EP3553071A4 - METHOD FOR PRODUCING PSICOSE USING RECYCLING - Google Patents

METHOD FOR PRODUCING PSICOSE USING RECYCLING Download PDF

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Publication number
EP3553071A4
EP3553071A4 EP17878321.3A EP17878321A EP3553071A4 EP 3553071 A4 EP3553071 A4 EP 3553071A4 EP 17878321 A EP17878321 A EP 17878321A EP 3553071 A4 EP3553071 A4 EP 3553071A4
Authority
EP
European Patent Office
Prior art keywords
recycling
producing psicose
psicose
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP17878321.3A
Other languages
German (de)
French (fr)
Other versions
EP3553071A1 (en
EP3553071B1 (en
Inventor
Ji Won Park
Sung Won Park
Chong Jin Park
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Samyang Corp
Original Assignee
Samyang Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Samyang Corp filed Critical Samyang Corp
Publication of EP3553071A1 publication Critical patent/EP3553071A1/en
Publication of EP3553071A4 publication Critical patent/EP3553071A4/en
Application granted granted Critical
Publication of EP3553071B1 publication Critical patent/EP3553071B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/02—Monosaccharides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterised by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361—Ion-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/02—Monosaccharides
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/24—Preparation of compounds containing saccharide radicals produced by the action of an isomerase, e.g. fructose
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D2009/0086—Processes or apparatus therefor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Analytical Chemistry (AREA)
  • Molecular Biology (AREA)
  • Microbiology (AREA)
  • General Engineering & Computer Science (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sustainable Development (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Enzymes And Modification Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
EP17878321.3A 2016-12-08 2017-11-22 Method for preparing psicose using recycling Active EP3553071B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020160167050A KR102072695B1 (en) 2016-12-08 2016-12-08 Method of preparing psicose with recycling
PCT/KR2017/013368 WO2018105931A1 (en) 2016-12-08 2017-11-22 Method for preparing psicose using recycling

Publications (3)

Publication Number Publication Date
EP3553071A1 EP3553071A1 (en) 2019-10-16
EP3553071A4 true EP3553071A4 (en) 2020-07-29
EP3553071B1 EP3553071B1 (en) 2026-01-07

Family

ID=62492292

Family Applications (1)

Application Number Title Priority Date Filing Date
EP17878321.3A Active EP3553071B1 (en) 2016-12-08 2017-11-22 Method for preparing psicose using recycling

Country Status (7)

Country Link
US (1) US11248015B2 (en)
EP (1) EP3553071B1 (en)
JP (2) JP2019536822A (en)
KR (1) KR102072695B1 (en)
CN (1) CN110036017B (en)
TW (1) TWI719271B (en)
WO (1) WO2018105931A1 (en)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106520863A (en) * 2016-11-22 2017-03-22 保龄宝生物股份有限公司 Production technology for preparing D-psicose through enzymatic transesferification of D-fructose
KR102004941B1 (en) * 2016-12-08 2019-07-29 주식회사 삼양사 Method of producing psicose efficiently
KR102065155B1 (en) * 2016-12-08 2020-02-11 주식회사 삼양사 Production of psciose
CN109432822B (en) * 2018-11-14 2023-09-29 内蒙古伊泰煤基新材料研究院有限公司 Efficient simulated moving bed equipment and efficient simulated moving bed process
CN110627847B (en) * 2019-09-17 2023-06-13 山东百龙创园生物科技股份有限公司 Preparation method of psicose crystal
WO2021086086A1 (en) * 2019-10-31 2021-05-06 주식회사 삼양사 Improved method for manufacturing allulose
KR102389709B1 (en) * 2019-11-29 2022-04-22 씨제이제일제당 주식회사 Composition for producing allulose and method of producing allulose using thereof
EP4090170A4 (en) * 2020-01-13 2024-02-14 Archer Daniels Midland Company TERTIARY SEPARATION OF ALLULOSE FROM CORN SYRUP USING CHROMATOGRAPHY
EP3865499A1 (en) * 2020-02-12 2021-08-18 Savanna Ingredients GmbH Allulose concentrates in solid amorphous form
MX2022014802A (en) 2020-05-27 2023-01-16 Savanna Ingredients Gmbh Crystallization of allulose under reduced pressure.
WO2022049307A1 (en) 2020-09-07 2022-03-10 Savanna Ingredients Gmbh Extrusion process for the preparation of a solid allulose composition
EP4000419A1 (en) 2020-11-23 2022-05-25 Savanna Ingredients GmbH Drying of allulose crystals
WO2022239028A1 (en) * 2021-05-08 2022-11-17 Petiva Private Limited A method and system for purifying d-allulose, fructose, and/or glucose
CN113080357B (en) * 2021-05-17 2023-09-15 江苏赛威分离科技有限公司 Low-calorie compound sweetener and production process thereof
CN114031649B (en) * 2021-07-16 2023-03-03 山东福洋生物科技股份有限公司 Method for improving granularity and fluidity of allulose crystals
CN113912655B (en) * 2021-09-30 2024-01-23 中粮营养健康研究院有限公司 Method for separating psicose from mixed syrup by using simulated moving bed
CN113667707B (en) * 2021-10-21 2022-04-15 中粮营养健康研究院有限公司 Method for producing D-psicose from glucose
CN114085768B (en) * 2021-11-11 2023-07-25 河南飞天生物科技股份有限公司 Purification device and purification method for producing psicose
CN114868898A (en) * 2022-03-01 2022-08-09 新拓洋生物工程有限公司 Sweetener composition containing psicose and preparation method thereof
CN114671919B (en) * 2022-03-25 2023-05-12 山东兆光色谱分离技术有限公司 Method for producing crystalline psicose based on chromatographic separation
WO2024047122A1 (en) 2022-09-01 2024-03-07 Savanna Ingredients Gmbh Process for the preparation of a particulate allulose composition
WO2025153524A1 (en) 2024-01-16 2025-07-24 Savanna Ingredients Gmbh Process for the synthesis and purification of allulose

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1834957A1 (en) * 2004-12-28 2007-09-19 Nippon Beet Sugar Mfg., Co., Ltd. Process for producing difructose dianhydride iii crystal
CN106520863A (en) * 2016-11-22 2017-03-22 保龄宝生物股份有限公司 Production technology for preparing D-psicose through enzymatic transesferification of D-fructose
WO2017150766A1 (en) * 2016-02-29 2017-09-08 Cj Cheiljedang Corporation Method of producing high purity d-psicose

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2985589A (en) 1957-05-22 1961-05-23 Universal Oil Prod Co Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets
JP4627841B2 (en) 2000-06-08 2011-02-09 国立大学法人 香川大学 Psicose separation method
CN102413890B (en) 2009-02-25 2014-06-04 杜邦营养生物科学有限公司 Separation process
KR101189640B1 (en) * 2010-03-26 2012-10-12 씨제이제일제당 (주) How to Make D-Pycosy Crystals
KR101539096B1 (en) 2012-08-10 2015-07-24 주식회사 삼양제넥스 Composition for converting fructose into psicose, and method for producing psicose using the same
KR20140054997A (en) 2012-10-30 2014-05-09 현대모비스 주식회사 Apparatus for locking glove box of vehicle
KR20140080282A (en) 2012-12-20 2014-06-30 주식회사 삼양제넥스 Method for preparing psicose from fructose by using D-psicose 3-epimerase
KR101318422B1 (en) 2013-04-09 2013-10-15 주식회사 삼양제넥스 D-psicose epimerase and method for producing psicose using the same
KR101455624B1 (en) * 2013-04-12 2014-10-28 주식회사한국야쿠르트 Novel D-psicose-3-epimerase from Clostridium bolteae having production of functional rare sugar D-psicose and production method of D-psicose using thereof
JP6171094B2 (en) 2013-06-05 2017-07-26 シージェイ チェイルジェダン コーポレーションＣｊ Ｃｈｅｉｌｊｅｄａｎｇ Ｃｏｒｐｏｒａｔｉｏｎ Tagatose manufacturing method
KR20160024193A (en) 2014-08-25 2016-03-04 한국건설기술연구원 X-ray Scan Method of Micro Cell Material using Saturation of Tracer
KR101749527B1 (en) 2014-10-20 2017-06-21 씨제이제일제당(주) A method of manufacturing a d-psicose crystal
KR20160062349A (en) * 2014-11-25 2016-06-02 씨제이제일제당 (주) A method of manufacturing high purity d-psicose
CN104447888B (en) * 2014-12-04 2017-08-01 青岛蜜福堂健康科技有限公司 A kind of preparation method and applications of psicose

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1834957A1 (en) * 2004-12-28 2007-09-19 Nippon Beet Sugar Mfg., Co., Ltd. Process for producing difructose dianhydride iii crystal
WO2017150766A1 (en) * 2016-02-29 2017-09-08 Cj Cheiljedang Corporation Method of producing high purity d-psicose
CN106520863A (en) * 2016-11-22 2017-03-22 保龄宝生物股份有限公司 Production technology for preparing D-psicose through enzymatic transesferification of D-fructose

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO2018105931A1 *

Also Published As

Publication number Publication date
KR20180065784A (en) 2018-06-18
WO2018105931A1 (en) 2018-06-14
JP7148656B2 (en) 2022-10-05
JP2021080275A (en) 2021-05-27
EP3553071A1 (en) 2019-10-16
US11248015B2 (en) 2022-02-15
JP2019536822A (en) 2019-12-19
US20200385415A1 (en) 2020-12-10
TW201835335A (en) 2018-10-01
CN110036017B (en) 2022-08-26
EP3553071B1 (en) 2026-01-07
TWI719271B (en) 2021-02-21
KR102072695B1 (en) 2020-03-02
CN110036017A (en) 2019-07-19

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