ES2142839T3 - Proceso para determinar la concentracion y distribucion de negro de carbon en compuestos de caucho y en otros materiales que contienen negro de carbon y dispositivo para realizar dicho proceso. - Google Patents

Proceso para determinar la concentracion y distribucion de negro de carbon en compuestos de caucho y en otros materiales que contienen negro de carbon y dispositivo para realizar dicho proceso.

Info

Publication number
ES2142839T3
ES2142839T3 ES93113036T ES93113036T ES2142839T3 ES 2142839 T3 ES2142839 T3 ES 2142839T3 ES 93113036 T ES93113036 T ES 93113036T ES 93113036 T ES93113036 T ES 93113036T ES 2142839 T3 ES2142839 T3 ES 2142839T3
Authority
ES
Spain
Prior art keywords
carbon black
delay times
concentration
distribution
rubber compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES93113036T
Other languages
English (en)
Inventor
Christoph Dr Dipl-Phy Carlhoff
Martin Dr Rer Nat Jogwich
Claus-Jurgen Dr Dipl- Lorenzen
Marco Nahmias
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pirelli and C SpA
Pirelli Tyre SpA
Original Assignee
Pirelli Pneumatici SpA
Pirelli SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pirelli Pneumatici SpA, Pirelli SpA filed Critical Pirelli Pneumatici SpA
Application granted granted Critical
Publication of ES2142839T3 publication Critical patent/ES2142839T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/71Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited
    • G01N21/718Laser microanalysis, i.e. with formation of sample plasma
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44Resins; Plastics; Rubber; Leather
    • G01N33/445Rubber

Landscapes

  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Optics & Photonics (AREA)
  • Plasma & Fusion (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)

Abstract

SE DESCRIBE UN METODO Y APARATO PARA DETERMINAR NEGRO DE CARBONO EN COMPUESTOS DE CAUCHO (EJ. PARA RUEDAS) BASADO EN ESPECTROSCOPIA DE DESCARGA LASER DE RESOLUCION TEMPORAL (TREUBS). SE REALIZA UNA EXPLORACION DE TRAMA POR RAYO LASER (4A) A TRAVES DE UNA SUPERFICIE DE MUESTRA (1A), Y SE RECOGE UNA EMISION ATOMICA O MOLECULAR A PARTIR DEL PLASMA (4C) EXCITADO POR LASER DESDE UNOS PUNTOS DE MEDIDA (4B) DISPERSADOS ESPECTRALMENTE MEDIANTE RETICULADO (11), Y DETECTADO UTILIZANDO UN SISTEMA FOTODIODO (12). PARA DETERMINAR LA DISTRIBUCION DEL NEGRO DE CARBONO, SE MIDEN LAS RELACIONES DE INTENSIDAD DE LINEA ESPECTRAL RELACIONADAS CON EL CARBON QUE ACTUA COMO MODELO INTERNO PARA ELEMENTOS PRESENTES EN LA MUESTRA EN DOS DIFERENTES TIEMPOS DE RETRASO TRAS EL IMPULSO DE EXCITACION LASER. EN CORTOS TIEMPOS DE RETRASO MENORES DE 0.5 NS, LA EMISION DE CARBONO SE DEBE SOBRE TODO AL NEGRO DE CARBONO; EN LARGOS TIEMPOS DE RETRASO, LA SEÑAL REPRESENTA EL TOTAL DE CARBONO PRESENTE EN LA MATRIZ. LA COMPARACIONDE LAS RELACIONES DE INTENSIDAD CON LAS CURVAS DE CALIBRACION PRODUCE ENTONCES LA CONCENTRACION DE NEGRO DE CARBON EN UN PUNTO MEDIDO.
ES93113036T 1993-08-13 1993-08-13 Proceso para determinar la concentracion y distribucion de negro de carbon en compuestos de caucho y en otros materiales que contienen negro de carbon y dispositivo para realizar dicho proceso. Expired - Lifetime ES2142839T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP93113036A EP0652430B1 (en) 1993-08-13 1993-08-13 Process for determining carbon black concentration and distribution in rubber compounds and other carbon black containing materials and device to carry out the process

Publications (1)

Publication Number Publication Date
ES2142839T3 true ES2142839T3 (es) 2000-05-01

Family

ID=8213179

Family Applications (1)

Application Number Title Priority Date Filing Date
ES93113036T Expired - Lifetime ES2142839T3 (es) 1993-08-13 1993-08-13 Proceso para determinar la concentracion y distribucion de negro de carbon en compuestos de caucho y en otros materiales que contienen negro de carbon y dispositivo para realizar dicho proceso.

Country Status (5)

Country Link
US (2) US5537207A (es)
EP (1) EP0652430B1 (es)
JP (1) JP3662953B2 (es)
DE (1) DE69327463T2 (es)
ES (1) ES2142839T3 (es)

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US6545240B2 (en) 1996-02-16 2003-04-08 Huron Valley Steel Corporation Metal scrap sorting system
US6034768A (en) * 1997-09-26 2000-03-07 Physical Sciences Inc. Induced breakdown spectroscopy detector system with controllable delay time
US6002478A (en) * 1998-03-20 1999-12-14 Transgenomic Inc. System and method of determining trace elements in high viscosity liquids, and powders, utilizing laser-ablation
US6008897A (en) * 1999-01-19 1999-12-28 National Research Council Of Canada Method and apparatus for materials analysis by enhanced laser induced plasma spectroscopy
FR2800466B1 (fr) * 1999-11-03 2001-11-23 Commissariat Energie Atomique Dispositif d'analyse element par spectrometrie d'emission optique sur plasma produit par laser
US6741345B2 (en) * 2001-02-08 2004-05-25 National Research Council Of Canada Method and apparatus for in-process liquid analysis by laser induced plasma spectroscopy
DE10229498A1 (de) * 2002-07-01 2004-01-22 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren und Vorrichtung zur Durchführung der Plasmaemissionsspektrometrie
DE60233799D1 (de) * 2002-11-01 2009-11-05 Huron Valley Steel Corp Abtastvorrichtung für Verwendung in einer Metallschrottsortiervorrichtung
DE10304337A1 (de) * 2003-02-03 2004-08-19 Luk Laser-Und Umweltmesstechnik Kiel Gmbh Verfahren und Sensorkopf zur berührungslosen Klassifizierung von Materialien
DE102005027260B4 (de) * 2005-06-13 2007-03-29 Daimlerchrysler Ag Verfahren und Vorrichtung zur Qualitätsbestimmung einer Schweißnaht oder einer thermischen Spritzschicht und Verwendung
JP2007010371A (ja) * 2005-06-28 2007-01-18 Kenji Yasuda 有害物検出システム、有害木材の検出方法及び廃棄木材処理システム
DE102007049133A1 (de) * 2007-02-13 2008-08-21 Vistec Semiconductor Systems Gmbh Vorrichtung zur Bestimmung der Position mindestens einer Struktur auf einem Objekt, Verwendung einer Beleuchtungseinrichtung für die Vorrichtung und Verwendung von Schutzgas für die Vorrichtung
US8582113B2 (en) 2007-02-13 2013-11-12 Kla-Tencor Mie Gmbh Device for determining the position of at least one structure on an object, use of an illumination apparatus with the device and use of protective gas with the device
US20100330805A1 (en) * 2007-11-02 2010-12-30 Kenny Linh Doan Methods for forming high aspect ratio features on a substrate
JP5220481B2 (ja) * 2008-05-30 2013-06-26 独立行政法人森林総合研究所 レーザ誘起プラズマ発光分析による木材密度の測定方法
DE102008042906A1 (de) * 2008-10-16 2010-04-22 Rhein-Chemie Rheinau Gmbh Säulenpresse zur Qualitätsanalyse
CN101738399B (zh) * 2008-11-26 2014-08-27 软控股份有限公司 轮胎激光散斑检验机及其检验方法
EP2427755B1 (fr) * 2009-05-07 2015-10-14 Primetals Technologies France SAS Méthode et dispositif d'analyse spectrale d'une couche de revêtement métallique déposé à la surface d'une bande d'acier
FR2964458B1 (fr) * 2010-09-06 2012-09-07 Commissariat Energie Atomique Dispositif de cartographie et d'analyse a haute resolution d'elements dans des solides
CN102680436B (zh) * 2012-06-16 2014-04-09 山西大学 测定煤灰含碳量的方法及装置
CN102830063A (zh) * 2012-08-13 2012-12-19 青岛科技大学 一种检测橡胶中炭黑的方法
WO2014150696A1 (en) * 2013-03-15 2014-09-25 Materialytics, LLC Methods and systems for analyzing samples
CZ2013314A3 (cs) * 2013-04-26 2014-07-16 Univerzita Tomáše Bati ve Zlíně Etalon k hodnocení topografie materiálů
DE102013009962B3 (de) 2013-06-14 2014-11-06 K+S Aktiengesellschaft LIBS-Messtubus
CN105572102B (zh) * 2016-01-15 2017-03-08 清华大学深圳研究生院 一种硅橡胶复合绝缘材料老化状态检测方法
NL2016124B1 (en) 2016-01-20 2017-07-25 Black Bear Carbon B V A method for sorting tires
US9785851B1 (en) 2016-06-30 2017-10-10 Huron Valley Steel Corporation Scrap sorting system
EP3640626A1 (en) * 2018-10-18 2020-04-22 Kraiburg Austria GmbH & Co. KG Laser-induced breakdown spectroscopy device and use thereof for the analysis of chemical elements in rubber

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4076220A (en) * 1976-02-10 1978-02-28 Bridgestone Tire Company Limited Method of mixing and kneading control of a rubber kneader
IE47808B1 (en) * 1979-02-01 1984-06-27 Trinity College Dublin Nmr test method for measuring the homogeneity of dispersions of carbon black in rubber compositions
US4641968A (en) * 1984-12-17 1987-02-10 Baird Corporation Mobile spectrometric apparatus
DE4004627C2 (de) * 1990-02-15 1994-03-31 Krupp Ag Hoesch Krupp Verfahren zur Bestimmung von Materialeigenschaften polymerer Werkstoffe und Vorrichtung zur Durchführung des Verfahrens

Also Published As

Publication number Publication date
EP0652430A1 (en) 1995-05-10
JPH07167785A (ja) 1995-07-04
JP3662953B2 (ja) 2005-06-22
US5537207A (en) 1996-07-16
US5702550A (en) 1997-12-30
DE69327463D1 (de) 2000-02-03
EP0652430B1 (en) 1999-12-29
DE69327463T2 (de) 2000-07-20

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