ES2051226A1 - Procedure for obtaining (-)-(2R,3R)-2-(2,4- dichlorophenyl)-3-(N-methanosulphonyl-N-methylamino)-1- (1H-1,2,4-triazol-1-yl)-2-butanol - Google Patents
Procedure for obtaining (-)-(2R,3R)-2-(2,4- dichlorophenyl)-3-(N-methanosulphonyl-N-methylamino)-1- (1H-1,2,4-triazol-1-yl)-2-butanolInfo
- Publication number
- ES2051226A1 ES2051226A1 ES09201562A ES9201562A ES2051226A1 ES 2051226 A1 ES2051226 A1 ES 2051226A1 ES 09201562 A ES09201562 A ES 09201562A ES 9201562 A ES9201562 A ES 9201562A ES 2051226 A1 ES2051226 A1 ES 2051226A1
- Authority
- ES
- Spain
- Prior art keywords
- methanosulphonyl
- procedure
- triazol
- dichlorophenyl
- methylamino
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 abstract 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 230000000843 anti-fungal effect Effects 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Abstract
Procedure for obtaining (-)-(2R,3R)-2-(2,4- dichlorophenyl)-3-(N-methanosulphonyl-N-methylamino)-1- (1H-1,2,4-triazol-1-yl)-2-butanol, of formula 1. A procedure is described which is characterized in that the amine 2 (obtained as described in Patent EP 332.387) is reacted with methanosulphonyl chloride in the presence of a base such as triethylamine within a suitable solvent such as chloroform or dichloromethane. Said compound has antifungal activity.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES9201562A ES2051226B1 (en) | 1992-07-15 | 1992-07-15 | PROCEDURE FOR OBTAINING (-) - (2R, 3R) -2- (2,4-DICLOROFENIL) -3- (N-METANOSULFONIL-N-METHYLAMINE) -1- (1H-1,2,4-TRIAZOL- 1-IL) -2-BUTANOL. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES9201562A ES2051226B1 (en) | 1992-07-15 | 1992-07-15 | PROCEDURE FOR OBTAINING (-) - (2R, 3R) -2- (2,4-DICLOROFENIL) -3- (N-METANOSULFONIL-N-METHYLAMINE) -1- (1H-1,2,4-TRIAZOL- 1-IL) -2-BUTANOL. |
Publications (2)
Publication Number | Publication Date |
---|---|
ES2051226A1 true ES2051226A1 (en) | 1994-06-01 |
ES2051226B1 ES2051226B1 (en) | 1994-12-16 |
Family
ID=8277781
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES9201562A Expired - Fee Related ES2051226B1 (en) | 1992-07-15 | 1992-07-15 | PROCEDURE FOR OBTAINING (-) - (2R, 3R) -2- (2,4-DICLOROFENIL) -3- (N-METANOSULFONIL-N-METHYLAMINE) -1- (1H-1,2,4-TRIAZOL- 1-IL) -2-BUTANOL. |
Country Status (1)
Country | Link |
---|---|
ES (1) | ES2051226B1 (en) |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0332387A1 (en) * | 1988-03-04 | 1989-09-13 | Sankyo Company Limited | Triazole derivatives, their preparation and their use as fungicides |
EP0480215A1 (en) * | 1990-10-08 | 1992-04-15 | J. URIACH & CIA. S.A. | New sulfonamides as antifungal agents |
-
1992
- 1992-07-15 ES ES9201562A patent/ES2051226B1/en not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0332387A1 (en) * | 1988-03-04 | 1989-09-13 | Sankyo Company Limited | Triazole derivatives, their preparation and their use as fungicides |
EP0480215A1 (en) * | 1990-10-08 | 1992-04-15 | J. URIACH & CIA. S.A. | New sulfonamides as antifungal agents |
Non-Patent Citations (1)
Title |
---|
CHEMICAL PHARMACEUTICAL BULLETIN, 39 (10), p. 2581-2589, 1991, OIDA et al.: "Triazole Antifungals. IV. Synthesis and Antifungal activities of 3-Acylamino-2-aryl-2-butanol Derivatives", Pharmaceutical Society of Japan, 1991. * |
Also Published As
Publication number | Publication date |
---|---|
ES2051226B1 (en) | 1994-12-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 20001009 |