EP3553071A4 - METHOD FOR PRODUCING PSICOSE USING RECYCLING - Google Patents
METHOD FOR PRODUCING PSICOSE USING RECYCLING Download PDFInfo
- Publication number
- EP3553071A4 EP3553071A4 EP17878321.3A EP17878321A EP3553071A4 EP 3553071 A4 EP3553071 A4 EP 3553071A4 EP 17878321 A EP17878321 A EP 17878321A EP 3553071 A4 EP3553071 A4 EP 3553071A4
- Authority
- EP
- European Patent Office
- Prior art keywords
- recycling
- producing psicose
- psicose
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/02—Monosaccharides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/185—Simulated moving beds characterised by the components to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
- B01D15/361—Ion-exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/24—Preparation of compounds containing saccharide radicals produced by the action of an isomerase, e.g. fructose
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Health & Medical Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Molecular Biology (AREA)
- Analytical Chemistry (AREA)
- Microbiology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Sustainable Development (AREA)
- Crystallography & Structural Chemistry (AREA)
- Saccharide Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Enzymes And Modification Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020160167050A KR102072695B1 (en) | 2016-12-08 | 2016-12-08 | Method of preparing psicose with recycling |
| PCT/KR2017/013368 WO2018105931A1 (en) | 2016-12-08 | 2017-11-22 | Method for preparing psicose using recycling |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP3553071A1 EP3553071A1 (en) | 2019-10-16 |
| EP3553071A4 true EP3553071A4 (en) | 2020-07-29 |
Family
ID=62492292
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP17878321.3A Pending EP3553071A4 (en) | 2016-12-08 | 2017-11-22 | METHOD FOR PRODUCING PSICOSE USING RECYCLING |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US11248015B2 (en) |
| EP (1) | EP3553071A4 (en) |
| JP (2) | JP2019536822A (en) |
| KR (1) | KR102072695B1 (en) |
| CN (1) | CN110036017B (en) |
| TW (1) | TWI719271B (en) |
| WO (1) | WO2018105931A1 (en) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106520863A (en) * | 2016-11-22 | 2017-03-22 | 保龄宝生物股份有限公司 | Production technology for preparing D-psicose through enzymatic transesferification of D-fructose |
| KR102065155B1 (en) * | 2016-12-08 | 2020-02-11 | 주식회사 삼양사 | Production of psciose |
| KR102004941B1 (en) * | 2016-12-08 | 2019-07-29 | 주식회사 삼양사 | Method of producing psicose efficiently |
| CN109432822B (en) * | 2018-11-14 | 2023-09-29 | 内蒙古伊泰煤基新材料研究院有限公司 | Efficient simulated moving bed equipment and efficient simulated moving bed process |
| CN110627847B (en) * | 2019-09-17 | 2023-06-13 | 山东百龙创园生物科技股份有限公司 | Preparation method of psicose crystal |
| US20220380400A1 (en) * | 2019-10-31 | 2022-12-01 | Samyang Corporation | Improved method for manufacturing allulose |
| KR102389709B1 (en) * | 2019-11-29 | 2022-04-22 | 씨제이제일제당 주식회사 | Composition for producing allulose and method of producing allulose using thereof |
| WO2021146134A1 (en) * | 2020-01-13 | 2021-07-22 | Archer Daniels Midland Company | Tertiary separation of allulose from corn syrup using chromatography |
| EP3865499A1 (en) * | 2020-02-12 | 2021-08-18 | Savanna Ingredients GmbH | Allulose concentrates in solid amorphous form |
| US20230159579A1 (en) | 2020-05-27 | 2023-05-25 | Savanna Ingredients Gmbh | Crystallization of allulose under reduced pressure |
| WO2022049307A1 (en) * | 2020-09-07 | 2022-03-10 | Savanna Ingredients Gmbh | Extrusion process for the preparation of a solid allulose composition |
| EP4000419A1 (en) | 2020-11-23 | 2022-05-25 | Savanna Ingredients GmbH | Drying of allulose crystals |
| WO2022239028A1 (en) * | 2021-05-08 | 2022-11-17 | Petiva Private Limited | A method and system for purifying d-allulose, fructose, and/or glucose |
| CN113080357B (en) * | 2021-05-17 | 2023-09-15 | 江苏赛威分离科技有限公司 | Low-calorie compound sweetener and production process thereof |
| CN114031649B (en) * | 2021-07-16 | 2023-03-03 | 山东福洋生物科技股份有限公司 | Method for improving granularity and fluidity of allulose crystals |
| CN113912655B (en) * | 2021-09-30 | 2024-01-23 | 中粮营养健康研究院有限公司 | Method for separating psicose from mixed syrup by using simulated moving bed |
| CN113667707B (en) * | 2021-10-21 | 2022-04-15 | 中粮营养健康研究院有限公司 | Method for producing D-psicose from glucose |
| CN114085768B (en) * | 2021-11-11 | 2023-07-25 | 河南飞天生物科技股份有限公司 | Purification device and purification method for producing psicose |
| CN114868898A (en) * | 2022-03-01 | 2022-08-09 | 新拓洋生物工程有限公司 | Sweetener composition containing psicose and preparation method thereof |
| CN114671919B (en) * | 2022-03-25 | 2023-05-12 | 山东兆光色谱分离技术有限公司 | Method for producing crystalline psicose based on chromatographic separation |
| WO2024047121A1 (en) | 2022-09-01 | 2024-03-07 | Savanna Ingredients Gmbh | Process for the preparation of a particulate allulose composition |
| WO2025153524A1 (en) | 2024-01-16 | 2025-07-24 | Savanna Ingredients Gmbh | Process for the synthesis and purification of allulose |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1834957A1 (en) * | 2004-12-28 | 2007-09-19 | Nippon Beet Sugar Mfg., Co., Ltd. | Process for producing difructose dianhydride iii crystal |
| CN106520863A (en) * | 2016-11-22 | 2017-03-22 | 保龄宝生物股份有限公司 | Production technology for preparing D-psicose through enzymatic transesferification of D-fructose |
| WO2017150766A1 (en) * | 2016-02-29 | 2017-09-08 | Cj Cheiljedang Corporation | Method of producing high purity d-psicose |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2985589A (en) | 1957-05-22 | 1961-05-23 | Universal Oil Prod Co | Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets |
| JP4627841B2 (en) * | 2000-06-08 | 2011-02-09 | 国立大学法人 香川大学 | Psicose separation method |
| UA105206C2 (en) * | 2009-02-25 | 2014-04-25 | Даниско А/С | Method of separating |
| KR101189640B1 (en) * | 2010-03-26 | 2012-10-12 | 씨제이제일제당 (주) | How to Make D-Pycosy Crystals |
| KR101539096B1 (en) | 2012-08-10 | 2015-07-24 | 주식회사 삼양제넥스 | Composition for converting fructose into psicose, and method for producing psicose using the same |
| KR20140054997A (en) | 2012-10-30 | 2014-05-09 | 현대모비스 주식회사 | Apparatus for locking glove box of vehicle |
| KR20140080282A (en) | 2012-12-20 | 2014-06-30 | 주식회사 삼양제넥스 | Method for preparing psicose from fructose by using D-psicose 3-epimerase |
| KR101318422B1 (en) | 2013-04-09 | 2013-10-15 | 주식회사 삼양제넥스 | D-psicose epimerase and method for producing psicose using the same |
| KR101455624B1 (en) | 2013-04-12 | 2014-10-28 | 주식회사한국야쿠르트 | Novel D-psicose-3-epimerase from Clostridium bolteae having production of functional rare sugar D-psicose and production method of D-psicose using thereof |
| HUE046414T2 (en) * | 2013-06-05 | 2020-02-28 | Cj Cheiljedang Corp | Process for the production of tagatose |
| KR20160024193A (en) | 2014-08-25 | 2016-03-04 | 한국건설기술연구원 | X-ray Scan Method of Micro Cell Material using Saturation of Tracer |
| KR101749527B1 (en) * | 2014-10-20 | 2017-06-21 | 씨제이제일제당(주) | A method of manufacturing a d-psicose crystal |
| KR20160062349A (en) * | 2014-11-25 | 2016-06-02 | 씨제이제일제당 (주) | A method of manufacturing high purity d-psicose |
| CN104447888B (en) * | 2014-12-04 | 2017-08-01 | 青岛蜜福堂健康科技有限公司 | A kind of preparation method and applications of psicose |
-
2016
- 2016-12-08 KR KR1020160167050A patent/KR102072695B1/en active Active
-
2017
- 2017-11-22 EP EP17878321.3A patent/EP3553071A4/en active Pending
- 2017-11-22 US US16/463,986 patent/US11248015B2/en active Active
- 2017-11-22 WO PCT/KR2017/013368 patent/WO2018105931A1/en not_active Ceased
- 2017-11-22 CN CN201780075218.5A patent/CN110036017B/en active Active
- 2017-11-22 JP JP2019550529A patent/JP2019536822A/en active Pending
- 2017-11-29 TW TW106141518A patent/TWI719271B/en active
-
2021
- 2021-02-19 JP JP2021025295A patent/JP7148656B2/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1834957A1 (en) * | 2004-12-28 | 2007-09-19 | Nippon Beet Sugar Mfg., Co., Ltd. | Process for producing difructose dianhydride iii crystal |
| WO2017150766A1 (en) * | 2016-02-29 | 2017-09-08 | Cj Cheiljedang Corporation | Method of producing high purity d-psicose |
| CN106520863A (en) * | 2016-11-22 | 2017-03-22 | 保龄宝生物股份有限公司 | Production technology for preparing D-psicose through enzymatic transesferification of D-fructose |
Non-Patent Citations (1)
| Title |
|---|
| See also references of WO2018105931A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| JP7148656B2 (en) | 2022-10-05 |
| WO2018105931A1 (en) | 2018-06-14 |
| CN110036017A (en) | 2019-07-19 |
| KR20180065784A (en) | 2018-06-18 |
| CN110036017B (en) | 2022-08-26 |
| US20200385415A1 (en) | 2020-12-10 |
| JP2021080275A (en) | 2021-05-27 |
| TWI719271B (en) | 2021-02-21 |
| JP2019536822A (en) | 2019-12-19 |
| KR102072695B1 (en) | 2020-03-02 |
| TW201835335A (en) | 2018-10-01 |
| EP3553071A1 (en) | 2019-10-16 |
| US11248015B2 (en) | 2022-02-15 |
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Legal Events
| Date | Code | Title | Description |
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| STAA | Information on the status of an ep patent application or granted ep patent |
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| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
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Effective date: 20190708 |
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| A4 | Supplementary search report drawn up and despatched |
Effective date: 20200630 |
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| RIC1 | Information provided on ipc code assigned before grant |
Ipc: B01D 15/36 20060101ALI20200624BHEP Ipc: C07H 1/06 20060101ALI20200624BHEP Ipc: C07H 3/02 20060101AFI20200624BHEP Ipc: C12P 19/02 20060101ALI20200624BHEP Ipc: B01D 15/18 20060101ALI20200624BHEP |
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