FI121626B - Förfarande för framställning av olefina monomerer - Google Patents

Förfarande för framställning av olefina monomerer Download PDF

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Publication number
FI121626B
FI121626B FI20095079A FI20095079A FI121626B FI 121626 B FI121626 B FI 121626B FI 20095079 A FI20095079 A FI 20095079A FI 20095079 A FI20095079 A FI 20095079A FI 121626 B FI121626 B FI 121626B
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FI
Finland
Prior art keywords
oil
bed
cracking
process according
deoxygenation
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FI20095079A
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English (en)
Finnish (fi)
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FI20095079A0 (sv
FI20095079A (sv
Inventor
Ali Harlin
Olli Aaltonen
Tapani Penttinen
Jari Raesaenen
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Stora Enso Oyj
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Application filed by Stora Enso Oyj filed Critical Stora Enso Oyj
Priority to FI20095079A priority Critical patent/FI121626B/sv
Publication of FI20095079A0 publication Critical patent/FI20095079A0/sv
Priority to BRPI1007459-7A priority patent/BRPI1007459B1/pt
Priority to ES10735515.8T priority patent/ES2596887T3/es
Priority to CN201080005979.1A priority patent/CN102300836B/zh
Priority to CA2750078A priority patent/CA2750078C/en
Priority to RU2011135331/04A priority patent/RU2493141C2/ru
Priority to EP10735515.8A priority patent/EP2391595B1/en
Priority to US13/146,857 priority patent/US8957269B2/en
Priority to PCT/FI2010/050051 priority patent/WO2010086507A1/en
Publication of FI20095079A publication Critical patent/FI20095079A/sv
Publication of FI121626B publication Critical patent/FI121626B/sv
Application granted granted Critical
Priority to CL2011001711A priority patent/CL2011001711A1/es

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/207—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms from carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G51/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only
    • C10G51/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only plural serial stages only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/04—Ethylene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/06—Propene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/42—Catalytic treatment
    • C10G3/44—Catalytic treatment characterised by the catalyst used
    • C10G3/45—Catalytic treatment characterised by the catalyst used containing iron group metals or compounds thereof
    • C10G3/46—Catalytic treatment characterised by the catalyst used containing iron group metals or compounds thereof in combination with chromium, molybdenum, tungsten metals or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/54—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids characterised by the catalytic bed
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/34—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils by direct contact with inert preheated fluids, e.g. with molten metals or salts
    • C10G9/36—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils by direct contact with inert preheated fluids, e.g. with molten metals or salts with heated gases or vapours
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80—Additives
    • C10G2300/805—Water
    • C10G2300/807—Steam
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/20—C2-C4 olefins
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/40—Ethylene production

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Claims (15)

1. Förfarande för producering av olefina monomerer för framställning av polymerer, kännetecknat av de följande stegen: - bioolja, som innehäller talloljefettsyror, vars andel av biooljan är över 50 %, 5 samt talloljehartssyror, vars andel av biooljan är högst 25 %, samt vätegas mätäs in i en katalytbädd (7), - oljan deoksygeneras i bädden (7) katalytiskt med väte, - strömmen som lämnar bädden (7) nedkyls ooh delas in i en kolvätehaltig vätskefas (10) ooh en gasfas, ooh 10. pä den kolvätehaltiga vätskan (13) utförs ängkrackning (4) tili en produkt som innehäller polymeriserbara olefiner.
2. Förfarande enligt patentkrav 1, kännetecknat av att oljan är en frän rä-tallolja separerbar fraktion, som bestär av 75-98 % talloljefettsyror ooh 2-25 % talloljehartssyror. 15
3. Förfarande enligt patentkrav 1 eller 2, kännetecknat av att deoksy- generingskatalyten är metallisk, säsom en NiMo-katalyt eller en CoMo-katalyt.
4. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att katalytbädden är en fast bädd (7) utgjord av fast bäddmaterial. 20
5. Förfarande enligt patentkrav 4, kännetecknat av att deoksygeneringen (2) i den fasta bädden (7) följs av en katalytisk krackning (3) för att sanka molmassan, varvid deoksygenerings- ooh krackningsstegens katalyter sins- emellan är olika. o
° 6. Förfarande enligt patentkrav 5, kännetecknat av att krackningsstegets ^ 25 katalyt är sur, säsom sur zeolitkatalyt. o 00
7. Förfarande enligt patentkrav 5 eller 6, kännetecknat av att deoksy- £ generings- ooh krackningsstegens (2, 3) katalyter ligger efter varandra ät- 05 skilt frän varandra i den av bäddmaterial utgjorda fasta bädden (7). o ίο o
8. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat O ™ 30 av att deoksygenerings- och/eller krackningsstegets katalyt är ett mckel- haltigt silikat, säsom nickelsubstituerad montmorolit.
9. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att strömningarna i bädden (7) sker uppifrän nerät.
10. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att den frän vätskefasen (10) separerade vätehaltiga gasfasen (16) cirku- 5 leras tillbaka tili insatsgas för deoksygeneringssteget (2).
11. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att frän vätskefasen (10) separeras vatien (12) innan den kolvätehaltiga vätskan (13) mätäs tili ängkrackningen (4).
12. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat 10 av att den kolvätehaltiga vätskefasen (10, 13) innehäller kolväten pä diesel- oljans kokningsomräde.
13. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att biooljan som mätäs tili bädden (7) utgörs tili ätminstone 75 %, fördel-aktigt tili ätminstone 95 % av oljesyra ooh linolsyra. 15
14. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att biooljan som mätäs tili bädden (7) innehäller 2-5 % talloljehartssyror.
15. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat av att man med ängkrackningen (4) producerar eten och/eller propen. o δ CM O CO X cc Q_ en o LO 05 O O CM
FI20095079A 2009-01-29 2009-01-29 Förfarande för framställning av olefina monomerer FI121626B (sv)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FI20095079A FI121626B (sv) 2009-01-29 2009-01-29 Förfarande för framställning av olefina monomerer
PCT/FI2010/050051 WO2010086507A1 (en) 2009-01-29 2010-01-29 Method for producing olefinic monomers from bio oil
BRPI1007459-7A BRPI1007459B1 (pt) 2009-01-29 2010-01-29 Método para produção de monômeros olefínicos
ES10735515.8T ES2596887T3 (es) 2009-01-29 2010-01-29 Método para producir monómeros olefínicos a partir de bioaceite
CN201080005979.1A CN102300836B (zh) 2009-01-29 2010-01-29 用生物油制备烯烃单体的方法
CA2750078A CA2750078C (en) 2009-01-29 2010-01-29 Method for producing olefinic monomers from bio oil
RU2011135331/04A RU2493141C2 (ru) 2009-01-29 2010-01-29 Способ получения олефиновых мономеров из биологических масел
EP10735515.8A EP2391595B1 (en) 2009-01-29 2010-01-29 Method for producing olefinic monomers from bio oil
US13/146,857 US8957269B2 (en) 2009-01-29 2010-01-29 Method for producing olefinic monomers from bio oil
CL2011001711A CL2011001711A1 (es) 2009-01-29 2011-07-14 Método para producir monómeros olefínicos que comprende introducir bioaceite con un contenido de 95-98% en peso de ácidos grasos de aceite de resina y 2-5% en peso de ácidos resinosos, desoxigenar catalíticamente con hidrógeno, enfriar el flujo de salida, separar y someter el líquido a desintegración en vapor.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20095079A FI121626B (sv) 2009-01-29 2009-01-29 Förfarande för framställning av olefina monomerer
FI20095079 2009-01-29

Publications (3)

Publication Number Publication Date
FI20095079A0 FI20095079A0 (sv) 2009-01-29
FI20095079A FI20095079A (sv) 2010-07-30
FI121626B true FI121626B (sv) 2011-02-15

Family

ID=40329534

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20095079A FI121626B (sv) 2009-01-29 2009-01-29 Förfarande för framställning av olefina monomerer

Country Status (10)

Country Link
US (1) US8957269B2 (sv)
EP (1) EP2391595B1 (sv)
CN (1) CN102300836B (sv)
BR (1) BRPI1007459B1 (sv)
CA (1) CA2750078C (sv)
CL (1) CL2011001711A1 (sv)
ES (1) ES2596887T3 (sv)
FI (1) FI121626B (sv)
RU (1) RU2493141C2 (sv)
WO (1) WO2010086507A1 (sv)

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FI20095079A0 (sv) 2009-01-29
RU2493141C2 (ru) 2013-09-20
RU2011135331A (ru) 2013-03-10
ES2596887T3 (es) 2017-01-12
EP2391595A1 (en) 2011-12-07
EP2391595A4 (en) 2015-03-04
EP2391595B1 (en) 2016-07-20
CL2011001711A1 (es) 2012-03-16
CN102300836B (zh) 2014-07-02
CA2750078A1 (en) 2010-08-05
FI20095079A (sv) 2010-07-30
US8957269B2 (en) 2015-02-17
CA2750078C (en) 2017-01-10
WO2010086507A1 (en) 2010-08-05
BRPI1007459B1 (pt) 2018-06-12
BRPI1007459A2 (pt) 2016-08-09
US20120053379A1 (en) 2012-03-01

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