FI991563A - Process for processing mother liquor in a urea phosphate process - Google Patents
Process for processing mother liquor in a urea phosphate process Download PDFInfo
- Publication number
- FI991563A FI991563A FI991563A FI991563A FI991563A FI 991563 A FI991563 A FI 991563A FI 991563 A FI991563 A FI 991563A FI 991563 A FI991563 A FI 991563A FI 991563 A FI991563 A FI 991563A
- Authority
- FI
- Finland
- Prior art keywords
- urea
- ammonium phosphate
- mother liquor
- solution
- urea phosphate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/28—Ammonium phosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
- Catalysts (AREA)
- Paper (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
A method for manufacturing a solid product containing nitrogen and phosphor, particular a solid ammonium phosphate and/or urea ammonium phosphate product, in which method the solution containing urea and phosphoric acid is heated. Water then evaporates from the solution and the urea in the solution decomposes into ammonia and carbon dioxide. The carbon dioxide exits the reactor together with water vapor; the generated ammonia neutralizes the phosphoric acid. A suspension containing ammonium phosphate and/or urea ammonium phosphate is obtained, which is solidified, dried, crushed, ground and/or granulated. The end product as such can be used as a fertilizer or it can be used as part of a mixed fertilizer.
Priority Applications (17)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI991563A FI116288B (en) | 1999-07-08 | 1999-07-08 | Method for treating the mother liquor of the urea phosphate process |
JO2000106A JO2185B1 (en) | 1999-07-08 | 2000-07-03 | Method for treating fertilizer process solutions |
SI200030436T SI1220815T1 (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
CNB008100535A CN1223512C (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
AU58330/00A AU768441B2 (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
PCT/FI2000/000623 WO2001004048A1 (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
AT00944094T ATE265392T1 (en) | 1999-07-08 | 2000-07-06 | METHOD FOR TREATING SOLUTIONS FROM FERTILIZER PRODUCTION |
US10/030,263 US6821311B1 (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
ES00944094T ES2220485T3 (en) | 1999-07-08 | 2000-07-06 | METHOD FOR THE TREATMENT OF DISSOLUTIONS OF PROCESSES OF PRODUCTION OF FERTILIZERS. |
DE60010300T DE60010300T2 (en) | 1999-07-08 | 2000-07-06 | METHOD FOR TREATING SOLUTIONS FROM FERTILIZER PRODUCTION |
TR2002/00003T TR200200003T2 (en) | 1999-07-08 | 2000-07-06 | The method of processing fertilizer process solutions. |
PT00944094T PT1220815E (en) | 1999-07-08 | 2000-07-06 | PROCESS FOR TREATING SOLUTIONS OF FERTILIZER PROCESSES |
EP00944094A EP1220815B1 (en) | 1999-07-08 | 2000-07-06 | Method for treating fertilizer process solutions |
BRPI0012259-9A BR0012259B1 (en) | 1999-07-08 | 2000-07-06 | A method for making a solid product of ammonium dihydrogen phosphate and / or ammonium urea phosphate. |
MYPI20003138 MY123489A (en) | 1999-07-08 | 2000-07-07 | Method for treating fertilizer process solutions |
SA00210454A SA00210454B1 (en) | 1999-07-08 | 2000-10-17 | A method for treating fertilizer solutions |
MA26466A MA25874A1 (en) | 1999-07-08 | 2002-01-03 | METHOD FOR THE TREATMENT OF PROCESS SOLUTIONS FOR FERTILIZERS. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI991563 | 1999-07-08 | ||
FI991563A FI116288B (en) | 1999-07-08 | 1999-07-08 | Method for treating the mother liquor of the urea phosphate process |
Publications (2)
Publication Number | Publication Date |
---|---|
FI991563A true FI991563A (en) | 2001-01-09 |
FI116288B FI116288B (en) | 2005-10-31 |
Family
ID=8555044
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FI991563A FI116288B (en) | 1999-07-08 | 1999-07-08 | Method for treating the mother liquor of the urea phosphate process |
Country Status (17)
Country | Link |
---|---|
US (1) | US6821311B1 (en) |
EP (1) | EP1220815B1 (en) |
CN (1) | CN1223512C (en) |
AT (1) | ATE265392T1 (en) |
AU (1) | AU768441B2 (en) |
BR (1) | BR0012259B1 (en) |
DE (1) | DE60010300T2 (en) |
ES (1) | ES2220485T3 (en) |
FI (1) | FI116288B (en) |
JO (1) | JO2185B1 (en) |
MA (1) | MA25874A1 (en) |
MY (1) | MY123489A (en) |
PT (1) | PT1220815E (en) |
SA (1) | SA00210454B1 (en) |
SI (1) | SI1220815T1 (en) |
TR (1) | TR200200003T2 (en) |
WO (1) | WO2001004048A1 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IL135432A0 (en) * | 2000-04-03 | 2001-05-20 | Rotem Amfert Negev Ltd | Improved solubility fertilizer compounds and compositions |
US7641881B2 (en) * | 2006-04-21 | 2010-01-05 | Hce, Llc | Fertilizer production from fossil fuel with minimal carbon dioxide emission |
EP2192099A1 (en) * | 2008-11-28 | 2010-06-02 | Uhde Fertilizer Technology B.V. | Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules |
RU2510626C1 (en) * | 2012-10-16 | 2014-04-10 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Башкирский государственный университет" | Method of obtaining liquid complex fertilisers |
RU2527794C1 (en) * | 2013-01-16 | 2014-09-10 | Открытое акционерное общество "Научно-исследовательский институт по удобрениям и инсектофунгицидам им. проф. Я.В. Самойлова" (ОАО "НИУИФ") | Method of production of complex fertiliser |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
USRE29149E (en) * | 1957-03-29 | 1977-03-08 | Union Oil Company Of California | Production of ammonium phosphates and product thereof |
US3333939A (en) | 1965-04-05 | 1967-08-01 | Arizona Agrochemical Corp | Discrete fertilizer granule containing a urea compound, sulfur and a phosphate plant food |
FR1558585A (en) * | 1968-01-18 | 1969-02-28 | ||
CA939876A (en) * | 1968-12-30 | 1974-01-15 | Ronald H. Carlson | Preparation of phosphates |
BE760491A (en) | 1970-01-09 | 1971-05-27 | Ugine Kuhlmann | PROCESS FOR OBTAINING NEW REACTION PRODUCTS OF PHOSPHORIC ACID, UREA AND AMMONIA, AND THEIR APPLICATIONS AS FERTILIZERS |
US3723086A (en) * | 1971-05-20 | 1973-03-27 | P Poynor | Process for producing ammonium phosphates and polyphosphates |
JPS537920B2 (en) | 1972-05-24 | 1978-03-23 | ||
DE2308408A1 (en) | 1973-02-21 | 1974-08-29 | Basf Ag | Water-soluble ammonium polyphosphates prodn. - by two-stage thermal decomposition of urea phosphate |
NL7417042A (en) * | 1974-01-16 | 1975-07-18 | Fisons Ltd | PROCESS FOR THE PREPARATION OF AMMONIUM PHOSPHATES. |
GB1483739A (en) * | 1974-09-13 | 1977-08-24 | Scottish Agricultural Ltd | Manufacture of solid ammonium phosphate |
US3985538A (en) * | 1974-10-24 | 1976-10-12 | Tennessee Valley Authority | Pipe reactor-continuous ammoniator process for production of granular phosphates |
SU608519A1 (en) * | 1974-11-26 | 1978-05-30 | Предприятие П/Я Г-4302 | Method of obtaining fodder additive based on urea phosphate |
UST969002I4 (en) * | 1977-07-25 | 1978-04-04 | Tennessee Valley Authority | Granular ammonium phosphate sulfate and urea-ammonium phosphate sulfate using a common pipe-cross reactor |
US4461913A (en) | 1981-11-24 | 1984-07-24 | Tennessee Valley Authority | Production of urea phosphate |
US5171349A (en) * | 1991-01-31 | 1992-12-15 | Vetanovetz Richard P | Solubility compound fertilizer compositions |
-
1999
- 1999-07-08 FI FI991563A patent/FI116288B/en not_active IP Right Cessation
-
2000
- 2000-07-03 JO JO2000106A patent/JO2185B1/en active
- 2000-07-06 ES ES00944094T patent/ES2220485T3/en not_active Expired - Lifetime
- 2000-07-06 SI SI200030436T patent/SI1220815T1/en unknown
- 2000-07-06 AU AU58330/00A patent/AU768441B2/en not_active Ceased
- 2000-07-06 US US10/030,263 patent/US6821311B1/en not_active Expired - Lifetime
- 2000-07-06 TR TR2002/00003T patent/TR200200003T2/en unknown
- 2000-07-06 WO PCT/FI2000/000623 patent/WO2001004048A1/en active IP Right Grant
- 2000-07-06 PT PT00944094T patent/PT1220815E/en unknown
- 2000-07-06 EP EP00944094A patent/EP1220815B1/en not_active Expired - Lifetime
- 2000-07-06 AT AT00944094T patent/ATE265392T1/en active
- 2000-07-06 DE DE60010300T patent/DE60010300T2/en not_active Expired - Lifetime
- 2000-07-06 CN CNB008100535A patent/CN1223512C/en not_active Expired - Fee Related
- 2000-07-06 BR BRPI0012259-9A patent/BR0012259B1/en not_active IP Right Cessation
- 2000-07-07 MY MYPI20003138 patent/MY123489A/en unknown
- 2000-10-17 SA SA00210454A patent/SA00210454B1/en unknown
-
2002
- 2002-01-03 MA MA26466A patent/MA25874A1/en unknown
Also Published As
Publication number | Publication date |
---|---|
SA00210454B1 (en) | 2006-09-25 |
WO2001004048A1 (en) | 2001-01-18 |
EP1220815B1 (en) | 2004-04-28 |
MA25874A1 (en) | 2003-10-01 |
ATE265392T1 (en) | 2004-05-15 |
BR0012259A (en) | 2002-03-12 |
AU5833000A (en) | 2001-01-30 |
ES2220485T3 (en) | 2004-12-16 |
DE60010300T2 (en) | 2005-05-04 |
BR0012259B1 (en) | 2010-10-05 |
DE60010300D1 (en) | 2004-06-03 |
MY123489A (en) | 2006-05-31 |
CN1223512C (en) | 2005-10-19 |
EP1220815A1 (en) | 2002-07-10 |
PT1220815E (en) | 2004-09-30 |
TR200200003T2 (en) | 2002-06-21 |
FI116288B (en) | 2005-10-31 |
JO2185B1 (en) | 2003-12-23 |
AU768441B2 (en) | 2003-12-11 |
SI1220815T1 (en) | 2004-10-31 |
CN1360557A (en) | 2002-07-24 |
US6821311B1 (en) | 2004-11-23 |
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Legal Events
Date | Code | Title | Description |
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PC | Transfer of assignment of patent |
Owner name: KEMIRA GROWHOW OYJ Free format text: KEMIRA GROWHOW OYJ |
|
FG | Patent granted |
Ref document number: 116288 Country of ref document: FI |
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PC | Transfer of assignment of patent |
Owner name: SQM EUROPE N.V. Free format text: SQM EUROPE N.V. |
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MM | Patent lapsed |