ES8304121A1 - Procedimiento para la obtencion del diclohidrato de 8,9-dimetil-4(3-(4-metilpiperazin-1-il)propionamido)-1,2,3,4,4a,9b-hexahidrodibenzofuran-3-ona. - Google Patents
Procedimiento para la obtencion del diclohidrato de 8,9-dimetil-4(3-(4-metilpiperazin-1-il)propionamido)-1,2,3,4,4a,9b-hexahidrodibenzofuran-3-ona.Info
- Publication number
- ES8304121A1 ES8304121A1 ES511297A ES511297A ES8304121A1 ES 8304121 A1 ES8304121 A1 ES 8304121A1 ES 511297 A ES511297 A ES 511297A ES 511297 A ES511297 A ES 511297A ES 8304121 A1 ES8304121 A1 ES 8304121A1
- Authority
- ES
- Spain
- Prior art keywords
- ona
- dimethyl
- hexahidrodibenzofuran
- methylpiperazin
- translation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
_(PROCEDIMIENTO PARA LA OBTENCION DEL DICLORHIDRATO DE 8,9B-DIMETIL-4 3-(4-METILPIPERAZIN-1-IL)PROPIONAMIDO -1,2,3,4,4A, 9B,-HEXAHIDRODIBENZOFURAN-3-ONA . CONSISTE EN HACER REACCIONAR LA 4-(3-CLORO-PROPIONAMIDO)-8,9B-DIMETIL-1,2,3,4,4A,9BHEXAHIDRODIBENZOFURAN-3-ONA, EN CONDICIONES ADECUADAS DE N-ALQUILACION CON N-METILPIPERAZINA. EL PRODUCTO RESULTANTE, SE PURIFICA POR METODOS CONVENCIONALES. LA REACCION PUEDE EFECTUARSE EN UN DISOLVENTE AROMATICO COMO BENCENO-TOLUENO, O UNA MEZCLA DE ESTOS Y CLOROFORMO; ADEMAS TIENE LUGAR EN PRESENCIA DE UNA BASE CAPAZ DE NEUTRALIZAR EL ACIDO CLORHIDRICO QUE SE DESPRENDE; LAS BASES EMPLEADAS SON NA CO , K CO Y OTRAS. LA TEMPERATURA OSCILA ENTRE LA DE REFLUJO DEL DISOLVENTE Y 35 C, SIENDO PREFERIBLE DE 50 A 60 C. AGENTE ANTITUSIVO.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES511297A ES511297A0 (es) | 1982-04-08 | 1982-04-08 | Procedimiento para la obtencion del diclohidrato de 8,9-dimetil-4(3-(4-metilpiperazin-1-il)propionamido)-1,2,3,4,4a,9b-hexahidrodibenzofuran-3-ona. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES511297A ES511297A0 (es) | 1982-04-08 | 1982-04-08 | Procedimiento para la obtencion del diclohidrato de 8,9-dimetil-4(3-(4-metilpiperazin-1-il)propionamido)-1,2,3,4,4a,9b-hexahidrodibenzofuran-3-ona. |
Publications (2)
Publication Number | Publication Date |
---|---|
ES8304121A1 true ES8304121A1 (es) | 1983-02-16 |
ES511297A0 ES511297A0 (es) | 1983-02-16 |
Family
ID=8483981
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES511297A Granted ES511297A0 (es) | 1982-04-08 | 1982-04-08 | Procedimiento para la obtencion del diclohidrato de 8,9-dimetil-4(3-(4-metilpiperazin-1-il)propionamido)-1,2,3,4,4a,9b-hexahidrodibenzofuran-3-ona. |
Country Status (1)
Country | Link |
---|---|
ES (1) | ES511297A0 (es) |
-
1982
- 1982-04-08 ES ES511297A patent/ES511297A0/es active Granted
Also Published As
Publication number | Publication date |
---|---|
ES511297A0 (es) | 1983-02-16 |
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