ES8406980A1 - Perfeccionamientos introducidos en la purificacion de acido fosforico de procedimiento en humedo. - Google Patents

Perfeccionamientos introducidos en la purificacion de acido fosforico de procedimiento en humedo.

Info

Publication number
ES8406980A1
ES8406980A1 ES522621A ES522621A ES8406980A1 ES 8406980 A1 ES8406980 A1 ES 8406980A1 ES 522621 A ES522621 A ES 522621A ES 522621 A ES522621 A ES 522621A ES 8406980 A1 ES8406980 A1 ES 8406980A1
Authority
ES
Spain
Prior art keywords
phosphoric acid
purifying phosphoric
organic
purifying
alcohol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES522621A
Other languages
English (en)
Other versions
ES522621A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FMC Corp
Original Assignee
FMC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FMC Corp filed Critical FMC Corp
Publication of ES522621A0 publication Critical patent/ES522621A0/es
Publication of ES8406980A1 publication Critical patent/ES8406980A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/46—Preparation involving solvent-solvent extraction
    • C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/46—Preparation involving solvent-solvent extraction
    • C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
    • C01B25/465—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound the extracting agent being an ester or a mixture of esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

PROCEDIMIENTO MEJORADO PARA PURIFICAR ACIDO FOSFORICO DE PROCEDIMIENTO HUMEDO.COMPRENDE LAS ETAPAS: A) EXTRAER EL ACIDO FOSFORICO DE LA FASE DISOLVENTE CON UN LIQUIDO DE EXTRACCION ORGANICO, INSOLUBLE EN AGUA PARA RECUPERAR UN EXTRACTO DE MAS BAJO CONTENIDO EN IMPUREZAS QUE EL ACIDO FOSFORICO HUMEDO; B) SEPARAR EL EXTRACTO A PARTIR DE UN REFINADO ACUOSO; C) PONER EN CONTACTO EL EXTRACTO CON AGUA PARA SEPARAR UN CONTENIDO VALIOSO DE P2O5 DEL MISMO Y FORMAR ACIDO FOSFORICO; D) SEPARAR UNA SOLUCION ACUOSA DE ACIDO FOSFORICO DEL REMANENTE DEL AGENTE DEEXTRACCION ORGANICO; Y E) CALENTAR LA SOLUCION ACUOSA DE ACIDO FOSFORICO A UNA TEMPERATURA ENTRE 100J Y 155J, PARA EVAPORAR EL CONTENIDO DE FLUOR DE LA SOLUCION Y RECUPERAR LA SOLUCION DE ACIDO FOSFORICO DE MAYOR PUREZA QUE LA DEL ACIDO HUMEDO. EL DISOLVENTE DE EXTRACCION CONSISTE EN UN FOSFATO ORGANICO FORMADO POR FOSFATO DE ARILO, FOSFATO DE ALQUILO O FOSDATO DE ALQUILARILO DILUIDO CON UN DISOLVENTE ORGANICO COMO DIISOBUTIL-CETONA-BENZOFENONA YOTROS.
ES522621A 1982-05-24 1983-05-23 Perfeccionamientos introducidos en la purificacion de acido fosforico de procedimiento en humedo. Expired ES8406980A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/381,279 US4394361A (en) 1982-05-24 1982-05-24 Method of purifying phosphoric acid

Publications (2)

Publication Number Publication Date
ES522621A0 ES522621A0 (es) 1984-08-16
ES8406980A1 true ES8406980A1 (es) 1984-08-16

Family

ID=23504419

Family Applications (1)

Application Number Title Priority Date Filing Date
ES522621A Expired ES8406980A1 (es) 1982-05-24 1983-05-23 Perfeccionamientos introducidos en la purificacion de acido fosforico de procedimiento en humedo.

Country Status (2)

Country Link
US (1) US4394361A (es)
ES (1) ES8406980A1 (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4543239A (en) * 1984-08-21 1985-09-24 International Minerals & Chemical Corp. Phosphoric acid extraction process
US4751066A (en) * 1986-05-08 1988-06-14 Fmc Corporation Process for preparing alkali metal phosphate
DE3622597A1 (de) * 1986-07-04 1988-01-07 Budenheim Rud A Oetker Chemie Verfahren zur faellung und abtrennung von cadmiumsulfid aus den raffinaten der phosphorsaeurereinigung
US4780295A (en) * 1987-07-06 1988-10-25 Fmc Corporation Process for purifying phosphoric acid
CN1094111C (zh) * 1999-12-30 2002-11-13 清华大学 用萃取－反萃交替法生产磷酸盐的方法
CN110116997A (zh) * 2019-06-25 2019-08-13 山东鲁北企业集团总公司 一种湿法磷酸净化除铁的方法
EP4015452A1 (en) 2020-12-21 2022-06-22 Técnicas Reunidas, S.A. Process for producing technical grade phosphoric acid from sewage sludge ash
CN114835094B (zh) * 2022-03-17 2024-04-26 中国科学院过程工程研究所 一种磷矿酸解原位萃磷制备湿法磷酸和硫酸钙的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1929441A (en) * 1930-08-26 1933-10-10 American Agricultural Chem Co Process for obtaining orthophosphoric acid and/or conversion product thereof
US1838431A (en) * 1930-08-26 1931-12-29 American Agricultural Chem Co Process for obtaining orthophosphoric acid and/or conversion products thereof
US1929442A (en) * 1930-08-26 1933-10-10 American Agricultural Chem Co Process for obtaining orthophosphoric acid and/or conversion products thereof
US1857470A (en) * 1930-08-26 1932-05-10 American Agricultural Chem Co Process for obtaining orthophosphoric acid and/or conversion products thereof
US1929443A (en) * 1930-08-26 1933-10-10 American Agricultural Chem Co Process for obtaining alkali metal phosphates
US2902454A (en) * 1952-06-25 1959-09-01 Robert L Moore Solvent composition for recovery of metal values from aqueous solutions by solvent extraction
US2859092A (en) * 1953-02-05 1958-11-04 Richard H Bailes Solvent extraction process for the recovery of metals from phosphoric acid
US2860031A (en) * 1956-06-29 1958-11-11 Robert R Grinstead Process for utilizing organic orthophosphate extractants
US3338674A (en) * 1963-05-09 1967-08-29 Avraham M Baniel Process for preparation of substantially pure phosphoric acid
US3410656A (en) * 1966-06-01 1968-11-12 Fmc Corp Phosphoric acid purification
US3433592A (en) * 1966-04-07 1969-03-18 Avraham Baniel Method of purifying phosphoric acid
US3708508A (en) * 1971-04-09 1973-01-02 Atomic Energy Commission Method for the purification and recovery of tributyl phosphate used in reprocessing nuclear fuel
LU66958A1 (es) * 1973-02-02 1974-09-25
US4196180A (en) * 1973-07-04 1980-04-01 Hoechst Aktiengesellschaft Purification of phosphoric acid by means of organic solvents
US4207302A (en) * 1974-07-18 1980-06-10 Freeport Minerals Company Method of treating phosphoric acid to prevent crud formation during solvent extraction
US4256716A (en) * 1979-03-01 1981-03-17 Occidental Research Corporation Process for treating loaded extractant from purification of phosphoric acid by extraction
US4311681A (en) * 1980-05-19 1982-01-19 Fmc Corporation Method of regenerating phosphoric acid extraction solvent

Also Published As

Publication number Publication date
US4394361A (en) 1983-07-19
ES522621A0 (es) 1984-08-16

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20041102