ES464485A1 - Polymerization and rcovery of 2-pyrrolidone - Google Patents

Polymerization and rcovery of 2-pyrrolidone

Info

Publication number
ES464485A1
ES464485A1 ES464485A ES464485A ES464485A1 ES 464485 A1 ES464485 A1 ES 464485A1 ES 464485 A ES464485 A ES 464485A ES 464485 A ES464485 A ES 464485A ES 464485 A1 ES464485 A1 ES 464485A1
Authority
ES
Spain
Prior art keywords
pyrrolidone
polymerization
rcovery
poly
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES464485A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chevron USA Inc
Original Assignee
Chevron Research and Technology Co
Chevron Research Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US05/745,501 external-priority patent/US4050994A/en
Priority claimed from US05/792,421 external-priority patent/US4139696A/en
Application filed by Chevron Research and Technology Co, Chevron Research Co filed Critical Chevron Research and Technology Co
Publication of ES464485A1 publication Critical patent/ES464485A1/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D207/00Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/22Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D207/24Oxygen or sulfur atoms
    • C07D207/262-Pyrrolidones
    • C07D207/2632-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
    • C07D207/2672-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16Separation or purification
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14Lactams
    • C08G69/24Pyrrolidones or piperidones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyamides (AREA)
  • Pyrrole Compounds (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)

Abstract

Process for the polymerization of pyrrolidine, characterized in that it comprises the steps of polymerizing a mixture containing alkaline catalyst, pyrrolidone and solvent, to form a reaction product mixture comprising poly-2-pyrrolidone in particulate form, alkaline catalyst and solvent; and before the poly-2-pyrrolidone is agglomerated appreciably, treating said reaction product mixture with an acid to reduce the ph of the resulting mixture to a value of about 5 to about 8. (Machine-translation by Google Translate, not legally binding)
ES464485A 1976-11-26 1977-11-25 Polymerization and rcovery of 2-pyrrolidone Expired ES464485A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US05/745,501 US4050994A (en) 1976-11-26 1976-11-26 Recovery of 2-pyrrolidone from dilute alkaline solutions
US05/792,421 US4139696A (en) 1977-04-29 1977-04-29 Continuous polymerization of 2-pyrrolidone

Publications (1)

Publication Number Publication Date
ES464485A1 true ES464485A1 (en) 1979-01-01

Family

ID=27114468

Family Applications (1)

Application Number Title Priority Date Filing Date
ES464485A Expired ES464485A1 (en) 1976-11-26 1977-11-25 Polymerization and rcovery of 2-pyrrolidone

Country Status (8)

Country Link
JP (1) JPS5367798A (en)
DE (1) DE2751535A1 (en)
ES (1) ES464485A1 (en)
FR (2) FR2382471A1 (en)
GB (1) GB1592178A (en)
IT (1) IT1087943B (en)
MX (1) MX4979E (en)
NL (1) NL7713024A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1566154A1 (en) 2004-02-20 2005-08-24 Argomedical AG Prosthesis for surface replacement in the area of the ball of ball bearings
KR101568908B1 (en) * 2013-12-02 2015-11-12 지에스칼텍스 주식회사 Apparatus and method for manufacturing particulate polyamide resin

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3681293A (en) * 1970-09-03 1972-08-01 Radiation Res Corp Continuous polymerization of 2-pyrrolidone with carbon dioxide as activator

Also Published As

Publication number Publication date
GB1592178A (en) 1981-07-01
DE2751535A1 (en) 1978-06-01
FR2382471A1 (en) 1978-09-29
FR2382442A1 (en) 1978-09-29
IT1087943B (en) 1985-06-04
NL7713024A (en) 1978-05-30
FR2382471B1 (en) 1981-01-02
FR2382442B1 (en) 1981-01-16
JPS5367798A (en) 1978-06-16
MX4979E (en) 1983-01-28
JPS5731742B2 (en) 1982-07-06

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