FR2067844A5 - Lithium dialuminium heptahydride prepn - Google Patents
Lithium dialuminium heptahydride prepnInfo
- Publication number
- FR2067844A5 FR2067844A5 FR6939718A FR6939718A FR2067844A5 FR 2067844 A5 FR2067844 A5 FR 2067844A5 FR 6939718 A FR6939718 A FR 6939718A FR 6939718 A FR6939718 A FR 6939718A FR 2067844 A5 FR2067844 A5 FR 2067844A5
- Authority
- FR
- France
- Prior art keywords
- heptahydride
- dialuminium
- prepn
- lithium
- lial2h7
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- FPBFIOYAKGHRLY-UHFFFAOYSA-N alumane;lithium Chemical compound [Li].[AlH3].[AlH3] FPBFIOYAKGHRLY-UHFFFAOYSA-N 0.000 title 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 3
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract 2
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 229960004132 diethyl ether Drugs 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
- C01B6/24—Hydrides containing at least two metals; Addition complexes thereof
- C01B6/243—Hydrides containing at least two metals; Addition complexes thereof containing only hydrogen, aluminium and alkali metals, e.g. Li(AlH4)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
LiAl2H7 is prepared by reacting LiH of particle size 1mu with AlCl3 in a diethylether soln. under inert gas. The reaction is effected for 8-15 hrs. at 5 degrees C. The process is simple and easy to control, and does not involve the use of expensive chemicals necessitated by prior art. The Cpd. is used as an extremely specific reducing agent.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR6939718A FR2067844A5 (en) | 1969-11-19 | 1969-11-19 | Lithium dialuminium heptahydride prepn |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR6939718A FR2067844A5 (en) | 1969-11-19 | 1969-11-19 | Lithium dialuminium heptahydride prepn |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2067844A5 true FR2067844A5 (en) | 1971-08-20 |
Family
ID=9043273
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR6939718A Expired FR2067844A5 (en) | 1969-11-19 | 1969-11-19 | Lithium dialuminium heptahydride prepn |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2067844A5 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999019250A1 (en) * | 1997-10-10 | 1999-04-22 | Mcgill University | Method of fabrication of complex alkali metal hydrides |
-
1969
- 1969-11-19 FR FR6939718A patent/FR2067844A5/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999019250A1 (en) * | 1997-10-10 | 1999-04-22 | Mcgill University | Method of fabrication of complex alkali metal hydrides |
US6251349B1 (en) | 1997-10-10 | 2001-06-26 | Mcgill University | Method of fabrication of complex alkali metal hydrides |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
TP | Transmission of property | ||
ST | Notification of lapse |