ES2174246T3 - Metodo para monitorizar y controlar procesos con sensores de microbalanza de cristal de cuarzo en linea. - Google Patents
Metodo para monitorizar y controlar procesos con sensores de microbalanza de cristal de cuarzo en linea.Info
- Publication number
- ES2174246T3 ES2174246T3 ES97917601T ES97917601T ES2174246T3 ES 2174246 T3 ES2174246 T3 ES 2174246T3 ES 97917601 T ES97917601 T ES 97917601T ES 97917601 T ES97917601 T ES 97917601T ES 2174246 T3 ES2174246 T3 ES 2174246T3
- Authority
- ES
- Spain
- Prior art keywords
- monitoring
- quartz crystal
- mass
- crystal microbalance
- controlling processes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title 2
- 238000012544 monitoring process Methods 0.000 title 1
- 238000003380 quartz crystal microbalance Methods 0.000 title 1
- 239000012530 fluid Substances 0.000 abstract 2
- 239000013078 crystal Substances 0.000 abstract 1
- 230000008021 deposition Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/022—Fluid sensors based on microsensors, e.g. quartz crystal-microbalance [QCM], surface acoustic wave [SAW] devices, tuning forks, cantilevers, flexural plate wave [FPW] devices
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/10—Starch-containing substances, e.g. dough
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N17/00—Investigating resistance of materials to the weather, to corrosion, or to light
- G01N17/008—Monitoring fouling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/036—Analysing fluids by measuring frequency or resonance of acoustic waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
- G01N2291/025—Change of phase or condition
- G01N2291/0256—Adsorption, desorption, surface mass change, e.g. on biosensors
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
- G01N2291/028—Material parameters
- G01N2291/02818—Density, viscosity
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/04—Wave modes and trajectories
- G01N2291/042—Wave modes
- G01N2291/0422—Shear waves, transverse waves, horizontally polarised waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/04—Wave modes and trajectories
- G01N2291/042—Wave modes
- G01N2291/0426—Bulk waves, e.g. quartz crystal microbalance, torsional waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/002—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Acoustics & Sound (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Ecology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Environmental Sciences (AREA)
- Medicinal Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Biodiversity & Conservation Biology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Length Measuring Devices With Unspecified Measuring Means (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Control Of Non-Electrical Variables (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Piezo-Electric Or Mechanical Vibrators, Or Delay Or Filter Circuits (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
SE PUEDEN UTILIZAR RESONADORES DE MODO DE CIZALLAMIENTO EN ESPESOR, QUE MIDEN SIMULTANEAMENTE LA DEPOSICION DE MASA Y LAS PROPIEDADES DE FLUIDOS, PARA MONITORIZAR EL PROCESAMIENTO DEL PETROLEO Y PRODUCTOS PETROQUIMICOS Y LOS SISTEMAS DE TRATAMIENTO DE AGUAS. SE PUEDEN AÑADIR SUSTANCIAS QUIMICAS ESPECIALES, DE FORMA PRECISA E INSTANTANEA, EN CONDICIONES DE CONTROL DETECTADAS MEDIANTE LOS RESONADORES DE MODO DE CIZALLAMIENTO EN ESPESOR. DICHOS RESONADORES SON CRISTALES PIEZOELECTRICOS UTILIZADOS CONJUNTAMENTE CON CIRCUITERIA DE OSCILADOR, QUE PUEDEN DETERMINAR LA MASA, ASI COMO LA VISCOSIDAD Y/O DENSIDAD DE UN FLUIDO EN CONTACTO CON LA SUPERFICIE PIEZOELECTRICA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/621,402 US5734098A (en) | 1996-03-25 | 1996-03-25 | Method to monitor and control chemical treatment of petroleum, petrochemical and processes with on-line quartz crystal microbalance sensors |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2174246T3 true ES2174246T3 (es) | 2002-11-01 |
Family
ID=24490021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES97917601T Expired - Lifetime ES2174246T3 (es) | 1996-03-25 | 1997-03-24 | Metodo para monitorizar y controlar procesos con sensores de microbalanza de cristal de cuarzo en linea. |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US5734098A (es) |
| EP (1) | EP0829010B1 (es) |
| JP (1) | JP3876293B2 (es) |
| KR (1) | KR100467948B1 (es) |
| CN (1) | CN1131431C (es) |
| AR (1) | AR006392A1 (es) |
| AT (1) | ATE218707T1 (es) |
| AU (1) | AU718367B2 (es) |
| BR (1) | BR9702225A (es) |
| CA (1) | CA2222046C (es) |
| DE (1) | DE69713009T2 (es) |
| ES (1) | ES2174246T3 (es) |
| ID (1) | ID16437A (es) |
| IN (1) | IN191903B (es) |
| MX (1) | MX9709033A (es) |
| MY (1) | MY119386A (es) |
| NO (1) | NO321041B1 (es) |
| NZ (1) | NZ329132A (es) |
| RU (1) | RU2241986C2 (es) |
| TW (1) | TW363079B (es) |
| WO (1) | WO1997036178A1 (es) |
Families Citing this family (107)
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| DE69735411T2 (de) * | 1996-10-09 | 2006-09-07 | Symyx Technologies, Inc., Santa Clara | Infrarot-spektroskopie und abbildung von bibliotheken |
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| US6141625A (en) * | 1997-06-09 | 2000-10-31 | Dickey-John Corporation | Viscometer module with crystal resonator-type sensor |
| US6494079B1 (en) * | 2001-03-07 | 2002-12-17 | Symyx Technologies, Inc. | Method and apparatus for characterizing materials by using a mechanical resonator |
| US6393895B1 (en) | 1997-10-08 | 2002-05-28 | Symyx Technologies, Inc. | Method and apparatus for characterizing materials by using a mechanical resonator |
| MY123949A (en) * | 1997-11-12 | 2006-06-30 | Fisher Controls Int | Fugitive emission sensing system |
| AU737392B2 (en) | 1997-12-02 | 2001-08-16 | Allan L Smith | Mass and heat flow measurement sensor |
| US6113774A (en) * | 1998-05-22 | 2000-09-05 | Phillips Petroleum Company | Antifoulant control process |
| US5969235A (en) * | 1998-07-02 | 1999-10-19 | Nalco Chemical Company | System and method for measuring scale deposition including a tuning fork for use in the system and the method |
| ES2153740B1 (es) * | 1998-07-08 | 2001-10-01 | Univ Valencia Politecnica | Sistema para compensar los efectos de rozamiento viscoso en la medida de la frecuencia de resonancia de un cristal piezometrico en un fluido |
| US6548026B1 (en) | 1998-08-13 | 2003-04-15 | Symyx Technologies, Inc. | Parallel reactor with internal sensing and method of using same |
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| US6250140B1 (en) | 1999-06-22 | 2001-06-26 | Nalco Chemical Company | Method for measuring the rate of a fouling reaction induced by heat transfer using a piezoelectric microbalance |
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| US7317989B2 (en) * | 2001-05-15 | 2008-01-08 | Baker Hughes Incorporated | Method and apparatus for chemometric estimations of fluid density, viscosity, dielectric constant, and resistivity from mechanical resonator data |
| EP1397661B1 (en) * | 2001-05-15 | 2008-09-10 | Baker Hughes Incorporated | Method and apparatus for downhole fluid characterization using flxural mechanical resonators |
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| BR112020005034B1 (pt) | 2017-09-19 | 2023-10-10 | Ecolab Usa Inc | Método para controlar tratamento de água de resfriamento, e,sistema |
| AU2018364983B2 (en) | 2017-11-10 | 2024-08-15 | Ecolab Usa Inc. | Cooling water monitoring and control system |
| US11137373B2 (en) * | 2018-05-24 | 2021-10-05 | Hf Scientific, Inc. | QCM measurement of scale formation |
| CN109138982B (zh) * | 2018-11-16 | 2023-09-26 | 美钻深海能源科技研发(上海)有限公司 | 水下装备生物腐蚀自动安全关井系统 |
| TW202043447A (zh) * | 2019-04-12 | 2020-12-01 | 美商Bl科技公司 | 減輕烴廠結垢的方法 |
| RU191599U1 (ru) * | 2019-06-06 | 2019-08-13 | Общество с ограниченной ответственностью «Газпромнефть - Битумные материалы» (ООО «Газпромнефть-БМ») | Контейнер-цистерна для перевозки вязких нефтепродуктов |
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| US4409553A (en) * | 1980-10-06 | 1983-10-11 | Texaco Inc. | Paraffin monitor |
| US4526480A (en) * | 1983-06-21 | 1985-07-02 | Quartztronics, Inc. | Fluid density temperature measurement apparatus and method |
| SE8401581L (sv) * | 1984-03-21 | 1985-09-22 | Foersvarets Forskningsanstalt | Metod och anordning for metning av vetskors korrosivitet eller reaktivitet mot fremst metaller |
| US4997574A (en) * | 1989-09-01 | 1991-03-05 | Lehigh University | Staged boundary layer treatment method and system for biofouling control |
| US5208162A (en) * | 1990-05-08 | 1993-05-04 | Purafil, Inc. | Method and apparatus for monitoring corrosion |
| DE4034883C2 (de) * | 1990-11-02 | 1994-05-05 | Fibronix Sensoren Gmbh | Vorrichtung zur Messung der Dichte einer Flüssigkeit |
| RU2045030C1 (ru) * | 1991-05-13 | 1995-09-27 | Беляков Виталий Леонидович | Устройство для измерения плотности жидкости |
| US5201215A (en) * | 1991-10-17 | 1993-04-13 | The United States Of America As Represented By The United States Department Of Energy | Method for simultaneous measurement of mass loading and fluid property changes using a quartz crystal microbalance |
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| US5484626A (en) * | 1992-04-06 | 1996-01-16 | Shipley Company L.L.C. | Methods and apparatus for maintaining electroless plating solutions |
| DE9317351U1 (de) * | 1992-12-11 | 1994-01-20 | Lang Apparatebau Gmbh, 83313 Siegsdorf | Vorrichtung zum Analysieren von Fluiden |
| US5360549A (en) * | 1993-04-27 | 1994-11-01 | Nalco Chemical Company | Feed back control deposit inhibitor dosage optimization system |
| US5487981A (en) * | 1993-07-30 | 1996-01-30 | The United States Of America As Represented By The Secretary Of The Navy | Apparatus for and method of detecting/identifying microbial contamination in ultra-pure water systems |
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-
1996
- 1996-03-25 US US08/621,402 patent/US5734098A/en not_active Expired - Lifetime
-
1997
- 1997-01-01 IN IN525CA1997 patent/IN191903B/en unknown
- 1997-03-24 NZ NZ329132A patent/NZ329132A/xx not_active IP Right Cessation
- 1997-03-24 DE DE69713009T patent/DE69713009T2/de not_active Expired - Lifetime
- 1997-03-24 AT AT97917601T patent/ATE218707T1/de not_active IP Right Cessation
- 1997-03-24 JP JP53453497A patent/JP3876293B2/ja not_active Expired - Lifetime
- 1997-03-24 CN CN97190339A patent/CN1131431C/zh not_active Expired - Fee Related
- 1997-03-24 AU AU25877/97A patent/AU718367B2/en not_active Ceased
- 1997-03-24 RU RU97121350/28A patent/RU2241986C2/ru active
- 1997-03-24 CA CA002222046A patent/CA2222046C/en not_active Expired - Fee Related
- 1997-03-24 EP EP97917601A patent/EP0829010B1/en not_active Expired - Lifetime
- 1997-03-24 KR KR1019970708508A patent/KR100467948B1/ko not_active Expired - Lifetime
- 1997-03-24 BR BR9702225A patent/BR9702225A/pt not_active IP Right Cessation
- 1997-03-24 WO PCT/US1997/004726 patent/WO1997036178A1/en not_active Ceased
- 1997-03-24 MX MX9709033A patent/MX9709033A/es unknown
- 1997-03-24 ES ES97917601T patent/ES2174246T3/es not_active Expired - Lifetime
- 1997-03-25 AR ARP970101202A patent/AR006392A1/es active IP Right Grant
- 1997-03-25 MY MYPI97001249A patent/MY119386A/en unknown
- 1997-03-25 ID IDP970973A patent/ID16437A/id unknown
- 1997-03-25 TW TW086103779A patent/TW363079B/zh not_active IP Right Cessation
- 1997-11-24 NO NO19975376A patent/NO321041B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0829010B1 (en) | 2002-06-05 |
| NO321041B1 (no) | 2006-03-06 |
| RU2241986C2 (ru) | 2004-12-10 |
| EP0829010A1 (en) | 1998-03-18 |
| CA2222046A1 (en) | 1997-10-02 |
| JPH11508054A (ja) | 1999-07-13 |
| CN1131431C (zh) | 2003-12-17 |
| MX9709033A (es) | 1998-03-31 |
| AU718367B2 (en) | 2000-04-13 |
| DE69713009T2 (de) | 2003-02-06 |
| NO975376L (no) | 1998-01-23 |
| KR100467948B1 (ko) | 2005-06-22 |
| NZ329132A (en) | 2000-01-28 |
| CA2222046C (en) | 2005-08-16 |
| CN1188546A (zh) | 1998-07-22 |
| AU2587797A (en) | 1997-10-17 |
| ATE218707T1 (de) | 2002-06-15 |
| AR006392A1 (es) | 1999-08-25 |
| WO1997036178A1 (en) | 1997-10-02 |
| IN191903B (es) | 2004-01-17 |
| TW363079B (en) | 1999-07-01 |
| NO975376D0 (no) | 1997-11-24 |
| ID16437A (id) | 1997-10-02 |
| MY119386A (en) | 2005-05-31 |
| US5734098A (en) | 1998-03-31 |
| KR19990022029A (ko) | 1999-03-25 |
| DE69713009D1 (de) | 2002-07-11 |
| JP3876293B2 (ja) | 2007-01-31 |
| BR9702225A (pt) | 1999-02-23 |
| HK1017922A1 (en) | 1999-12-03 |
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