970-08-07 | 1971-08-04 | |
NO2945/71A NO135635C (en) | 1970-08-07 | 1971-08-05 | |
ES393940A ES393940A1 (en) | 1970-08-07 | 1971-08-05 | Procedure for the separation of sulphonic acids contained in a gross sulphonic solution. (Machine-translation by Google Translate, not legally binding) |
SE7110050A SE382631B (en) | 1970-08-07 | 1971-08-05 | PROCEDURE FOR THE PREPARATION OF PARAFFIN SULPONATES FROM CLEAN AUTO DISPOSAL OF SULPHONIC ACIDS OF PARAFFINS, WHICH SOLUTION ALSO CONTAINS SULFUR ACID AND NON-SULPHONATED CARBON |
CS570171A CS171252B2 (en) | 1970-08-07 | 1971-08-05 | |
CA120,040*7A CA952122A (en) | 1970-08-07 | 1971-08-06 | Preparation des acides sulfoniques et des sulfonates |
SU711684922A SU791225A3 (en) | 1970-08-07 | 1971-08-06 | Method of producing alkaline metal alkane sulfonates |
BE771038A BE771038A (en) | 1970-08-07 | 1971-08-06 | PERFECTION IN THE PREPARATION OF SULPHONIC ACIDS AND SULPHONATES |
NLAANVRAGE7110917,A NL170281B (en) | 1970-08-07 | 1971-08-06 | PROCESS FOR SEPARATING ALPHANE SULFONIC ACIDS FROM A RAW SULFONIC ACID SOLUTION. |
GB3707571A GB1358095A (en) | 1970-08-07 | 1971-08-06 | Sulphonic acids and sulphonates |
DE19712139477 DE2139477A1 (en) | 1970-08-07 | 1971-08-06 | Process for the separation of sulphonic acids from a sulphonation mixture |
RO67930A RO62196A (en) | 1970-08-07 | 1971-08-07 | |
JP46059871A JPS505689B1 (en) | 1970-08-07 | 1971-08-07 | |
US05/895,549 US4178307A (en) | 1970-08-07 | 1978-04-12 | Process for preparing sulphonic acids and sulphonates |
US05/895,795 US4177208A (en) | 1970-08-07 | 1978-04-12 | Process for preparing sulphonic acids and sulphonates |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7029211A FR2102540A5 (en) | 1970-08-07 | 1970-08-07 | Sepn of sulphonic acids - from solns also contg sulphuric water and unsulphonated hydrocarbons |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2102540A5 true FR2102540A5 (en) | 1972-04-07 |
Family
ID=9059966
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7029211A Expired FR2102540A5 (en) | 1970-08-07 | 1970-08-07 | Sepn of sulphonic acids - from solns also contg sulphuric water and unsulphonated hydrocarbons |
Country Status (4)
Country | Link |
---|---|
CS (1) | CS171252B2 (en) |
ES (1) | ES393940A1 (en) |
FR (1) | FR2102540A5 (en) |
SU (1) | SU791225A3 (en) |
-
1970
- 1970-08-07 FR FR7029211A patent/FR2102540A5/en not_active Expired
-
1971
- 1971-08-05 ES ES393940A patent/ES393940A1/en not_active Expired
- 1971-08-05 CS CS570171A patent/CS171252B2/cs unknown
- 1971-08-06 SU SU711684922A patent/SU791225A3/en active
Also Published As
Publication number | Publication date |
---|---|
SU791225A3 (en) | 1980-12-23 |
CS171252B2 (en) | 1976-10-29 |
ES393940A1 (en) | 1974-07-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
TP | Transmission of property | ||
ST | Notification of lapse |