EP4220055A1 - Pulse combustion dryer - Google Patents
Pulse combustion dryer Download PDFInfo
- Publication number
- EP4220055A1 EP4220055A1 EP22382065.5A EP22382065A EP4220055A1 EP 4220055 A1 EP4220055 A1 EP 4220055A1 EP 22382065 A EP22382065 A EP 22382065A EP 4220055 A1 EP4220055 A1 EP 4220055A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- steam
- pulse combustion
- chamber
- drying chamber
- line
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002485 combustion reaction Methods 0.000 title claims abstract description 157
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 73
- 238000001035 drying Methods 0.000 claims abstract description 58
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000001301 oxygen Substances 0.000 claims abstract description 25
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 25
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000001257 hydrogen Substances 0.000 claims abstract description 24
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 24
- 238000000926 separation method Methods 0.000 claims abstract description 20
- 239000000567 combustion gas Substances 0.000 claims abstract description 15
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims description 27
- 239000007789 gas Substances 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 16
- 235000011837 pasties Nutrition 0.000 claims description 13
- 239000007921 spray Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000002826 coolant Substances 0.000 claims description 4
- 238000011144 upstream manufacturing Methods 0.000 claims description 4
- 239000012855 volatile organic compound Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 abstract description 3
- 239000000446 fuel Substances 0.000 description 16
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 5
- 229910001882 dioxygen Inorganic materials 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- 230000010349 pulsation Effects 0.000 description 3
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 239000002360 explosive Substances 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- -1 i.e. Substances 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 239000003345 natural gas Substances 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 230000010355 oscillation Effects 0.000 description 2
- 238000013021 overheating Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000003915 liquefied petroleum gas Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
- 239000002918 waste heat Substances 0.000 description 1
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B23/00—Heating arrangements
- F26B23/02—Heating arrangements using combustion heating
- F26B23/026—Heating arrangements using combustion heating with pulse combustion, e.g. pulse jet combustion drying of particulate materials
Definitions
- the present invention relates to a device for drying liquid or pasty products by applying heated pulsed gas flow that impinges on the products.
- the invention relates to a pulse combustion dryer or pulse combustion spray dryer that comprises a pulse combustion burner using hydrogen as a fuel and oxygen as an oxidizing agent for the combustion.
- a pulse combustion dryer or pulse combustion spray dryer, is a kind of dryer that atomizes liquids or pasty products inside a drying chamber. To generate the spray, a pulse combustion burner is used.
- a pulse combustion burner has a cylindrical combustion chamber where fuel (usually a gaseous fuel like natural gas, propane, LPG etc., or a liquid fuel), is injected in a continuous way.
- fuel usually a gaseous fuel like natural gas, propane, LPG etc., or a liquid fuel
- air is introduced in a pulsating way, that means, air is introduced through a valve that opens and closes between 50 and 500 times per second, or at higher frequencies. That makes the combustion to be a pulsating or oscillating combustion, at same frequencies.
- the outlet of the combustion chamber is a narrow tailpipe. Combustion gases, combustion heat, and a number of pulses of between 50 and 500 times per second or more, leave the combustion chamber through the tailpipe.
- Pulse combustion burners are widely described in prior art. In some configurations, pulse combustion burners work valveless, and the pulsating of the combustion can suck the air without the need of valves.
- Known fuels used in pulse combustion dryers are fuel gases such as natural gas, methane or hydrogen, and liquid fuels such as alcohol.
- the end of the tailpipe is connected to a drying chamber, in this point a liquid or pasty product is introduced through a suitable injector.
- the pulses or strong pressure oscillations break the liquid or paste into thousands of small droplets, and the stream of hot combustion gases accelerate those droplets to near the speed of sound, which dramatically increases the heat and mass transfer rates.
- a spray is generated inside the drying chamber that evaporates the water from the droplets in an extremely short time, without product overheating, transforming the liquid or pasty product to be dried, into a dried powder.
- Dried powder, combustion gases and evaporated moisture leave the drying chamber to a powder separation system, which normally is a cyclone and/or a bag filter.
- a powder separation system which normally is a cyclone and/or a bag filter.
- an aspiration fan sucks the gases and directs them to a stack.
- EP1092060B1 discloses a pulse combustion dryer for dewatering a fibrous web in paper manufacturing using an unspecified fuel.
- US20170314778A1 discloses a pulse combustion dryer which may use hydrogen as a fuel in which the burner is designed to generate a pulsating flame for generating a pulsating hot gas flow as a swirl burner having a diffuser as element at is outlet.
- US20170307211A1 discloses a pulse combustion dryer which may use hydrogen as a fuel wherein an externally drivable pulsation device for at least a part of the mass flow directed to the burner is arranged upstream in the pipeline leading to the flame.
- US20070251120A1 discloses a pulse combustion dryer which may use hydrogen as a fuel which comprises a processing engine for generating a high velocity airstream and directing the high velocity airstream into an acceleration tube, the high velocity airstream having sufficient volume, heat and velocity to vaporize substantially all water present in an organic material stream; a work chamber mounted to the acceleration tube of the processing engine, the high velocity airstream routed into the work chamber, and the work chamber terminated within a micronizing dryer; and an injector pump to inject the organic material into the work chamber for interaction with the high velocity airstream.
- EP236152A1 discloses a pulse combustion dryer which may use hydrogen as a fuel, comprising a line located upstream the flame connected to an independent, externally driven pulsation device for at least a part of the mass flow directed to the burner.
- the solution given to that problem according to prior art is basically to circulate cooling water inside the walls of the pulse combustion burner, by means of, e.g., a cooling jacket or cooling coil, which makes the burner complex to build, and makes the operation of the pulse combustion dryer risky in case of cooling water failure during operation.
- a first aspect of the invention relates to a pulse combustion dryer wherein hydrogen is used as a fuel and wherein exhaust gases from the pulse combustion dryer are used efficiently to regulate the temperature in the pulse combustion burner.
- a second aspect of the invention relates to a pulse combustion dryer using hydrogen as a fuel, which does not require circulating cooling water inside the walls to lower the combustion temperature below 1500°C.
- a third aspect of the invention relates to a pulse combustion dryer that allows recirculating a portion of the water steam that leaves the dryer, into the combustion chamber of the pulse combustion burner for cooling the pulse combustion burner.
- a pulse combustion dryer comprising
- the flow rate and the speed at which the water steam is deviated towards and introduced into the pulse combustion chamber may depend on different factors such as the temperature difference between the inside of the pulse combustion chamber and the water steam, the volume of the pulse combustion chamber and how much the temperature of hot combustion gas passing to the dryer chamber is to be reduced, among others.
- the product feeding line may comprise a free end with an injector arranged within or at the end of the tailpipe to inject the product to be dried into the drying chamber.
- the pulse combustion dryer may further comprise at least one steam blower arranged in the steam supply line for sucking water steam from the steam outlet line.
- the steam supply line comprises:
- the oxygen inlet is arranged in the first branch downstream the first steam blower.
- the pulse combustion dryer may further comprise an aspiration fan arranged in the steam outlet line in a position between the steam supply line and the connection of the outlet line to the powder separation system for keeping a vacuum pressure of 1 to 50 mbar below atmospheric pressure in the drying chamber.
- a valve for example a rotary valve, may be arranged in the steam supply line upstream the at least one steam inlet of the pulse combustion burner.
- the valve is configured to operate such that it is able to provide a pulsed water steam flow entering the pulse combustion chamber.
- the separation system comprises a cyclone connected to an outlet of the drying chamber and to the steam outlet line.
- the separation system comprises a bag filter connected to an outlet (9a) of the drying chamber and to the steam outlet line.
- the separation system comprises a cyclone connected to an outlet of the drying chamber, and a bag filter connected to the cyclone and to the steam outlet line.
- the separation system comprises a cyclone connectable to an outlet of the drying chamber and to the steam outlet line, and a bag filter connectable to the cyclone and to the outlet of the drying chamber, and connected to the steam outlet line.
- the steam outlet line can contain a filter, like an activated carbon filter or similar, to eliminate organic volatile compounds than can volatilize from the dried product during the drying process. These organic volatile compounds are eliminated, in particular, from the water steam once separated from the dried product.
- the pulse combustion dryer according to the invention provides some advantages, e.g.:
- Figure 1 shows a schematic view of an embodiment of a pulse combustion dryer according to the invention.
- the pulse combustion dryer comprises a product tank 1 for containing a liquid or a pasty product to be dried, an injector 3, a pulse combustion burner 4, a drying chamber 9, a cyclone 10, and a bag filter 11.
- the tank 1 is connected to a tailpipe 4a of the pulse combustion burner 4 by a product feeding line 1a to the injector 3 which is arranged at end of the tailpipe 4a.
- the tailpipe 4a connects an outlet of the pulse combustion burner 4 to an inlet of the drying chamber 9.
- the pulse combustion burner 4 comprises a combustion chamber 4b and a hydrogen inlet connected to a hydrogen gas train 5.
- a feeding pump 2 is arranged in the product feeding line 1a.
- the drying chamber 9 comprises an outlet 9a which is connected by an outlet line 9b to an inlet of the cyclone 10, and also to a first bypass line 9c which is connected to an inlet of the bag filter 11.
- a first check valve 15 is positioned in the first bypass line 9c to open or close access to the first bypass line 9c and a second check valve 15a is positioned in the outlet line 9b between the inlet of the cyclone 10 and the connection of the outlet line 9a and the first bypass line 9c, to open or close the outlet line 9a.
- the cyclone 10 and the bag filter 11 constitute a particle separation system.
- the particle separation system comprises only the cyclone 10 or only the bag filter 11.
- the cyclone 10 comprises an outlet which is connected to an inlet of the bag filter 11 through an outlet line 10a, and to a second bypass line 10c connected to the steam outlet line 13a.
- the bag filter 11 comprises a steam evacuation outlet 11a which is also connected to the steam outlet line 13a.
- a third check valve 16 is connected in the outlet line 10a to open or close access to the outlet line 10a, and a fourth check valve 15a is positioned in the second bypass line 10c to open or close access to the second bypass line 10c.
- a steam supply line 14,14a,14b derives from the steam outlet line 13a, downstream the steam evacuation outlet 11a of the bag filter 11 and the connection of the second bypass line 10c to the steam outlet line 13a.
- An aspiration fan 12 is arranged in the steam outlet line 13a in a position between the steam supply line 14, and the steam evacuation outlet 11a of the bag filter 11 and the connection of the second bypass line 10c to the steam outlet line 13a.
- the steam supply line 14 comprises a first branch 14a and a second branch 14b which are each connected to a respective steam inlet of the pulse combustion burner 4.
- a first steam blower 7 is arranged in the first branch 14a and an oxygen gas train 6 is connected to the first between the first steam blower 7 and the corresponding steam inlet of the pulse combustion burner 4.
- a second steam blower 8 is arranged in the second branch 14a of the steam supply line 14.
- the liquid or pasty product to be dried is pumped by pump 2 through the product feeding line 1a, from product tank 1 to the injector 3 that within the tailpipe 4a of the pulse combustion burner 4.
- the pulse combustion burner 4 uses hydrogen H 2 as fuel and oxygen O 2 as an oxidizing agent for the combustion.
- Hydrogen flow can come from an in-situ electrolysis process, or can be any other conventional hydrogen source.
- the hydrogen is introduced in the pulse combustion burner 4 through a proper hydrogen gas train 5, in a constant mass flow.
- a first steam blower 7 introduces water steam into the pulse combustion burner 4.
- the water steam is introduced through a valve, e.g., a rotary valve, (not shown in figure 1 ), because this allows controlling the frequency of pulsations, independently from other combustion parameters like combustion temperature.
- a valveless pulse combustion burner 4 the water steam will enter the pulse combustion burner 4 without the need of valves or a blower, using the aspiration provided by the pulses of the pulse combustion burner 4 itself.
- the steam blower 7 sucks a portion of the water steam flowing through the steam outlet line 13a, into the steam supply line 14 which means that a portion of the water steam is recirculated after the product has been dried, and there is no need of a specific water steam generator or an external water steam supply.
- Pure oxygen O 2 provided by the oxygen gas train 6 is introduced into the first branch 14a of the steam supply line 14, as the oxidizing agent for combustion in the combustion chamber 4b of the pulse combustion burner 4.
- This oxygen supplied may originate from an in-situ electrolysis process, from an air purification process, or can come from any other conventional oxygen source.
- the oxygen is introduced through a proper oxygen gas train 6, in a constant mass flow.
- Hydrogen mass flow is constant and is directly proportional to the amount of water that has to be evaporated from the liquid or pasty product to be dried. Oxygen mass flow is also constant and stoichiometric to the hydrogen flow combustion.
- Water steam flow from the first steam blower 7, is controlled by the desired combustion temperature in the pulse combustion burner 4, i.e., when a lower combustion temperature is desired, a higher flow of water steam is blown, and vice versa. Without this adjustable water steam flow, combustion temperature would be higher than 1500°C, but using the adjustable water steam flow, temperature can be cooled down to 300°C to 1200°C.No cooling jacket or coil is needed to protect the pulse combustion burner 4 from overheating.
- pure water steam is the only product of the combustion in the combustion chamber 4b of the pulse combustion burner 4.
- the second steam blower 8 (optional) in the second branch 14b can be used to get cooler temperatures around the product injector 3, and to direct spray to the inside the drying chamber 9.
- Temperature at which the mixture of powder and water steam leave the drying chamber 9, is controlled by the flow of product to be dried; if a lower temperature is desired, flow is increased, and vice versa.
- any point of the drying process between product injector 3 and the steam outlet 13 have to be at least 100°C, at atmospheric pressure. At pressures lower than atmospheric, less than 100°C can be reached without steam condensations in the pulse combustion dryer.
- the mixture of gases i.e., water steam from pulse combustion burner 4 and evaporated moisture from the product to be dried, and powder
- the outlet line 9b is led through the drying chamber 9 through the outlet 9a thereof.
- the steam/product mixture exiting the drying chamber 9 may be guided through the outlet line 9a only the cyclone 10 and from there through the second bypass line 10c, so that water steam coming from the cyclone 11 is guided to the steam outlet line 13a by closing outlet line 10a by means of the third check valve 16 and opening the second bypass line 10c by means of the fourth check valve 16a.
- the steam/product mixture exiting the drying chamber 9 may be guided through the outlet line 9a and the first bypass line 9c only to the bag filter 11, so that water steam coming from the bag filter 11 is guided to the steam outlet line 13a, by opening the first check valve 15 and closing the second check valve 15a.
- the steam/product mixture exiting the drying chamber 9 is guided to the cyclone 10 through the outlet line 9b by closing the first check valve 15 and opening the second check valve 15a, and from the cyclone 10 to the bag filter 11 through the outlet line 10a by opening the third check valve 16 and closing the fourth check valve 16a, so that water steam coming from the bag filter 11 is guided to the steam outlet line 13a.
- Election of the path of the flow of the steam/product mixture exiting the drying chamber 9 only through the cyclone 10 or only through the bag filter 11 or both the cyclone 10 and the bag filter 11 depends on the properties of the product to be dried.
- the cyclone 10 and the bag filter 11 are provided respective powder outlets 10b,11b allowing extraction of the dried powder product which has been separated from the water steam.
- the aspiration fan 12 sucks the water steam originating in the drying chamber 9 which is present in the cyclone 10 and/or the bag filter 11, to keep a slight vacuum pressure of 1 to 50 mbar below atmospheric pressure in the drying chamber. A higher vacuum can be used, if low drying temperatures are desired without water steam condensation problems.
- a portion of the water steam sucked by the fan 12 through the steam outlet line 13a is sucked into the steam supply line 14 and blown towards through the first branch 14a by action of the first steam blower 7 and, where desired, also to through the second branch 14b by action of the second steam blower 8, to the respective steam inlets of the pulse combustion burner 4.
- a portion of the water steam coming from the drying chamber 9 and from which the dried product has been removed is recirculated by the first steam blower 7 and, optionally, by the second steam blower 8, into the pulse combustion burner 4, whilst the remaining water steam leaves the pulse combustion dryer through the steam outlet 13.
- the gas flow in the outlet line 13a is a pure, or almost pure water steam flow.
- the pulse combustion dryer of the invention provides some advantages, e.g.:
- first, second, third, etc. have been used herein to describe devices, elements or parameters. It will be understood that the devices, elements or parameters should not be limited by these terms since the terms are only used to distinguish one device, element or parameter from another.
- first branch could as well be named second branch, and the second branch could be named first branch without departing from the scope of this disclosure.
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Fluidized-Bed Combustion And Resonant Combustion (AREA)
- Drying Of Solid Materials (AREA)
Abstract
Description
- The present invention relates to a device for drying liquid or pasty products by applying heated pulsed gas flow that impinges on the products. Particularly, the invention relates to a pulse combustion dryer or pulse combustion spray dryer that comprises a pulse combustion burner using hydrogen as a fuel and oxygen as an oxidizing agent for the combustion.
- A pulse combustion dryer, or pulse combustion spray dryer, is a kind of dryer that atomizes liquids or pasty products inside a drying chamber. To generate the spray, a pulse combustion burner is used.
- A pulse combustion burner, has a cylindrical combustion chamber where fuel (usually a gaseous fuel like natural gas, propane, LPG etc., or a liquid fuel), is injected in a continuous way. On the other hand, air is introduced in a pulsating way, that means, air is introduced through a valve that opens and closes between 50 and 500 times per second, or at higher frequencies. That makes the combustion to be a pulsating or oscillating combustion, at same frequencies. The outlet of the combustion chamber is a narrow tailpipe. Combustion gases, combustion heat, and a number of pulses of between 50 and 500 times per second or more, leave the combustion chamber through the tailpipe. When the frequency of the pulses is more or less equal to the natural resonance of the combustion chamber and/or the tailpipe, the combustion reaches resonance and the pulses get a higher amplitude or pressure oscillation. Pulse combustion burners are widely described in prior art. In some configurations, pulse combustion burners work valveless, and the pulsating of the combustion can suck the air without the need of valves. Known fuels used in pulse combustion dryers are fuel gases such as natural gas, methane or hydrogen, and liquid fuels such as alcohol.
- The end of the tailpipe is connected to a drying chamber, in this point a liquid or pasty product is introduced through a suitable injector. The pulses or strong pressure oscillations break the liquid or paste into thousands of small droplets, and the stream of hot combustion gases accelerate those droplets to near the speed of sound, which dramatically increases the heat and mass transfer rates. As a result, a spray is generated inside the drying chamber that evaporates the water from the droplets in an extremely short time, without product overheating, transforming the liquid or pasty product to be dried, into a dried powder.
- Dried powder, combustion gases and evaporated moisture, leave the drying chamber to a powder separation system, which normally is a cyclone and/or a bag filter. In the end, an aspiration fan sucks the gases and directs them to a stack.
-
EP1092060B1 discloses a pulse combustion dryer for dewatering a fibrous web in paper manufacturing using an unspecified fuel. -
US20170314778A1 discloses a pulse combustion dryer which may use hydrogen as a fuel in which the burner is designed to generate a pulsating flame for generating a pulsating hot gas flow as a swirl burner having a diffuser as element at is outlet. -
US20170307211A1 discloses a pulse combustion dryer which may use hydrogen as a fuel wherein an externally drivable pulsation device for at least a part of the mass flow directed to the burner is arranged upstream in the pipeline leading to the flame. -
US20070251120A1 discloses a pulse combustion dryer which may use hydrogen as a fuel which comprises a processing engine for generating a high velocity airstream and directing the high velocity airstream into an acceleration tube, the high velocity airstream having sufficient volume, heat and velocity to vaporize substantially all water present in an organic material stream; a work chamber mounted to the acceleration tube of the processing engine, the high velocity airstream routed into the work chamber, and the work chamber terminated within a micronizing dryer; and an injector pump to inject the organic material into the work chamber for interaction with the high velocity airstream. -
EP236152A1 - One problem of operating the burner of a pulse combustion dryer with hydrogen and oxygen in stoichiometric conditions, is that the combustion temperature will be higher than 1500°C. Such a high combustion temperature can melt or highly damage the burner. The solution given to that problem according to prior art is basically to circulate cooling water inside the walls of the pulse combustion burner, by means of, e.g., a cooling jacket or cooling coil, which makes the burner complex to build, and makes the operation of the pulse combustion dryer risky in case of cooling water failure during operation.
- A first aspect of the invention relates to a pulse combustion dryer wherein hydrogen is used as a fuel and wherein exhaust gases from the pulse combustion dryer are used efficiently to regulate the temperature in the pulse combustion burner.
- A second aspect of the invention relates to a pulse combustion dryer using hydrogen as a fuel, which does not require circulating cooling water inside the walls to lower the combustion temperature below 1500°C.
- A third aspect of the invention relates to a pulse combustion dryer that allows recirculating a portion of the water steam that leaves the dryer, into the combustion chamber of the pulse combustion burner for cooling the pulse combustion burner.
- According to the invention, there is provided a pulse combustion dryer comprising
- a pulse combustion burner having a cylindrical pulse combustion chamber, to generate a pulsating combustion, a drying chamber and a tailpipe connected to the pulse combustion chamber for receiving and pressurizing pulses of hot combustion gas, and to the drying chamber for receiving pressurized pulses of hot combustion gas,
- a hydrogen inlet for feeding hydrogen into the pulse combustion chamber,
- an oxygen inlet for feeding oxygen into the pulse combustion chamber,
- a product feeding line for feeding a liquid or pasty product to be dried into the drying chamber to produce a spray of water steam and dried product powder,
- a powder separation system having at least one powder outlet connected to the drying chamber to separate the dried product powder from water steam coming from the drying chamber,
- a steam outlet line connected to the powder separation system to evacuate the water steam,
- wherein
- the steam outlet line is connected to a steam supply line which is connected to at least one steam inlet of the pulse combustion burner, the steam supply line being configured to deviate at least a portion of the water steam that passes through the steam outlet line to the at least one steam inlet of the pulse combustion burner to enter the pulse combustion chamber as a cooling medium at a rate of water steam sufficient for cooling the hot combustion gas passing to the dryer chamber, or combustion temperature, to a reduced gas temperature to between 300°C and 1200°C;
- the oxygen inlet is arranged in a portion of the steam supply line to mix oxygen and water steam that passes through the steam supply line to the at least one steam inlet of the pulse combustion burner.
- The flow rate and the speed at which the water steam is deviated towards and introduced into the pulse combustion chamber may depend on different factors such as the temperature difference between the inside of the pulse combustion chamber and the water steam, the volume of the pulse combustion chamber and how much the temperature of hot combustion gas passing to the dryer chamber is to be reduced, among others.
- In some embodiments, the product feeding line may comprise a free end with an injector arranged within or at the end of the tailpipe to inject the product to be dried into the drying chamber.
- In some embodiments, the pulse combustion dryer may further comprise at least one steam blower arranged in the steam supply line for sucking water steam from the steam outlet line.
- In some embodiments, the steam supply line comprises:
- a first branch connected to a first steam inlet of the pulse combustion burner,
- a second branch connected to a second steam inlet of the pulse combustion burner,
- a first steam blower arranged in the first branch for sucking a first portion of water steam from the steam outlet line to provide a basic water steam entering into the pulse combustion chamber at a basic rate sufficient to reduce the combustion temperature or to cool the hot combustion gas passing to the dryer chamber to a first reduced gas temperature, and
- a second steam blower arranged in the second branch for sucking a second portion of water steam from the steam outlet line to provide a further water steam entering into or surrounding the pulse combustion chamber or the tailpipe, together with the basic water steam, at a further rate sufficient, to cool the hot combustion gas passing to the dryer chamber to a second reduced gas temperature.
- In some embodiments, the oxygen inlet is arranged in the first branch downstream the first steam blower.
- In some embodiments, the pulse combustion dryer may further comprise an aspiration fan arranged in the steam outlet line in a position between the steam supply line and the connection of the outlet line to the powder separation system for keeping a vacuum pressure of 1 to 50 mbar below atmospheric pressure in the drying chamber.
- In some embodiments, a valve, for example a rotary valve, may be arranged in the steam supply line upstream the at least one steam inlet of the pulse combustion burner. The valve is configured to operate such that it is able to provide a pulsed water steam flow entering the pulse combustion chamber.
- In some embodiments, the separation system comprises a cyclone connected to an outlet of the drying chamber and to the steam outlet line.
- In other embodiments, the separation system comprises a bag filter connected to an outlet (9a) of the drying chamber and to the steam outlet line.
- In still other embodiments, the separation system comprises a cyclone connected to an outlet of the drying chamber, and a bag filter connected to the cyclone and to the steam outlet line.
- In further embodiments, the separation system comprises a cyclone connectable to an outlet of the drying chamber and to the steam outlet line, and a bag filter connectable to the cyclone and to the outlet of the drying chamber, and connected to the steam outlet line.
- In some embodiments, the steam outlet line can contain a filter, like an activated carbon filter or similar, to eliminate organic volatile compounds than can volatilize from the dried product during the drying process. These organic volatile compounds are eliminated, in particular, from the water steam once separated from the dried product.
- The pulse combustion dryer according to the invention provides some advantages, e.g.:
- Water steam contained in the exhaust gases generated is used as a cooling medium for the pulse combustion burner.
- Basically, no free oxygen is present in the drying medium, which makes the atmosphere inside the dryer, a non-explosive atmosphere.
- The drying medium will not oxidize the product to be dried.
- Treatment of exhaust gases to eliminate odors, will be minimized, or not needed.
- No product of combustion by fuels containing carbon that may contact the product to be dried, is generated.
- No NOx is generated in the combustion, as there is no N2 present in combustion.
- Other aspects, advantages and features of the invention become apparent from the present specification and drawings.
- To complete the description and in order to provide for a better understanding of the invention, a drawing is provided. Said drawing forms an integral part of the description and illustrates an embodiment of the invention, which should not be interpreted as restricting the scope of the invention, but just as an example of how the invention can be carried out. The drawing comprises the following figure:
Figure 1 shows a schematic view of an embodiment of a pulse combustion dryer according to the invention. - The reference signs in this drawing have the following meanings:
- 1
- Product tank for containing liquid or pasty product to be dried
- 1a
- Product feeding line
- 2
- Feeding pump for liquid or pasty product to be dried
- 3
- Injector of liquid or pasty product to be dried
- 4
- Pulse combustion burner
- 4a
- Tailpipe
- 4b
- Pulse combustion chamber
- 5
- Hydrogen gas train
- 6
- Oxygen gas train
- 7
- First steam blower
- 8
- Second steam blower for temperature control around product injector
- 9
- Drying chamber
- 9a
- Outlet
- 9b
- Outlet line
- 9c
- Bypass line
- 10
- Cyclone for dried powder separation
- 10a
- Outlet line
- 10b
- Powder outlet
- 10c
- Bypass line
- 11
- Bag filter
- 11a
- Outlet line
- 11b
- Powder outlet
- 12
- Aspiration fan
- 13
- Steam outlet
- 13a
- Steam outlet line
- 14
- steam supply line
- 14a
- First branch of the steam supply line
- 14b
- Second branch of the steam supply line
- 15
- First check valve
- 15a
- Second check valve
- 16
- Third check valve
- 16a
- Fourth check valve
- H2
- Hydrogen
- O2
- Oxygen
- In the embodiment shown in
figure 1 , the pulse combustion dryer comprises aproduct tank 1 for containing a liquid or a pasty product to be dried, aninjector 3, a pulse combustion burner 4, a dryingchamber 9, acyclone 10, and abag filter 11. - The
tank 1 is connected to atailpipe 4a of the pulse combustion burner 4 by aproduct feeding line 1a to theinjector 3 which is arranged at end of thetailpipe 4a. Thetailpipe 4a connects an outlet of the pulse combustion burner 4 to an inlet of the dryingchamber 9. The pulse combustion burner 4 comprises acombustion chamber 4b and a hydrogen inlet connected to ahydrogen gas train 5. Afeeding pump 2 is arranged in theproduct feeding line 1a. - The drying
chamber 9 comprises anoutlet 9a which is connected by anoutlet line 9b to an inlet of thecyclone 10, and also to afirst bypass line 9c which is connected to an inlet of thebag filter 11. Afirst check valve 15 is positioned in thefirst bypass line 9c to open or close access to thefirst bypass line 9c and asecond check valve 15a is positioned in theoutlet line 9b between the inlet of thecyclone 10 and the connection of theoutlet line 9a and thefirst bypass line 9c, to open or close theoutlet line 9a. In the embodiment shown, thecyclone 10 and thebag filter 11 constitute a particle separation system. In other embodiments, the particle separation system comprises only thecyclone 10 or only thebag filter 11. - The
cyclone 10 comprises an outlet which is connected to an inlet of thebag filter 11 through anoutlet line 10a, and to asecond bypass line 10c connected to thesteam outlet line 13a. Thebag filter 11 comprises asteam evacuation outlet 11a which is also connected to thesteam outlet line 13a. Athird check valve 16 is connected in theoutlet line 10a to open or close access to theoutlet line 10a, and afourth check valve 15a is positioned in thesecond bypass line 10c to open or close access to thesecond bypass line 10c. - A
steam supply line steam outlet line 13a, downstream thesteam evacuation outlet 11a of thebag filter 11 and the connection of thesecond bypass line 10c to thesteam outlet line 13a. Anaspiration fan 12 is arranged in thesteam outlet line 13a in a position between thesteam supply line 14, and thesteam evacuation outlet 11a of thebag filter 11 and the connection of thesecond bypass line 10c to thesteam outlet line 13a. - The
steam supply line 14 comprises afirst branch 14a and asecond branch 14b which are each connected to a respective steam inlet of the pulse combustion burner 4. Afirst steam blower 7 is arranged in thefirst branch 14a and anoxygen gas train 6 is connected to the first between thefirst steam blower 7 and the corresponding steam inlet of the pulse combustion burner 4. Asecond steam blower 8 is arranged in thesecond branch 14a of thesteam supply line 14. - In operation, the liquid or pasty product to be dried, is pumped by
pump 2 through theproduct feeding line 1a, fromproduct tank 1 to theinjector 3 that within thetailpipe 4a of the pulse combustion burner 4. - The pulse combustion burner 4, uses hydrogen H2 as fuel and oxygen O2 as an oxidizing agent for the combustion. Hydrogen flow can come from an in-situ electrolysis process, or can be any other conventional hydrogen source. The hydrogen is introduced in the pulse combustion burner 4 through a proper
hydrogen gas train 5, in a constant mass flow. - Instead of using a blower to introduce combustion air into the pulse combustion burner 4, like conventional pulse combustion burners do, according to this invention, a
first steam blower 7 introduces water steam into the pulse combustion burner 4. Preferably, the water steam is introduced through a valve, e.g., a rotary valve, (not shown infigure 1 ), because this allows controlling the frequency of pulsations, independently from other combustion parameters like combustion temperature. When a valveless pulse combustion burner 4 is used, the water steam will enter the pulse combustion burner 4 without the need of valves or a blower, using the aspiration provided by the pulses of the pulse combustion burner 4 itself. - The
steam blower 7 sucks a portion of the water steam flowing through thesteam outlet line 13a, into thesteam supply line 14 which means that a portion of the water steam is recirculated after the product has been dried, and there is no need of a specific water steam generator or an external water steam supply. - Pure oxygen O2 provided by the
oxygen gas train 6 is introduced into thefirst branch 14a of thesteam supply line 14, as the oxidizing agent for combustion in thecombustion chamber 4b of the pulse combustion burner 4. This oxygen supplied may originate from an in-situ electrolysis process, from an air purification process, or can come from any other conventional oxygen source. The oxygen is introduced through a properoxygen gas train 6, in a constant mass flow. - Hydrogen mass flow is constant and is directly proportional to the amount of water that has to be evaporated from the liquid or pasty product to be dried. Oxygen mass flow is also constant and stoichiometric to the hydrogen flow combustion. Water steam flow from the
first steam blower 7, is controlled by the desired combustion temperature in the pulse combustion burner 4, i.e., when a lower combustion temperature is desired, a higher flow of water steam is blown, and vice versa. Without this adjustable water steam flow, combustion temperature would be higher than 1500°C, but using the adjustable water steam flow, temperature can be cooled down to 300°C to 1200°C.No cooling jacket or coil is needed to protect the pulse combustion burner 4 from overheating. - In this way, pure water steam is the only product of the combustion in the
combustion chamber 4b of the pulse combustion burner 4. Additionally, the second steam blower 8 (optional) in thesecond branch 14b can be used to get cooler temperatures around theproduct injector 3, and to direct spray to the inside the dryingchamber 9. - Water steam leaves the pulse combustion burner 4 at a temperature between 300 and 1200 °C, which means that superheated water steam is the drying medium in all the volume of the drying
chamber 9. Water steam from the pulse combustion burner 4, together with the pulses generated, hit the liquid or pasty product to be dried that is introduced through theinjector 3. Atomization of the product takes place in dryingchamber 9, and water from droplets is quickly evaporated, so that the water steam in the dryingchamber 9 is cooled down from between 300-1200°C, to a lower temperature between 100 and 200°C, depending on the product to be dried. Temperature at which the mixture of powder and water steam leave the dryingchamber 9, is controlled by the flow of product to be dried; if a lower temperature is desired, flow is increased, and vice versa. - To avoid condensation, any point of the drying process between
product injector 3 and thesteam outlet 13, have to be at least 100°C, at atmospheric pressure. At pressures lower than atmospheric, less than 100°C can be reached without steam condensations in the pulse combustion dryer. - After leaving the drying
chamber 9 through theoutlet 9a thereof, the mixture of gases, i.e., water steam from pulse combustion burner 4 and evaporated moisture from the product to be dried, and powder, are led through theoutlet line 9b to thecyclone 10, or through thefirst bypass line 9c directly to thebag filter 11 through thefirst bypass line 9c. - The steam/product mixture exiting the drying
chamber 9 may be guided through theoutlet line 9a only thecyclone 10 and from there through thesecond bypass line 10c, so that water steam coming from thecyclone 11 is guided to thesteam outlet line 13a by closingoutlet line 10a by means of thethird check valve 16 and opening thesecond bypass line 10c by means of thefourth check valve 16a. Alternatively, the steam/product mixture exiting the dryingchamber 9 may be guided through theoutlet line 9a and thefirst bypass line 9c only to thebag filter 11, so that water steam coming from thebag filter 11 is guided to thesteam outlet line 13a, by opening thefirst check valve 15 and closing thesecond check valve 15a. In another alternative, the steam/product mixture exiting the dryingchamber 9 is guided to thecyclone 10 through theoutlet line 9b by closing thefirst check valve 15 and opening thesecond check valve 15a, and from thecyclone 10 to thebag filter 11 through theoutlet line 10a by opening thethird check valve 16 and closing thefourth check valve 16a, so that water steam coming from thebag filter 11 is guided to thesteam outlet line 13a. Election of the path of the flow of the steam/product mixture exiting the dryingchamber 9 only through thecyclone 10 or only through thebag filter 11 or both thecyclone 10 and thebag filter 11 depends on the properties of the product to be dried. Thecyclone 10 and thebag filter 11 are providedrespective powder outlets - The
aspiration fan 12 sucks the water steam originating in the dryingchamber 9 which is present in thecyclone 10 and/or thebag filter 11, to keep a slight vacuum pressure of 1 to 50 mbar below atmospheric pressure in the drying chamber. A higher vacuum can be used, if low drying temperatures are desired without water steam condensation problems. A portion of the water steam sucked by thefan 12 through thesteam outlet line 13a, is sucked into thesteam supply line 14 and blown towards through thefirst branch 14a by action of thefirst steam blower 7 and, where desired, also to through thesecond branch 14b by action of thesecond steam blower 8, to the respective steam inlets of the pulse combustion burner 4.Thereby, a portion of the water steam coming from the dryingchamber 9 and from which the dried product has been removed, is recirculated by thefirst steam blower 7 and, optionally, by thesecond steam blower 8, into the pulse combustion burner 4, whilst the remaining water steam leaves the pulse combustion dryer through thesteam outlet 13. - The gas flow in the
outlet line 13a is a pure, or almost pure water steam flow. The amount of water steam leaving the pulse combustion dryer 4 throughsteam outlet 13, basically equals the amount of water evaporated from the product to be dried, plus the water steam generated in hydrogen and oxygen combustion. This makes the pulse combustion dryer work as a superheated water steam dryer. - As apparent, the pulse combustion dryer of the invention provides some advantages, e.g.:
- Water steam contained in the exhaust gases generated is used as a cooling medium for the pulse combustion burner, and waste heat contained in the exhaust gases generated may be relatively easy to be re-used, in other thermal processes like for example evaporators.
- Basically, no free oxygen is present in the drying medium, which makes the atmosphere inside the dryer, a non-explosive atmosphere.
- The drying medium will not oxidize the product to be dried.
- Treatment of exhaust gases to eliminate odors, will be minimized, or not needed.
- No product of combustion by fuels containing carbon that may contact the product to be dried, is generated.
- No NOx is generated in the combustion, as there is no N2 present in combustion.
- In this text, the terms first, second, third, etc. have been used herein to describe devices, elements or parameters. It will be understood that the devices, elements or parameters should not be limited by these terms since the terms are only used to distinguish one device, element or parameter from another. For example, the first branch could as well be named second branch, and the second branch could be named first branch without departing from the scope of this disclosure.
- In this text, the term "comprises" and its derivations (such as "comprising", etc.) should not be understood in an excluding sense, that is, these terms should not be interpreted as excluding the possibility that what is described and defined may include further elements, steps, etc.
- On the other hand, the invention is obviously not limited to the specific embodiment(s) described herein, but also encompasses any variations that may be considered by any person skilled in the art (for example, as regards the choice of materials, dimensions, components, configuration, etc.), within the general scope of the invention as defined in the claims.
Claims (13)
- A pulse combustion dryer comprisinga pulse combustion burner (4) having a cylindrical pulse combustion chamber (4b), to generate a pulsating combustion, a drying chamber (9) and a tailpipe (4a) connected to the pulse combustion chamber (4b) for receiving and pressurizing pulses of hot combustion gas, and to the drying chamber (9) for receiving pressurized pulses of hot combustion gas,a hydrogen inlet for feeding hydrogen into the pulse combustion chamber (4b),an oxygen inlet for feeding oxygen into the pulse combustion chamber (4b),a product feeding line (1a) for feeding a liquid or pasty product to be dried into the drying chamber (9) to produce a spray of water steam and dried product powder,a powder separation system (10, 11) having at least one powder outlet (10b, 11b) connected to the drying chamber (9) to separate the dried product powder and water steam coming from the drying chamber (9),a steam outlet line (13a) connected to the powder separation system (10, 11) to evacuate water steam,characterized in thatthe steam outlet line (13a) is connected to a steam supply line (14, 14a, 14b) which is connected to at least one steam inlet of the pulse combustion burner (4), the steam supply line (14, 14a, 14b) for deviating at least a portion of the water steam that passes through the steam outlet line (13a) to the at least one steam inlet of the pulse combustion burner (4) to enter the pulse combustion chamber (4b) as a cooling medium at a rate of water steam sufficient for cooling the hot combustion gas passing to the dryer chamber (9) to a reduced gas temperature of between 300°C to 1200°C; andthe oxygen inlet is arranged in a portion of the steam supply line (14, 14a, 14b) to mix oxygen and water steam that passes through the steam supply line (14, 14a, 14b) to the at least one steam inlet of the pulse combustion burner (4).
- The pulse combustion dryer according to claim 1, wherein the product feeding line (1a) comprises a free end with an injector (3) arranged within or at the end of the tailpipe (4a) to inject the product to be dried into the drying chamber (9).
- The pulse combustion dryer according to claim 1 or 2, comprising at least one steam blower (7, 8) arranged in the steam supply line (14, 14a, 14b) for sucking water steam from the steam outlet line (13a).
- The pulse combustion dryer according to claim 1, 2 or 3, wherein the steam supply line (14, 14a, 14b) comprises:a first branch (14a) connected to a first steam inlet of the pulse combustion burner (4),a second branch (14b) connected to a second steam inlet of the pulse combustion burner (4),a first steam blower (7) arranged in the first branch (14a) for sucking a first portion of water steam from the steam outlet line (13a) to provide a basic water steam entering into the pulse combustion chamber (4b) at a basic rate sufficient to cool the hot combustion gas passing to the dryer chamber (9) to a first reduced gas temperature, anda second steam blower (8) arranged in the second branch (14b) for sucking a second portion of water steam from the steam outlet line (13a) to provide a further water steam entering into or surrounding the pulse combustion chamber (4b) or the tailpipe (4a), together with the basic water steam, at a further rate sufficient, to cool the hot combustion gas passing to the dryer chamber (9) to a second reduced gas temperature.
- The pulse combustion dryer according to claim 4, wherein the oxygen inlet is arranged in the first branch (14a) downstream the first steam blower (7).
- The pulse combustion dryer according to any one of claims 1 to 5, comprising an aspiration fan (12) arranged in the steam outlet line (13) in a position between the steam supply line (14) and the connection of the outlet line (13a) to the powder separation system (10, 11), the aspiration fan being configured to keep a vacuum pressure of 1 to 50 mbar below atmospheric pressure in the drying chamber.
- The pulse combustion dryer according to any one of claims 1 to 6, comprising a valve, preferably a rotary valve, arranged in the steam supply line (14, 14a, 14b) upstream the at least one steam inlet of the pulse combustion burner (4), to provide a pulsed water steam flow entering the pulse combustion chamber (4b).
- The pulse combustion dryer according to any one of claims 1 to 7, wherein the powder separation system comprises a cyclone (10) connected to an outlet (9a) of the drying chamber (9) and to the steam outlet line (13a).
- The pulse combustion dryer according to any one of claims 1 to 7, wherein the powder separation system comprises a bag filter (11) connected to an outlet (9a) of the drying chamber (9) and to the steam outlet line (13a).
- The pulse combustion dryer according to any one of claims 1 to 7, wherein the powder separation system comprises a cyclone (10) connected to an outlet (9a) of the drying chamber (9), and a bag filter (11) connected to the cyclone (10) and to the steam outlet line (13a).
- The pulse combustion dryer according to any one of claims 1 to 7, wherein the powder separation system comprises a cyclone (10) connected to an outlet (9a) of the drying chamber (9), and a bag filter (11) connected to the cyclone (10) and to the steam outlet line (13a).
- The pulse combustion dryer according to any one of claims 1 to 7, wherein the powder separation system comprises a cyclone (10) connectable to an outlet (9a) of the drying chamber (9) and to the steam outlet line (13a), and a bag filter (11) connectable to the cyclone (10) and to the outlet (9a) of the drying chamber (9) and connected to the steam outlet line (13a).
- The pulse combustion dryer according to any one of the preceding claims, wherein the steam outlet line (13a) comprises a filter, preferably an activated carbon filter, to eliminate volatile organic compounds from the water steam.
Priority Applications (1)
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EP22382065.5A EP4220055A1 (en) | 2022-01-27 | 2022-01-27 | Pulse combustion dryer |
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EP22382065.5A EP4220055A1 (en) | 2022-01-27 | 2022-01-27 | Pulse combustion dryer |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0236152A1 (en) | 1986-01-17 | 1987-09-09 | Aerosol Inventions And Development S.A.A.I.D. S.A. | Sterile packaging of liquid and semi-liquid substances |
EP1092060B1 (en) | 1998-07-01 | 2003-08-20 | Institute of Paper Science and Technology, Inc. | Process for removing water from fibrous web using oscillatory flow-reversing impingement gas |
US20070251120A1 (en) | 2006-04-20 | 2007-11-01 | Connell Larry V | Method of drying and pulverizing organic materials |
US20170307211A1 (en) | 2016-04-22 | 2017-10-26 | Horst Büchner | Method and device for thermal material treatment in a pulsation reactor |
US20170314778A1 (en) | 2016-04-28 | 2017-11-02 | Horst Büchner | Pulsed combustion reactor with pulsating flame, in particular for thermal material treatment or material synthesis |
-
2022
- 2022-01-27 EP EP22382065.5A patent/EP4220055A1/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0236152A1 (en) | 1986-01-17 | 1987-09-09 | Aerosol Inventions And Development S.A.A.I.D. S.A. | Sterile packaging of liquid and semi-liquid substances |
EP1092060B1 (en) | 1998-07-01 | 2003-08-20 | Institute of Paper Science and Technology, Inc. | Process for removing water from fibrous web using oscillatory flow-reversing impingement gas |
US20070251120A1 (en) | 2006-04-20 | 2007-11-01 | Connell Larry V | Method of drying and pulverizing organic materials |
US20170307211A1 (en) | 2016-04-22 | 2017-10-26 | Horst Büchner | Method and device for thermal material treatment in a pulsation reactor |
US20170314778A1 (en) | 2016-04-28 | 2017-11-02 | Horst Büchner | Pulsed combustion reactor with pulsating flame, in particular for thermal material treatment or material synthesis |
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