ES2109511T3 - Procedimiento para la preparacion de una mezcla 2,4/2,6-diaminotolueno exenta de residuo. - Google Patents
Procedimiento para la preparacion de una mezcla 2,4/2,6-diaminotolueno exenta de residuo.Info
- Publication number
- ES2109511T3 ES2109511T3 ES93919214T ES93919214T ES2109511T3 ES 2109511 T3 ES2109511 T3 ES 2109511T3 ES 93919214 T ES93919214 T ES 93919214T ES 93919214 T ES93919214 T ES 93919214T ES 2109511 T3 ES2109511 T3 ES 2109511T3
- Authority
- ES
- Spain
- Prior art keywords
- mixture
- free
- tda
- toluilenodiamina
- diaminotoluol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
- C08G18/7621—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring being toluene diisocyanate including isomer mixtures
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/86—Separation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
EL PROCEDIMIENTO HACE POSIBLE LA SEPARACION CONTINUA DE RESIDUOS A PARTIR DE MEZCLAS M - DIAMINOTOLUOL EN BRUTO (MEZCLA M - TDA; 2,4/2,6 DIAMINOTOLUOL) PARA LA ELABORACION DE MEZCLAS 2,4/2,6 - DIAMINOTOLUOL (M - TDA) LIBRES DE RESIDUOS Y UTILIZACION DE LA MEZCLA M - TDA LIBRE DE RESIDUOS. PROCEDIMIENTO PARA LA ELABORACION DE M - TOLUILENODIAMINA LIBRE DE RESIDUOS MEDIANTE NITRIFICACION DE TOLUOL, HIDROGENACION DE LOS COMPUESTOS NITRO, SEPARACION DESTILATIVA DEL AGUA Y DE LOS DISOLVENTES, ASI COMO ELIMINACION DESTILATIVA DE ORTO-ISOMEROS A PARTIR DE LA MEZCLA TOLUILENODIAMINA. A PARTIR DEL RESTO QUE PERMANECE SE DESTILA 2,4 - Y 2,6 TOLUILENODIAMINA (M - TOLUILENODIAMINA - M TDA) DE TAL FORMA, QUE PERMANECE UN DEPOSITO CON UNA CONCENTRACION DE RESIDUO DESDE 30 HASTA 70 % EN PERO, SIENDO MEZCLADO ESTE DEPOSITO CON AGENTE AUXILIAR INERTE CONTRA TOLUILENODIAMINAS CON UN PUNTO DE EBULLICION MAYOR DE 290 TAL, QUE SE AJUSTA UNA CONCENTRACION DE RESIDUOS DESDE 28 HASTA 50 % EN PESO, ALTERNANDOSE ELDEPOSITO CON MEDIO AUXILIAR TAN LARGO COMO SE OBTIENE UNA DESTILACION DE UNA O MULTIPLES FASES, HASTA QUE SE CONSIGUE UNA CONCENTRACION RESIDUAL EN 2,4 - Y 2,6 - TOLUILENODIAMINA DESDE 1 HASTA 5 % EN PESO EN EL DEPOSITO Y SE DIVIDE EL RESIDUO PERMANENTE REMANENTE, SIENDO MOJADO CON LIQUIDO A TEMPERATURA BAJA.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4230098A DE4230098C1 (es) | 1992-09-09 | 1992-09-09 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2109511T3 true ES2109511T3 (es) | 1998-01-16 |
Family
ID=6467567
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES93919214T Expired - Lifetime ES2109511T3 (es) | 1992-09-09 | 1993-08-30 | Procedimiento para la preparacion de una mezcla 2,4/2,6-diaminotolueno exenta de residuo. |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP0659173B1 (es) |
JP (1) | JPH08501106A (es) |
KR (1) | KR950703513A (es) |
CA (1) | CA2142911A1 (es) |
DE (2) | DE4230098C1 (es) |
ES (1) | ES2109511T3 (es) |
MX (1) | MX9305506A (es) |
TW (1) | TW261604B (es) |
WO (1) | WO1994006752A1 (es) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19528781A1 (de) * | 1995-08-04 | 1997-02-06 | Bayer Ag | Verfahren zur Herstellung von Toluylendiisocyanat, spezielle Gemische aus Toluylendiamin und Wasser und deren Verwendung zur Herstellung von Toluylendiisocyanat |
DE19608443C1 (de) * | 1996-03-05 | 1997-07-24 | Bayer Ag | Verfahren zur Aufarbeitung von Amingemischen bei der Diaminotoluol-Herstellung unter Abtrennung der Schwersieder |
FR2777560B1 (fr) * | 1998-04-17 | 2000-06-09 | Rhodia Chimie Sa | Procede de purification de polyamines aromatiques |
DE102004001456A1 (de) | 2004-01-08 | 2005-08-11 | Basf Ag | Verfahren zur destillativen Aufbereitung von Toluylendiamin |
DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
US8030522B2 (en) * | 2006-06-07 | 2011-10-04 | Bayer Materialscience Llc | Process for the production of toluene diisocyanate |
DE102008063991A1 (de) | 2008-12-19 | 2010-06-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
JP7125406B2 (ja) | 2017-01-27 | 2022-08-24 | コベストロ・エルエルシー | 安定なトルエンジアミン残留物/水ブレンドの製造方法、関連組成物、およびそのようなブレンドの燃料としての使用法 |
-
1992
- 1992-09-09 DE DE4230098A patent/DE4230098C1/de not_active Expired - Fee Related
-
1993
- 1993-08-02 TW TW082106153A patent/TW261604B/zh active
- 1993-08-30 WO PCT/EP1993/002335 patent/WO1994006752A1/de active IP Right Grant
- 1993-08-30 CA CA002142911A patent/CA2142911A1/en not_active Abandoned
- 1993-08-30 DE DE59307795T patent/DE59307795D1/de not_active Expired - Fee Related
- 1993-08-30 KR KR1019950700912A patent/KR950703513A/ko not_active Application Discontinuation
- 1993-08-30 JP JP6507738A patent/JPH08501106A/ja active Pending
- 1993-08-30 EP EP93919214A patent/EP0659173B1/de not_active Expired - Lifetime
- 1993-08-30 ES ES93919214T patent/ES2109511T3/es not_active Expired - Lifetime
- 1993-09-08 MX MX9305506A patent/MX9305506A/es unknown
Also Published As
Publication number | Publication date |
---|---|
DE59307795D1 (de) | 1998-01-15 |
JPH08501106A (ja) | 1996-02-06 |
MX9305506A (es) | 1994-05-31 |
WO1994006752A1 (de) | 1994-03-31 |
KR950703513A (ko) | 1995-09-20 |
CA2142911A1 (en) | 1994-03-31 |
EP0659173A1 (de) | 1995-06-28 |
DE4230098C1 (es) | 1993-06-03 |
TW261604B (es) | 1995-11-01 |
EP0659173B1 (de) | 1997-12-03 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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