EP3516031A1 - Solid particulate compositions comprising water-soluble carrier polymer and perfume - Google Patents
Solid particulate compositions comprising water-soluble carrier polymer and perfumeInfo
- Publication number
- EP3516031A1 EP3516031A1 EP17776991.6A EP17776991A EP3516031A1 EP 3516031 A1 EP3516031 A1 EP 3516031A1 EP 17776991 A EP17776991 A EP 17776991A EP 3516031 A1 EP3516031 A1 EP 3516031A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- composition
- water
- oil
- perfume
- composition according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 140
- 229920000642 polymer Polymers 0.000 title claims abstract description 46
- 239000007787 solid Substances 0.000 title claims abstract description 23
- 239000002304 perfume Substances 0.000 title claims description 45
- 239000004753 textile Substances 0.000 claims abstract description 26
- 238000005406 washing Methods 0.000 claims abstract description 23
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 18
- 238000004140 cleaning Methods 0.000 claims abstract description 11
- 239000008247 solid mixture Substances 0.000 claims abstract description 11
- 239000003921 oil Substances 0.000 claims description 40
- 150000001875 compounds Chemical class 0.000 claims description 36
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 34
- -1 alkaline earth metal salts Chemical class 0.000 claims description 32
- 229910052615 phyllosilicate Inorganic materials 0.000 claims description 22
- 229920001223 polyethylene glycol Polymers 0.000 claims description 22
- 229920001282 polysaccharide Polymers 0.000 claims description 22
- 239000005017 polysaccharide Substances 0.000 claims description 22
- 150000004804 polysaccharides Chemical class 0.000 claims description 22
- 239000004744 fabric Substances 0.000 claims description 21
- 239000000155 melt Substances 0.000 claims description 21
- 239000003795 chemical substances by application Substances 0.000 claims description 17
- 239000002202 Polyethylene glycol Substances 0.000 claims description 16
- 229920002472 Starch Polymers 0.000 claims description 16
- 235000019698 starch Nutrition 0.000 claims description 16
- 238000002844 melting Methods 0.000 claims description 15
- 230000008018 melting Effects 0.000 claims description 15
- 239000008107 starch Substances 0.000 claims description 14
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 13
- 229920001515 polyalkylene glycol Polymers 0.000 claims description 12
- 239000000377 silicon dioxide Substances 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 11
- 235000012216 bentonite Nutrition 0.000 claims description 10
- 125000003545 alkoxy group Chemical group 0.000 claims description 9
- 229910021485 fumed silica Inorganic materials 0.000 claims description 8
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 8
- 229920001400 block copolymer Polymers 0.000 claims description 6
- 229920002678 cellulose Polymers 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000002775 capsule Substances 0.000 claims description 5
- 239000004927 clay Substances 0.000 claims description 5
- 230000003750 conditioning effect Effects 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000003112 inhibitor Substances 0.000 claims description 5
- 239000011777 magnesium Substances 0.000 claims description 5
- 229920001661 Chitosan Polymers 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
- 229940045110 chitosan Drugs 0.000 claims description 4
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 claims description 4
- 229910000271 hectorite Inorganic materials 0.000 claims description 4
- 229910000275 saponite Inorganic materials 0.000 claims description 4
- 229920002545 silicone oil Polymers 0.000 claims description 4
- 238000012546 transfer Methods 0.000 claims description 4
- GJCOSYZMQJWQCA-UHFFFAOYSA-N 9H-xanthene Chemical compound C1=CC=C2CC3=CC=CC=C3OC2=C1 GJCOSYZMQJWQCA-UHFFFAOYSA-N 0.000 claims description 3
- 244000215068 Acacia senegal Species 0.000 claims description 3
- 229920001817 Agar Polymers 0.000 claims description 3
- 241000416162 Astragalus gummifer Species 0.000 claims description 3
- 229920000018 Callose Polymers 0.000 claims description 3
- 229920002101 Chitin Polymers 0.000 claims description 3
- 229920002307 Dextran Polymers 0.000 claims description 3
- 229920002148 Gellan gum Polymers 0.000 claims description 3
- 229920002527 Glycogen Polymers 0.000 claims description 3
- 229920000084 Gum arabic Polymers 0.000 claims description 3
- 229920000569 Gum karaya Polymers 0.000 claims description 3
- HTTJABKRGRZYRN-UHFFFAOYSA-N Heparin Chemical compound OC1C(NC(=O)C)C(O)OC(COS(O)(=O)=O)C1OC1C(OS(O)(=O)=O)C(O)C(OC2C(C(OS(O)(=O)=O)C(OC3C(C(O)C(O)C(O3)C(O)=O)OS(O)(=O)=O)C(CO)O2)NS(O)(=O)=O)C(C(O)=O)O1 HTTJABKRGRZYRN-UHFFFAOYSA-N 0.000 claims description 3
- 229920001202 Inulin Polymers 0.000 claims description 3
- 229920000161 Locust bean gum Polymers 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 3
- 241000934878 Sterculia Species 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 3
- 229920001615 Tragacanth Polymers 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 239000000205 acacia gum Substances 0.000 claims description 3
- 239000004480 active ingredient Substances 0.000 claims description 3
- 239000008272 agar Substances 0.000 claims description 3
- 229940023476 agar Drugs 0.000 claims description 3
- 235000010419 agar Nutrition 0.000 claims description 3
- 229920000615 alginic acid Polymers 0.000 claims description 3
- 235000010443 alginic acid Nutrition 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 235000010418 carrageenan Nutrition 0.000 claims description 3
- 229920001525 carrageenan Polymers 0.000 claims description 3
- 239000000679 carrageenan Substances 0.000 claims description 3
- 229940113118 carrageenan Drugs 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 239000001913 cellulose Substances 0.000 claims description 3
- 150000002191 fatty alcohols Chemical class 0.000 claims description 3
- 229940096919 glycogen Drugs 0.000 claims description 3
- 150000004820 halides Chemical class 0.000 claims description 3
- 229920000669 heparin Polymers 0.000 claims description 3
- 229960002897 heparin Drugs 0.000 claims description 3
- 229940029339 inulin Drugs 0.000 claims description 3
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims description 3
- FZWBNHMXJMCXLU-BLAUPYHCSA-N isomaltotriose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)O1 FZWBNHMXJMCXLU-BLAUPYHCSA-N 0.000 claims description 3
- 235000010494 karaya gum Nutrition 0.000 claims description 3
- 239000000231 karaya gum Substances 0.000 claims description 3
- 229940039371 karaya gum Drugs 0.000 claims description 3
- 235000010420 locust bean gum Nutrition 0.000 claims description 3
- 239000000711 locust bean gum Substances 0.000 claims description 3
- NEMFQSKAPLGFIP-UHFFFAOYSA-N magnesiosodium Chemical compound [Na].[Mg] NEMFQSKAPLGFIP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052749 magnesium Inorganic materials 0.000 claims description 3
- 229920001277 pectin Polymers 0.000 claims description 3
- 235000010987 pectin Nutrition 0.000 claims description 3
- 239000001814 pectin Substances 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- 235000010487 tragacanth Nutrition 0.000 claims description 3
- 239000000196 tragacanth Substances 0.000 claims description 3
- 229940116362 tragacanth Drugs 0.000 claims description 3
- 229920001285 xanthan gum Polymers 0.000 claims description 3
- 229920001221 xylan Polymers 0.000 claims description 3
- 150000004823 xylans Chemical class 0.000 claims description 3
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 3
- 229920002907 Guar gum Polymers 0.000 claims description 2
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 2
- 239000006096 absorbing agent Substances 0.000 claims description 2
- 239000000420 anogeissus latifolia wall. gum Substances 0.000 claims description 2
- 239000012753 anti-shrinkage agent Substances 0.000 claims description 2
- 239000004599 antimicrobial Substances 0.000 claims description 2
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- 239000002216 antistatic agent Substances 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 239000000417 fungicide Substances 0.000 claims description 2
- 230000002070 germicidal effect Effects 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- 229920000591 gum Polymers 0.000 claims description 2
- 235000019314 gum ghatti Nutrition 0.000 claims description 2
- 238000010409 ironing Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 230000003287 optical effect Effects 0.000 claims description 2
- 235000021317 phosphate Nutrition 0.000 claims description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 235000017550 sodium carbonate Nutrition 0.000 claims description 2
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 2
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 230000008961 swelling Effects 0.000 claims description 2
- 239000005871 repellent Substances 0.000 claims 1
- 230000002940 repellent Effects 0.000 claims 1
- 239000012748 slip agent Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 32
- 239000012459 cleaning agent Substances 0.000 abstract description 15
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 235000019198 oils Nutrition 0.000 description 39
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 15
- 239000004615 ingredient Substances 0.000 description 15
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 14
- 239000000047 product Substances 0.000 description 13
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 13
- 150000004760 silicates Chemical class 0.000 description 13
- 229910001868 water Inorganic materials 0.000 description 13
- 210000003298 dental enamel Anatomy 0.000 description 12
- 229920001577 copolymer Polymers 0.000 description 11
- 239000003599 detergent Substances 0.000 description 11
- 229920001296 polysiloxane Polymers 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- 238000009472 formulation Methods 0.000 description 9
- 229910052739 hydrogen Chemical group 0.000 description 8
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 description 8
- 239000003094 microcapsule Substances 0.000 description 7
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 6
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 6
- 239000002979 fabric softener Substances 0.000 description 6
- 229940094522 laponite Drugs 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- XCOBTUNSZUJCDH-UHFFFAOYSA-B lithium magnesium sodium silicate Chemical compound [Li+].[Li+].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Na+].[Na+].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3 XCOBTUNSZUJCDH-UHFFFAOYSA-B 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- YGFGZTXGYTUXBA-UHFFFAOYSA-N (±)-2,6-dimethyl-5-heptenal Chemical compound O=CC(C)CCC=C(C)C YGFGZTXGYTUXBA-UHFFFAOYSA-N 0.000 description 5
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 5
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 5
- 125000002091 cationic group Chemical group 0.000 description 5
- 239000002734 clay mineral Substances 0.000 description 5
- HFJRKMMYBMWEAD-UHFFFAOYSA-N dodecanal Chemical compound CCCCCCCCCCCC=O HFJRKMMYBMWEAD-UHFFFAOYSA-N 0.000 description 5
- 239000000975 dye Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
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- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 description 4
- NFAVNWJJYQAGNB-UHFFFAOYSA-N 2-methylundecanal Chemical compound CCCCCCCCCC(C)C=O NFAVNWJJYQAGNB-UHFFFAOYSA-N 0.000 description 4
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 4
- NTPLXRHDUXRPNE-UHFFFAOYSA-N 4-methoxyacetophenone Chemical compound COC1=CC=C(C(C)=O)C=C1 NTPLXRHDUXRPNE-UHFFFAOYSA-N 0.000 description 4
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 4
- ZCTQGTTXIYCGGC-UHFFFAOYSA-N Benzyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OCC1=CC=CC=C1 ZCTQGTTXIYCGGC-UHFFFAOYSA-N 0.000 description 4
- 229920005682 EO-PO block copolymer Polymers 0.000 description 4
- LHXDLQBQYFFVNW-UHFFFAOYSA-N Fenchone Chemical compound C1CC2(C)C(=O)C(C)(C)C1C2 LHXDLQBQYFFVNW-UHFFFAOYSA-N 0.000 description 4
- 240000003183 Manihot esculenta Species 0.000 description 4
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
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- 229910000278 bentonite Inorganic materials 0.000 description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 4
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 4
- AKGGYBADQZYZPD-UHFFFAOYSA-N benzylacetone Chemical compound CC(=O)CCC1=CC=CC=C1 AKGGYBADQZYZPD-UHFFFAOYSA-N 0.000 description 4
- ULDHMXUKGWMISQ-UHFFFAOYSA-N carvone Chemical compound CC(=C)C1CC=C(C)C(=O)C1 ULDHMXUKGWMISQ-UHFFFAOYSA-N 0.000 description 4
- 239000000470 constituent Substances 0.000 description 4
- GQOKIYDTHHZSCJ-UHFFFAOYSA-M dimethyl-bis(prop-2-enyl)azanium;chloride Chemical compound [Cl-].C=CC[N+](C)(C)CC=C GQOKIYDTHHZSCJ-UHFFFAOYSA-M 0.000 description 4
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 description 4
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 4
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 4
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 description 4
- VAMXMNNIEUEQDV-UHFFFAOYSA-N methyl anthranilate Chemical compound COC(=O)C1=CC=CC=C1N VAMXMNNIEUEQDV-UHFFFAOYSA-N 0.000 description 4
- ZWRUINPWMLAQRD-UHFFFAOYSA-N nonan-1-ol Chemical compound CCCCCCCCCO ZWRUINPWMLAQRD-UHFFFAOYSA-N 0.000 description 4
- 235000010603 pastilles Nutrition 0.000 description 4
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 description 4
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- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000012243 magnesium silicates Nutrition 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 1
- 239000001683 mentha spicata herb oil Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 1
- UNSKAUSCLTVFGO-KCDKBNATSA-N methyl (2s,3r,4s,5r)-2,3,4,5-tetrahydroxy-6-oxohexanoate Chemical compound COC(=O)[C@@H](O)[C@H](O)[C@H](O)[C@@H](O)C=O UNSKAUSCLTVFGO-KCDKBNATSA-N 0.000 description 1
- 229940102396 methyl bromide Drugs 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 description 1
- 229960001047 methyl salicylate Drugs 0.000 description 1
- SBENKNZHVXGNTP-UHFFFAOYSA-N methylconiferyl ether Natural products COCC=CC1=CC=C(O)C(OC)=C1 SBENKNZHVXGNTP-UHFFFAOYSA-N 0.000 description 1
- 229920003087 methylethyl cellulose Polymers 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- ALHUZKCOMYUFRB-UHFFFAOYSA-N muskone Natural products CC1CCCCCCCCCCCCC(=O)C1 ALHUZKCOMYUFRB-UHFFFAOYSA-N 0.000 description 1
- 229940078812 myristyl myristate Drugs 0.000 description 1
- YWFWDNVOPHGWMX-UHFFFAOYSA-N n,n-dimethyldodecan-1-amine Chemical group CCCCCCCCCCCCN(C)C YWFWDNVOPHGWMX-UHFFFAOYSA-N 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 229910021527 natrosilite Inorganic materials 0.000 description 1
- ZYTMANIQRDEHIO-UHFFFAOYSA-N neo-Isopulegol Natural products CC1CCC(C(C)=C)C(O)C1 ZYTMANIQRDEHIO-UHFFFAOYSA-N 0.000 description 1
- 235000019720 niaouli oil Nutrition 0.000 description 1
- XJHRZBIBSSVCEL-UHFFFAOYSA-N non-6-en-1-ol Chemical compound CCC=CCCCCCO XJHRZBIBSSVCEL-UHFFFAOYSA-N 0.000 description 1
- 229910000273 nontronite Inorganic materials 0.000 description 1
- 239000010466 nut oil Substances 0.000 description 1
- KKVZAVRSVHUSPL-UHFFFAOYSA-N o-methoxycinnamic aldehyde Natural products COC1=CC=CC=C1C=CC=O KKVZAVRSVHUSPL-UHFFFAOYSA-N 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- HEKJOMVJRYMUDB-UHFFFAOYSA-N octahydro-6-isopropyl-2(1h)-naphthalenone Chemical compound C1C(=O)CCC2CC(C(C)C)CCC21 HEKJOMVJRYMUDB-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 229940055577 oleyl alcohol Drugs 0.000 description 1
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 150000002924 oxiranes Chemical class 0.000 description 1
- 229930007459 p-menth-8-en-3-one Natural products 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- RUVINXPYWBROJD-UHFFFAOYSA-N para-methoxyphenyl Natural products COC1=CC=C(C=CC)C=C1 RUVINXPYWBROJD-UHFFFAOYSA-N 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- LVECZGHBXXYWBO-UHFFFAOYSA-N pentadecanolide Natural products CC1CCCCCCCCCCCCC(=O)O1 LVECZGHBXXYWBO-UHFFFAOYSA-N 0.000 description 1
- 125000002255 pentenyl group Chemical group C(=CCCC)* 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 229960003742 phenol Drugs 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- 229960000969 phenyl salicylate Drugs 0.000 description 1
- 229940067107 phenylethyl alcohol Drugs 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000001738 pogostemon cablin oil Substances 0.000 description 1
- 229920002553 poly(2-methacrylolyloxyethyltrimethylammonium chloride) polymer Polymers 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- ODGAOXROABLFNM-UHFFFAOYSA-N polynoxylin Chemical compound O=C.NC(N)=O ODGAOXROABLFNM-UHFFFAOYSA-N 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 239000010491 poppyseed oil Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000001944 prunus armeniaca kernel oil Substances 0.000 description 1
- 239000008171 pumpkin seed oil Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 235000019719 rose oil Nutrition 0.000 description 1
- 239000010666 rose oil Substances 0.000 description 1
- 239000010668 rosemary oil Substances 0.000 description 1
- 229940058206 rosemary oil Drugs 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000010670 sage oil Substances 0.000 description 1
- 239000010671 sandalwood oil Substances 0.000 description 1
- 229910000276 sauconite Inorganic materials 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 230000008786 sensory perception of smell Effects 0.000 description 1
- 229910052616 serpentine group Inorganic materials 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 1
- 229940074386 skatole Drugs 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000012217 sodium aluminium silicate Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000013042 solid detergent Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000019721 spearmint oil Nutrition 0.000 description 1
- 239000012177 spermaceti Substances 0.000 description 1
- 229940084106 spermaceti Drugs 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 229940012831 stearyl alcohol Drugs 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- QJVXKWHHAMZTBY-GCPOEHJPSA-N syringin Chemical compound COC1=CC(\C=C\CO)=CC(OC)=C1O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 QJVXKWHHAMZTBY-GCPOEHJPSA-N 0.000 description 1
- 235000010491 tara gum Nutrition 0.000 description 1
- 239000000213 tara gum Substances 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- BORJONZPSTVSFP-UHFFFAOYSA-N tetradecyl 2-hydroxypropanoate Chemical compound CCCCCCCCCCCCCCOC(=O)C(C)O BORJONZPSTVSFP-UHFFFAOYSA-N 0.000 description 1
- DZKXJUASMGQEMA-UHFFFAOYSA-N tetradecyl tetradecanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCC DZKXJUASMGQEMA-UHFFFAOYSA-N 0.000 description 1
- 239000010678 thyme oil Substances 0.000 description 1
- MBDOYVRWFFCFHM-UHFFFAOYSA-N trans-2-hexenal Natural products CCCC=CC=O MBDOYVRWFFCFHM-UHFFFAOYSA-N 0.000 description 1
- DKZBBWMURDFHNE-UHFFFAOYSA-N trans-coniferylaldehyde Natural products COC1=CC(C=CC=O)=CC=C1O DKZBBWMURDFHNE-UHFFFAOYSA-N 0.000 description 1
- NSSALFVIQPAIQK-UHFFFAOYSA-N trans-non-2-en-1-ol Natural products CCCCCCC=CCO NSSALFVIQPAIQK-UHFFFAOYSA-N 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- USFMMZYROHDWPJ-UHFFFAOYSA-N trimethyl-[2-(2-methylprop-2-enoyloxy)ethyl]azanium Chemical compound CC(=C)C(=O)OCC[N+](C)(C)C USFMMZYROHDWPJ-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- WJUFSDZVCOTFON-UHFFFAOYSA-N veratraldehyde Chemical compound COC1=CC=C(C=O)C=C1OC WJUFSDZVCOTFON-UHFFFAOYSA-N 0.000 description 1
- 235000020047 vermouth Nutrition 0.000 description 1
- 239000010679 vetiver oil Substances 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
- 239000009637 wintergreen oil Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- OJYLAHXKWMRDGS-UHFFFAOYSA-N zingerone Chemical compound COC1=CC(CCC(C)=O)=CC=C1O OJYLAHXKWMRDGS-UHFFFAOYSA-N 0.000 description 1
- 229930007850 β-damascenone Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/1273—Crystalline layered silicates of type NaMeSixO2x+1YH2O
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
Definitions
- the present invention relates to a solid, particulate composition
- a solid, particulate composition comprising at least one water-soluble or water-dispersible carrier polymer, at least one perfume and from 1, 1 to 40.0 wt .-% phyllosilicate.
- the invention relates to processes for the preparation of the solid composition, as well as a detergent or cleaning agent containing the solid
- composition contains. Moreover, the present invention also relates to the use of such a washing or cleaning agent for cleaning textiles or hard surfaces and corresponding methods for cleaning textiles or hard surfaces using such a washing or cleaning agent. The invention also relates to solid, particulate compositions which have been prepared by the process according to the invention.
- the consumer In the use of detergents and cleaners, the consumer not only aims to wash, cleanse or care for the objects to be treated, but also desires that the treated objects, e.g. Textiles, after the treatment, for example after the wash, smell pleasant. For this reason in particular, most commercially available detergents and cleaners contain fragrances.
- fragrances are used in the form of perfume particles either as an integral part of a washing or cleaning agent, or dosed directly into the washing drum at the beginning of a wash cycle in a separate form. In this way, the consumer can control the fragrance of the laundry to be washed by individual dosage. By replacing the wash liquor several times in the course of a wash cycle, however, the majority of the metered perfume particles is dissolved, even before the last rinse, whereby only an insufficient scenting of the washed laundry can be achieved.
- compositions which, in the case of objects to be treated, preferably textiles, enable improved scenting of the object, with the scent intensity as well as the sense of freshness over a long period of time being to be perceived as pleasant.
- fragrance compositions are already known in the art. They are usually prepared as a melt and then dropped by means of a nozzle on a cooling belt, where they should solidify as quickly as possible and take a nice geometric figure. With conventional products, it is frequently observed that their melt, after being dropped on the cooling belt, runs off into unsightly particles with a small layer thickness. Thus, it is problematic to produce uniform products, let alone for the consumer visually appealing products.
- lozenges having a height / diameter ratio of 0.5, since this example, a
- melt products have the disadvantage that they can break during transport and storage or that caused by breaking the thin edges much unwanted abrasion.
- a solid, particulate composition comprising at least one water-soluble or water-dispersible carrier polymer having a
- the inventors of the present invention have surprisingly found that the incorporation of 1, 1 to 40.0 wt .-% phyllosilicate can eliminate the problems described above.
- the composition gives an aesthetic and abrasion-resistant product.
- washing process improved.
- the inventors have found that the washed textiles not only smoother, but are also softer than textiles washed with comparable detergents. Without wishing to be bound by theory, this could be due to a prolonged release of the phyllosilicate, which surprisingly is achieved by incorporation into the solid, particulate composition.
- the present invention is directed to the use of the solid composition as described herein as a fabric care, preferably fragrance and / or fabric softener, conditioner and / or conditioner for fabrics.
- the present invention is further directed to a laundry or cleaning composition comprising a solid composition as described herein and a method of making the compositions of the invention.
- compositions of the invention are also hereby disclosed for the other aspects of the invention.
- At least one refers to 1 or more, for example, 1, 2, 3, 4, 5, 6, 7, 8, 9 or more, more particularly, this indication refers to the type of agent / compound and not the absolute number of molecules. "At least one perfume”, therefore, means that at least one type of perfume is detected but may also contain 2 or more different types of perfume.
- a first object of the present invention is a solid, particulate composition
- a solid, particulate composition comprising at least one water-soluble or water-dispersible carrier polymer having a Melting point> 30 ° C to 250 ° C, preferably> 40 ° C to 150 ° C, preferably selected from polyalkylene glycols, more preferably polyethylene glycol, and at least one perfume, characterized in that the composition 1, 1 to 40.0 wt. % Phyllosilicate.
- at least one inorganic salt is further included.
- layered silicate refers to silicates whose silicate anions consist of layers of corner-sharing SiC tetrahedra, which layers are not linked to each other by further Si-O bonds to form scaffolds to avoid misunderstanding, zeolites not covered by the term layered silicate
- Phyllosilicates include important groups of rock-forming minerals such.
- the technically important and in sedimentary rocks widespread clay minerals are also phyllosilicates.
- Phyllosilicate preferably the clay mineral, is present in an amount of from 1.1% to 40.0% by weight, preferably from 1.5 to 38% by weight, more preferably from 5 to 35% by weight. %, more preferably from 15 to 30 wt .-%, in particular from 18 to 22 wt .-% in each case based on the total solid composition.
- composition may comprise a layered silicate or a mixture of multiple layered silicates, as long as the limits described herein are not exceeded.
- crystalline layered silicates of general formula NaMSix02x + i ⁇ y H2O are used, wherein M is sodium or hydrogen, x is a number from 1, 9 to 22, preferably from 1: 9 to 4, particularly preferred values for x being 2, 3 or 4, and y is a number from 0 to 33, preferably from 0 to 20.
- the crystalline layered silicates of the formula NaMSix02x + i ⁇ y H2O for example, by Clariant GmbH (Germany) under the trade name Na-SKS.
- silicates Na-SKS-1 (Na2Si22045 ⁇ x H2O, kenyaite), Na-SKS-2 (Na2 Sii40 2 9 ⁇ x H2O, magadiite), Na-SKS-3 (Na 2 Si 8 0i7 ⁇ x H2O) or Na-SKS-4 (Na 2 Si 4 09 ⁇ x H20, Makatite).
- a montmorillonite-based clay mineral in particular a bentonite
- a bentonite is used as the silicate.
- An equally suitable clay material is, for example, a smectite clay.
- Preferred smectite clays are beidellite clays, hectorite clays, laponite clays, montmorillonite clays, nontronite clays, saponite clays, sauconite clays, and mixtures thereof.
- Montmorillonite clays are the preferred clays.
- Bentonites contain mainly montmorillonites. The bentonites can be used as powder or crystals.
- Suitable bentonites are sold, for example, under the names Laundrosil® by Süd-Chemie or under the name Detercal by Laviosa.
- the layered silicate comprises clay, especially selected from the group consisting of smectites, montmorillonites, bentonites, kaolinites, saponite, hectorite and / or mixtures thereof.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- the layered silicate is native layered silicate and / or organo-modified layered silicate.
- organomodified phyllosilicate
- layered silicate is meant layered silicate which has not been subjected to any particular organomodification.
- the layered silicate comprises clay, in particular selected from the group consisting of smectites, montmorillonites, bentonites, kaolinites, saponite, hectorite and / or mixtures thereof, and the phyllosilicate is native phyllosilicate and / or organomodified phyllosilicate.
- the composition is characterized in that the layered silicate is selected from the group consisting of magnesium or sodium magnesium phyllosilicates.
- Clay minerals such as montmorillonites are particularly preferred according to the invention.
- particularly preferred sheet silicates are the magnesium available under the trade name Laponite ® or sodium magnesium layer silicates from Solvay Alkali, in particular Laponite ® RD or Laponite ® RDS, and magnesium silicates from Süd-Chemie, especially the Optigel® ® SH.
- the composition is characterized in that the composition further contains no inorganic salts.
- the composition is characterized in that the composition further contains an inorganic salt.
- the at least one inorganic salt contained in preferred embodiments may be any inorganic salt consisting of at least one cationic component and at least one anionic component.
- the cationic component may be selected from the metals of Groups 1-15 of the Periodic Table (CAS Groups IA, IIA, INA, IVA, VA, HIB, IVB, VB, VIB, VIIB, VIIIB, IB, IIB and main groups IV and transition metals, respectively ). In various embodiments, it is mono-, di- or trivalent cations.
- the cationic component is selected from Na + , K + , Mg 2+ , Al 3+ , Ca 2+ , Fe 2+ , Fe 3+ , Cu + , Cu 2+ , and Zn 2+ . In further embodiments, the cationic component is selected from Na + , K + , Mg 2+ , Ca 2+ , especially Na + and K + .
- the anionic component may be any anion selected, without limitation, from the group consisting of inorganic anions such as P, Cr, Br, I “ , OH “ , HSOs “ , SOs 2" , SC 2 " , HSOv, N0 2 - , NOs, "PC 3", HPO 4 2 -, H2PO4-, BPr, PF 6 ", CIO4" S1O4 "HCO3- and C0 3 2_.
- the anionic component is preferably halide, SO4 2 " , PO4 3" , HCO3 " and
- the at least one inorganic salt is preferably selected from the group consisting of alkali or alkaline earth metal salts, especially carbonates, sulfates, halides or phosphates. Particularly preferred is selected from sodium sulfate, sodium carbonate, sodium bicarbonate, sodium diphosphate and
- sodium aluminosilicates of the formula (Na 2 O) x. Al 2 O 3. (SiO 2) y . (H 2 O) z , where x is a number from 0.7 to 1.5, y is a number from 1.3 to 4 and z is one Number is from 1 to 6, and magnesium silicate.
- the corresponding potassium salts can also be used.
- mixtures of one or more of the aforementioned inorganic salts are also be used.
- the inorganic salt is not the layered silicate of the present invention.
- the at least one inorganic salt as defined herein is present in an amount of 0.01 to 30% by weight, preferably in an amount of 1 to 30% by weight, based on the total weight of the composition , used. In various embodiments, the at least one inorganic salt is included in the composition in an amount of 10 to 25 weight percent.
- composition of the invention does not comprise
- compositions according to the invention does not comprise a polysaccharide.
- the composition according to the invention does not comprise fumed silica.
- the composition of the invention comprises no precipitated silica.
- the composition of the invention may not comprise polysaccharide, fumed silica, and precipitated silica.
- the composition comprises at least one polysaccharide, at least one fumed silica and / or at least one precipitated silica.
- the at least one polysaccharide which may be included in the composition according to the present invention may be of plant or animal origin or a product of the metabolism of microorganisms as well as a degradation and modification product thereof.
- the polysaccharide is selected from the group consisting of glycogen, starch, callose, cellulose, tunicin, pectin, algin, inulin, chitin, chitosan, heparin, carrageenan, agar, gum arabic, tragacanth, locust bean gum, karaya gum, ghatti - Rubber, Guar Gum, Tara Gum, Gellan, Xanthan, Dextran, Sucrose, Nigeran and
- Pentosans such as xylan and araban, derivatives or mixtures thereof.
- Glycogen starch (amylose and amylopectin), callose, cellulose, tunicin, pectin (s), algin, inulin, chitin, chitosan, heparin, carrageenan, agar, gum arabic, tragacanth, locust bean gum, karaya gum, ghatti gum, guar gum Gum, tara gum, gellan, xanthan, dextran, sucrose, nigeran and pentosans such as xylan and araban, the main constituents of which are D-glucuronic acid, D-galacturonic acid, D-galacturonic acid methyl ester, D-mannuronic acid, L-guluronic acid, D- and L- Galactose, 3,6-anhydro-D-galactose, L-arabinose, L-rhamnose, D-glucuronic acid, D-xylose, L-fucose, D-mannose
- chemically modified polysaccharides include, without limitation, propylcellulose, methylethylcellulose, carboxymethylcellulose,
- Hydroxypropylcellulose hydroxypropylmethylcellulose, carboxymethylhydroxyethylcellulose, sulfoethylcellulose, carboxymethylsulfoethylcellulose, hydroxypropylsulfoethylcellulose,
- Hydroxyethylsulfoethylcellulose methylethylhydroxyethylcellulose, methylsulfoethylcellulose and ethylsulfoethylcellulose.
- the at least one polysaccharide is preferably starch, thermally and / or mechanically treated starch, oxidatively, hydrolytically or oxidized enzymatically degraded starches, oxidized hydrolytic or oxidized enzymatically degraded starches and chemically modified starches.
- starch may be, without limitation, corn, wheat, rice, peas, barley, rye, manioc, tapioca, sweet potatoes, or potatoes.
- native starch is preferably used. As native starch is called starch, as it is accessible from natural, for example, the aforementioned, sources. Native starch is a commercial product and thus easily accessible.
- the at least one polysaccharide is maize, wheat, rice, pea, barley, rye, manioc, tapioca, sweet potato or potato starch.
- the at least one polysaccharide is the corresponding native starch of the abovementioned type. Mixtures of the abovementioned are also suitable.
- the at least one polysaccharide is preferably maize starch, in particular native maize starch. Most preferred is the corn starch Collamyl 8412 from Agrabne Wien.
- fumed silicas are those marketed by Evonik under the trade name Aerosil ® products, in particular of the type Aerosil ® 200; examples for
- inventively preferred precipitated silicas are for example marketed by Evonik under the trade name Sipernat ® products, in particular of the Sipernat ® 22S.
- the fused bodies of the invention contain only each one of these ingredients.
- the at least one polysaccharide is included in the composition in an amount of 10 to 25% by weight, especially 20 to 25% by weight.
- the fumed or precipitated silica is included in the composition in an amount of 1 to 10 wt%, especially 2 to 7 wt%.
- the main component of the solid particulate composition according to the present invention is at least one water-soluble or water-dispersible one Carrier polymer. In various embodiments, this is characterized by at least one
- Carrier polymer characterized in that it has a melting point of 48 ° C to 120 ° C, preferably from 48 ° C to 80 ° C.
- Water Soluble as used herein means a solubility in water at 20 ° C of at least 1 g / L, preferably at least 10 g / L, more preferably at least 50 g / L.
- Water-dispersible as used herein means that the carrier polymer can be dispersed by known methods in water at a temperature of 20 ° C.
- the at least one carrier polymer is preferably selected from polyalkylene glycols.
- those polyalkylene glycols are suitable which have an average molar mass of> 1000 g / mol, in particular> 1500 g / mol, preferably between 3000 and 15,000, more preferably an average molar mass between 4000 and 13000 and
- an average molar mass is between 9,000 and 13,000, most preferably 1,000 to 13,000 or 1,500 to 12,500.
- polyalkyl glycols are suitable which have a melting point between 40 ° C and 90 ° C, in particular in the range of 45 to 70 ° C. examples for
- Polyalkylene glycols suitable in the context of the present invention are:
- Polyalkylene glycols in particular the aforementioned.
- polyalkylene glycols which have an average molar mass of> 1000 g / mol, in particular> 1500 g / mol, preferably between 3000 and 15,000, more preferably an average molar mass between 3000 and 13000 and particularly preferably one average molar mass between 3,000 and 9,000, more preferably an average molar mass between preferably 3,500 to 9,000, in particular between 4,000 to 8,000, most preferably between 6,000 to 8,000.
- those polyalkyl glycols are suitable which have a
- polyalkylene glycols useful in the context of the present invention are polypropylene glycol and polyethylene glycol, as well as block copolymers of various types
- Polyalkylene glycols in particular the aforementioned.
- Preferred commercial products are e.g. Pluriol E 4000, Pluriol E 6000 and Pluriol E 8000 (BASF).
- the at least one carrier polymer is preferably polyethylene glycol.
- the at least one carrier polymer is a polyethylene glycol having an average molar mass of> 1500 g / mol, preferably between 3,000 and 15,000, more preferably with an average molar mass between 4,000 and 13,000, and most preferably with an intermediate molar Mass between 6,000 and 8,000 or 9,000 to 13,000.
- the at least one carrier polymer is a polyethylene glycol having an average molar mass of> 1500 g / mol, preferably between 3,000 and 15,000, more preferably with an average molar mass between 4,000 and 13,000, and most preferably with an intermediate molar Mass between 6,000 and 8,000 or 9,000 to 13,000.
- the at least one carrier polymer is a polyethylene glycol having an average molar mass of> 1,500 g / mol, preferably between 3,000 and 15,000, especially between 3,500 and 13,000, more preferably an average molar mass between preferably 3,500 to 9,000 , in particular between 4,000 and 8,000, very particularly preferably between 6,000 and 8,000.
- the at least one carrier polymer is preferably polyethylene glycol having an average molecular weight of from 10,000 to 15,000, preferably from 1,000 to 13,000, most preferably from 1,500 to 12,500.
- such a polyethylene glycol is characterized by a
- Melting point in the range of 45 to 70 ° C, preferably 50 to 65 ° C, more preferably 50 to 60 ° C.
- compositions as a carrier polymer in addition to the polyethylene glycol according to the invention or also in place of which at least one alkoxy block copolymer.
- Alkoxy block polymers which are suitable according to the invention are preferably of alternating type
- alkoxy block polymers of the formulas HO- (EO) x (PO) y (EO) z -H, HO- (PO) x (EO) y (PO) z -H, HO- (EO) x (PO) y ( PO) zH, HO- (EO) x (EO) y (PO) zH, HO- (EO) x (BO) y (EO) zH, HO- (EO) x (BO) y (EO) z -H, HO- (BO) x (EO) y (BO) z -H, HO- (EO) x (BO) y (BO) zH, HO- (EO) x (BO) y (BO) zH, HO- (EO) x (BO) y (BO) zH, HO- (EO) x (EO) y (BO) zH, HO- (EO) x (EO) y (BO)
- the block polymers preferably have molecular weights between 4,000 and 20,000, in particular 5,000 to 7,000 g / mol.
- Particular preferred are pure EO-PO block copolymers as for example marketed by BASF under the trade name Pluronic ®.
- Pluronic ® PE 6800 is an inventively particularly preferred Alkoxyblockcopolymer.
- the solid compositions contain as carrier polymer at least one polyethylene glycol having an average molar mass of 10,000 to 15,000 and are optionally formulated free of EO-PO block copolymers. It may likewise be preferred according to the invention if the solid preparations comprise at least one EO-PO block copolymer as the carrier polymer and are optionally formulated free of polyethylene glycols having an average molar mass of from 10,000 to 15,000. In a third embodiment, however, it may also be preferred for the solid compositions to contain as carrier material a mixture of at least one EO-PO block copolymer and at least one polyethylene glycol having an average molar mass of from 10,000 to 15,000.
- the at least one carrier polymer or the mixture of various carrier polymers is in an amount of 30 to 95 wt .-%, preferably from 35 to 85 wt .-%, for example 40 to 80 or 40 to 78 wt .-% in the Composition based on the total weight of the composition.
- water-soluble carrier polymer is a polyalkylene glycol, particularly preferably from the
- Polyethylene glycols having an average molar mass in the range of 10,000 to 15,000, preferably from 1 1 .000 to 13,000, most preferably from 1 1 .500 to 12,500, and the composition further comprises at least one active ingredient selected from the group of Polyethlyenglykole with a average molar mass greater than 16,000, the fatty alcohol alkoxylates having at least 10 C atoms in the fatty chain and at least 10 alkoxy units, the alkoxylated castor oils having at least 5 alkoxy units and the alkoxy block copolymers.
- a fragrance is an odor-causing chemical substance.
- the chemical substance should be at least partially redistributable in the air, ie the fragrance should be volatile at 25 ° C, at least to a small extent. If the fragrance is now very volatile, the odor intensity then quickly decreases again. At a lower volatility, the smell impression is more sustainable, ie it does not disappear so quickly.
- the perfume has a melting point that is within the range of -100 ° C to 100 ° C, preferably from -80 ° C to 80 ° C more preferably from -20 ° C to 50 ° C, especially from -30 ° C to 20 ° C.
- the fragrance has a boiling point ranging from 25 ° C to 400 ° C, preferably from 50 ° C to 380 ° C, more preferably from 75 ° C to 350 ° C, especially from 100 ° C to 330 ° C lies.
- the fragrance has a molecular weight of 40 to 700 g / mol, more preferably 60 to 400 g / mol.
- fragrance The smell of a fragrance is perceived by most people as pleasant and often corresponds to the smell of, for example, flowers, fruits, spices, bark, resin, leaves, grasses, mosses and roots. Thus, fragrances can also be used to superimpose unpleasant odors or even to provide a non-smelling substance with a desired odor.
- perfumes individual perfume compounds, e.g. the synthetic products of the ester, ether, aldehyde, ketone, alcohol and type
- Hydrocarbons are used.
- Fragrance compounds of the aldehyde type are, for example, adoxal (2,6,10-trimethyl-9-undecenal), anisaldehyde (4-methoxybenzaldehyde), cymal (3- (4-isopropyl-phenyl) -2-methylpropanal), ethylvanillin, florhydral ( 3- (3-isopropylphenyl) butanal), helional (3- (3,4-methylenedioxyphenyl) -2-methylpropanal), heliotropin, hydroxycitronellal, lauraldehyde, lyral (3- and 4- (4-hydroxy-4-methylpentyl) - 3-cyclohexene-1-carboxaldehyde), methylnonylacetaldehyde, lilial (3- (4-tert-butylphenyl) -2-methylpropanal), phenylacetaldehyde, undecylenealdehyde, vanill
- Ketone-type perfume compounds are, for example, methyl-beta-naphthyl ketone, muskedanone-1-one (2,3,3,6,7-hexahydro-1,1,3,3,3-pentamethyl-4H-inden-4-one), Tonalid (6-acetyl-1,1,1,4,4,7-hexamethyltetralin), alpha-damascone, beta-damascone, delta-damascone, iso-damascone, damascenone, methyldihydrojasmonate, menthone, carvone, camphor, koavon (3 , 4,5,6,6-pentamethylhept-3-en-2-one), fenchone, alpha-ionone, beta- lonone, gamma-methyl-ionone, fleuramon (2-heptylcyclopentanone), dihydrojasmon, cis-jasmone , Iso-E-
- Fragrance compounds of the alcohol type are, for example, 10-undecen-1-ol, 2,6-dimethylheptan-2-ol, 2-methylbutanol, 2-methylpentanol, 2-phenoxyethanol, 2-phenylpropanol, 2-tert-butycyclohexanol, 3,5,5-trimethylcyclohexanol, 3-hexanol, 3-methyl-5-phenyl-pentanol, 3 Octanol, 3-phenyl-propanol, 4-heptenol, 4-isopropyl-cyclohexanol, 4-tert-butylcyclohexanol, 6,8-dimethyl-2-nonanol, 6-nonene-1-ol, 9-decene-1 -ol, ⁇ -methylbenzyl alcohol, ⁇ -terpineol,
- Fragrance type ester compounds are e.g. Benzyl acetate, phenoxyethyl isobutyrate, p-tert-butylcyclohexyl acetate, linalyl acetate, dimethylbenzylcarbinylacetate (DMBCA), phenylethylacetate, benzylacetate, ethylmethylphenylglycinate, allylcyclohexylpropionate, styrallylpropionate,
- DMBCA dimethylbenzylcarbinylacetate
- Ethers include, for example, benzyl ethyl ether and ambroxan.
- Hydrocarbons mainly include terpenes such as limonene and pinene.
- perfume oils may also contain natural perfume mixtures as are available from plant sources.
- Fragrances of plant origin include essential oils such as angelica root oil, aniseed oil, arnica blossom oil, basil oil, bay oil, champacilla oil, citrus oil, fir pine oil, pinecone oil, elemi oil, eucalyptus oil, fennel oil, pine needle oil, galbanum oil, geranium oil, ginger grass oil, guaiac wood oil, gurdy balm oil, helichrysum oil, Ho oil , Ginger oil, iris oil, jasmin oil, cajeput oil,
- Methyl anthranilate p-methylacetophenone, methylchavikole, p-methylquinoline, methyl-beta-naphthyl ketone, methyl-n-nonylacetaldehyde, methyl n-nonyl ketone, muscone, beta-naphthol ethyl ether, beta-naphthol methyl ether, nerol, n-nonyl aldehyde, nonyl alcohol, n-octylaldehyde, p-oxyacetophenone, pentadecanolide, beta-phenylethyl alcohol, phenylacetic acid, pulegone, safrole, isoamyl salicylate, methyl salicylate, salicylic acid hexyl ester, cyclohexyl salicylate, santalol, sandelice, skatole, terpine
- Cinnamic acid ethyl ester Cinnamic acid ethyl ester, cinnamic acid benzyl ester, diphenyloxide, limonene, linalool, linalyl acetate and propionate, melusate, menthol, menthone, methyl-n-heptenone, pinene, phenylacetaldehyde,
- perfume precursor or in encapsulated form (perfume capsules), especially in microcapsules.
- the microcapsules may be water-soluble and / or water-insoluble microcapsules.
- melamine-urea-formaldehyde microcapsules, melamine-formaldehyde microcapsules, urea-formaldehyde microcapsules, or starch microcapsules can be used.
- Perfume precursor refers to compounds that undergo chemical conversion / cleavage, typically by the action of light or other environmental conditions, such as pH, temperature, etc., to release the actual fragrance Such compounds are often referred to as fragrance or "fragrance fragrance".
- the amount of perfume in the composition according to the present invention is preferably between 1 and 20% by weight, preferably between 1 and 15% by weight, in particular between 3 and 10% by weight. based on the
- the solid preparation may contain at least one amorphous silicate or zeolite.
- amorphous sodium silicates with a Na 2 U: SiO 2 modulus of from 1: 2 to 1: 3.3, preferably from 1: 2 to 1: 2.8, and in particular from 1: 2 to 1: 2.6.
- the term "amorphous" is understood to mean that the silicates do not yield sharp X-ray reflections in X-ray diffraction experiments, as they are typical for crystalline substances, but instead possibly one or more maxima of the scattered X-radiation, which have a width of several degrees of the diffraction angle, cause.
- X-ray-amorphous silicates are used whose silicate particles give washed-out or even sharp diffraction maxima in electron diffraction experiments. This is to be interpreted as meaning that the products have microcrystalline regions of the size of ten to a few hundred nm, with values of up to max. 50 nm and in particular up to max. 20 nm are preferred.
- Such X-ray amorphous silicates also have a dissolution delay compared to conventional water glasses. Particularly preferred are compacted / compacted amorphous silicates, compounded amorphous silicates and overdried X-ray amorphous silicates.
- the fuser composition as described herein may further comprise at least one fabric conditioning compound.
- a textile care compound is understood to mean any compound which gives textile fabrics treated therewith a beneficial effect, such as, for example, a textile softening effect, crease resistance or the harmful or negative effects which result during cleaning and / or conditioning and / or or wearing, such as
- the fabric care composition may preferably be made of fabric softening compounds, bleaches, bleach activators, enzymes, silicone oils, anti redeposition agents, optical brighteners, grayness inhibitors, anti-shrinkage agents, wrinkle inhibitors, color transfer inhibitors, antimicrobials, germicides, fungicides, antioxidants, antistatic agents, ironing aids, phobizers and the like Impregnating agents, swelling and slipping agents, UV absorbers and mixtures thereof are selected.
- the fabric care compound is a fabric softening compound. It is most preferred that the fabric softening compound is selected from polysiloxanes, fabric softening clays, cationic polymers and mixtures thereof.
- the use of polysiloxanes and / or cationic polymers as a fabric care compound in the fuser composition is advantageous because it not only exhibits a softening effect but also enhances the perfume impression on the wash.
- the use of softening clays as textile-care compound in the melted body composition is advantageous because they additionally have a water-softening effect and thus, for example, limescale deposits on the laundry can be prevented.
- the fusible composition contain a combination of at least two fabric care compounds.
- the fused-state composition according to the invention contains such textile-care compounds, it is used in particular as a textile care agent or softener or as a constituent of such an agent or else as a constituent of a detergent.
- Such a fabric conditioner may be in the main wash of an automatic washing or
- the enamel composition may be added to the drum or dispenser compartment of a washing machine along with the detergent or cleaning agent. This has the advantage that no additional rinse is necessary and no unsightly deposits occur in the dispenser
- Laundry cleaning process can be used and so the textile-care compound and the perfume already at the beginning of the washing process to transport laundry, so as to be able to develop their full potential.
- the enamel composition according to the invention is simpler and easier to handle than liquid compositions, since no drops remain on the edge of the bottle, which lead to edges on the substrate during subsequent storage of the bottle or to unsightly deposits in the region of the closure. The same is true in the case where some of the enamel body composition is accidentally spilled during dosing. The spilled amount can also be removed easier and cleaner.
- a preferably usable polysiloxane has at least the following structural unit
- R independently of one another C 1 -C 30 -alkyl, preferably C 1 -C 4 -alkyl, in particular methyl or ethyl,
- n 1 to 5000, preferably 10 to 2500, in particular 100 to 1500.
- polysiloxane additionally has the following structural unit:
- R is C 1 -C 30 -alkyl, preferably C 1 -C 4 -alkyl, in particular methyl or ethyl,
- R 2 , R 3 independently of one another are H or optionally substituted, linear or branched C 1 -C 30 -alkyl, preferably C 1 -C 30 -alkyl which is substituted by amino groups, especially
- x 1 to 5000, preferably 10 to 2500, in particular 100 to 1500.
- Polydimethylpolysiloxanes are known as efficient fabric care compounds.
- Suitable polydimethysiloxanes include DC-200 (ex Dow Corning), Baysilone® M 50,
- polysiloxane contains the structural units a) and b).
- a particularly preferred polysiloxane has the following structure:
- Suitable polysiloxanes having the structural units a) and b) are for example commercially available under the trade names DC2-8663, DC2-8035, DC2-8203, DC05-7022 or DC2-8566 (all ex Dow Corning). According to the invention are also suitable for example the products commercially available Dow Corning ® 7224, Dow Corning ® 929 Cationic Emulsion or Formasil 410 (GE Silicones).
- Suitable textile-softening clays are the smectite clays already described above, in particular bentonite.
- Suitable cationic polymers include, in particular, those described in "CTFA International Cosmetic Ingredient Dictionary", Fourth Edition, JM Nikitakis, et al., Editors, published by the Cosmetic, Toiletry, and Fragrance Association, 1991, and the collective name "Polyquaternium Below are some of the more suitable Polyquaternium compounds.
- Celquat® H 100 or Celquat® L200 available as Celquat® H 100 or Celquat® L200 (ex National Starch)
- POLYQUATERNIUM-1 1 (CAS number: 53633-54-8) Definition: Quaternary ammonium polymer formed by reaction of diethyl sulfate with the copolymer of vinylpyrrolidone and dimethylaminoethyl methacrylate.
- Quaternary ammonium polymer salt obtainable by reaction of the ethyl methacrylate / -abietyl methacrylate / diethylaminoethyl methacrylate copolymer with dimethyl sulfate
- Polymeric quaternary ammonium salt which is obtainable by reaction of azelaic acid and dimethylaminopropylamine with dichloroethyl ether.
- Polymeric quaternary ammonium salt which is obtainable by reaction of polyvinyl alcohol with 2,3-epoxypropylamine.
- Polymeric quaternary ammonium salt obtainable by reaction of polyvinyl octadecyl ether with 2,3-epoxypropylamine.
- POLYQUATERNIUM-21 (CAS number: 102523-94-4)
- Synthalen® CR (ex 3V Sigma)
- the melted body composition contains a fabric softening compound and one or more other fabric care compounds.
- the amount of fabric care compound in the fuser composition may, in various embodiments, be from 0.1 to 15 weight percent, and preferably from 2 to 12 weight percent.
- the fuser composition may optionally contain other ingredients. To the application-technical and / or aesthetic characteristics independently of her
- Purpose to improve these additional ingredients are preferably selected from the group consisting of dyes, pearlescing agents, skin-care compounds, bittering agents and mixtures thereof.
- the enamel composition In order to improve the aesthetic impression of the enamel composition, it can be colored with suitable dyes.
- Preferred dyes the selection of which presents no difficulty to the skilled person, should have a high storage stability and insensitivity to the other ingredients of detergents or cleaning agents and to light and no pronounced substantivity to textile fibers so as not to stain them.
- the enamel composition may also contain a pearlescer to increase gloss.
- suitable pearlescing agents are ethylene glycol mono- and distearate and PEG-3-distearate.
- the enamel composition may comprise a skin care compound.
- a skin care compound is a compound or mixture of
- the skin care compound is preferably hydrophobic, may be liquid or solid, and must be compatible with the other ingredients of the solid fused body composition.
- the skin care compound a) waxes such as carnauba, spermaceti, beeswax, lanolin, derivatives thereof and mixtures thereof;
- Plant extracts for example vegetable oils such as avocado oil, olive oil, palm oil, palm kernel oil, rapeseed oil, linseed oil, soybean oil, peanut oil, coriander oil, castor oil, poppy seed oil, cocoa oil, coconut oil, pumpkin seed oil, wheat germ oil, sesame oil, sunflower oil, almond oil, macadamia nut oil, apricot kernel oil, hazelnut oil , Jojoba oil or canola oil, chamomile, aloe vera and mixtures thereof;
- vegetable oils such as avocado oil, olive oil, palm oil, palm kernel oil, rapeseed oil, linseed oil, soybean oil, peanut oil, coriander oil, castor oil, poppy seed oil, cocoa oil, coconut oil, pumpkin seed oil, wheat germ oil, sesame oil, sunflower oil, almond oil, macadamia nut oil, apricot kernel oil, hazelnut oil , Jojoba oil or canola oil, chamomile, aloe vera and mixtures thereof
- higher fatty acids such as lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, oleic acid, linoleic acid, linolenic acid, isostearic acid or polyunsaturated fatty acids
- higher fatty alcohols such as lauryl alcohol, cetyl alcohol, stearyl alcohol, oleyl alcohol,
- esters such as cetyloctanoate, lauryl lactate, myristyl lactate, cetyl lactate, isopropyl myristate,
- Cholesterol isostearate glycerol monostearate, glyceryl distearate, glycerol tristearate, alkyl lactate, alkyl citrate or alkyl tartrate;
- hydrocarbons such as paraffins, mineral oils, squalane or squalene
- vitamins such as vitamins A, C or E or vitamin alkyl esters
- sunscreens such as octyl methoxyl cinnamate and butyl methoxybenzoyl methane;
- silicone oils such as linear or cyclic polydimethylsiloxanes, amino-, alkyl-, alkylaryl- or aryl-substituted silicone oils and
- the amount of skin-care compound is preferably between 0.01 and 10% by weight, preferably between 0.1 and 5% by weight and very particularly preferably between 0.3 and 3% by weight, based on the total weight of the enamel body. Composition. It may be that the skin-nourishing compound additionally has a textile care effect.
- the enamel composition may contain a bittering agent such as Bitrex®.
- Example formulations of suitable enamel compositions include the following ingredients:
- phyllosilicate preferably clay mineral, more preferably bentonite, 0.00 to 30, preferably 10 to 25 wt .-% of an inorganic salt, in particular
- Polysaccharide in particular starch, or from 0.0030 to 30, preferably from 1 to 10, more preferably from 2 to 7,% by weight of a pyrogenic or precipitated silica,
- polyethylene glycol having 4,000 to 15,000 g / mol, preferably 9,000 to 13,000 g / mol as a water-soluble or water-dispersible carrier polymer.
- the fused-state composition according to the present invention is a solid, particulate composition.
- the individual particles of the composition can be referred to as a melting body, which are solid at room temperature and temperatures up to 30 ° C, preferably up to 40 ° C.
- a process for producing such fused bodies can be carried out by means of known batch processes in which the ingredients are mixed and heated together, or one or more of the ingredients are initially charged and heated and then the remaining ingredients are added successively.
- the melt thus obtained can then be subjected to cooling and reshaping.
- methods may be used which include the following steps:
- the at least one polysaccharide (s), and optionally the at least one inorganic salt in step (a), in step (b) or one or more separate steps (b1), (b2), etc., respectively or after step (b) or (c) can be metered.
- the mixing step (c) can then take place after each metering step or only after one or more metering steps.
- the fusible bodies produced in this way can have any desired shape.
- the shaping takes place in particular in step (d) of the described method.
- solid, particulate forms are preferred, such as, for example, substantially spherical, figural, flaky, cuboid, cylindrical, conical, spherical cap or lenticular, hemispherical, disc or needle-shaped particles or even figurative forms.
- the particles may have a gummy-like, figurative design.
- the maximum extent of the particles in a spatial dimension is preferably from 0.5 to 10 mm, in particular 0.8 to 8 mm, particularly preferably 1 to 7 mm and most preferably 2 to 6 mm.
- the diameter of the particles is from 0.5 to 10 mm, in particular 0.8 to 8 mm, more preferably 1 to 7 mm and most preferably 2 to 6 mm.
- the height of the particles is preferably from 0.5 to 6 mm, in particular 0.8 to 5 mm, particularly preferably 1 to 4 mm and very particularly preferably 1 to 5 to 3 mm ,
- the weight of the individual particles is between 2 and 150 mg, preferably between 5 and 10 mg.
- carrier polymer As used herein, when referring to carrier polymer is meant the water-soluble or water-dispersible carrier polymer of the present invention unless the context implies otherwise.
- the melting in step (a) of the processes described herein is accomplished by heating to a temperature not more than 20 ° C above the melting point of the carrier polymer.
- the melting can be carried out using all customary methods and devices known to the person skilled in the art.
- the melt containing the at least one carrier polymer is produced, for example, continuously by the at least one carrier polymer and optionally further constituents of the melt body being continuously fed to a corresponding device in which it is heated and the melt thus produced is further conveyed, for example pumped.
- the at least one perfume can then be added continuously to the melt.
- the at least one perfume is preferably used in liquid form, for example as perfume oil, solution in a suitable solvent or as a slurry of perfume capsules in a typically water-containing solvent.
- "Liquid” as used in this context means liquid under the conditions of use , preferably liquid at 20 ° C.
- the flow can optionally be measured by measuring the flow rate of the individual metered streams, i. the melt, the perfume stream and possibly other ingredient streams are controlled. This also allows, for example, the proportions of the individual metered streams, i. the melt, the perfume stream and possibly other ingredient streams are controlled. This also allows, for example, the proportions of the individual metered streams, i. the melt, the perfume stream and possibly other ingredient streams are controlled. This also allows, for example, the proportions of the individual metered streams, i. the melt, the perfume stream and possibly other ingredient streams are controlled. This also allows, for example, the proportions of the individual
- the ingredients besides the carrier polymer (s) and fragrances can either be produced directly with the carrier polymer together as a melt, be dosed with the fragrances together or separately to the melt. In the latter alternative the metered addition can be carried out before or after addition of the fragrances.
- pyrogenic / precipitated silica and optionally also the at least one inorganic salt are added together or separately from one another in step (a) or step (b) or one or more further steps. It is also possible to choose one of the two aforementioned
- the mixing of the combined metering streams can then be carried out in each case directly after metering or downstream after metering in several or all of the ingredients with suitable mixers, such as customary static or dynamic mixing units.
- the melt which contains the carrier polymer, the fragrances and the phyllosilicate and optionally further ingredients, in particular at least one polysaccharide and / or the at least one pyrogenic or precipitated silica, and / or inorganic salts, is cooled and optionally subjected to transformation fed, where the melt solidifies and receives its final shape.
- suitable methods for shaping are known to the person skilled in the art. Usual forms have already been described above.
- the invention also relates to the use of the solid particulate described herein
- Composition as a textile care agent, preferably fragrancing and / or fabric softener, for scenting and / or conditioning textile fabrics.
- the enamel bodies may be a textile treatment agent, such as, for example, a fabric softener or a part of such an agent.
- the invention relates to a washing or cleaning agent comprising the composition according to the invention.
- composition of the invention By introducing the composition of the invention into a washing or
- Detergent is the consumer a textile-care washing or cleaning agent ("2in1" washing or cleaning agent) available and he does not need to dose two agents and no separate rinse Since the compositions according to the invention are perfumed, not washing This not only results in lower costs, but is also beneficial for consumers with sensitive skin and / or allergies.
- 2in1 textile-care washing or cleaning agent
- the fused-state compositions described herein are particularly suitable for conditioning textile fabrics and are used together with a conventional washing or cleaning agents in the (main) wash of a conventional washing and cleaning process brought into contact with the fabrics.
- Detergent a solid detergent or cleaning agent is preferably mixed with 1 to 20 wt .-%, in particular with 5 to 15 wt .-%, of the composition according to the invention.
- compositions according to the invention are also based on processes for the preparation thereof, the washing and cleaning compositions containing them
- the present invention also relates to fused bodies which have been produced by the process according to the invention.
- Example 1 Formulation of Enamel Formulations
- the layered silicates were incorporated under high shear (5 min Ultra-Turrax at 6500 min "1 ) into the melt of the PEG at 80 ° C.
- the melt viscosity is determined using a rotary rheometer (TA-Instruments, AR G2) with a PP measuring system 40 mm at a shear stress of 3 Pa and at a temperature of 60 ° C.
- Pastilles were prepared from the formulations by dropping the melts through a 2 mm diameter die at a temperature of 60 ° C. from a height of 2 cm onto a steel sheet tempered to 25 ° C.
- the resulting pastilles have on average the following dimensions:
- formulations according to the invention have a more favorable diameter / height ratio.
- E1 and E2 provide almost hemispherical lozenges. Thus, they are subject to a lower edge breakage and act more aesthetically.
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
Description
Claims
Applications Claiming Priority (12)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102016218483 | 2016-09-26 | ||
DE102016218480 | 2016-09-26 | ||
DE102016219296.5A DE102016219296A1 (en) | 2016-09-26 | 2016-10-05 | Perfume-containing enamel body |
DE102016219293.0A DE102016219293A1 (en) | 2016-09-26 | 2016-10-05 | Processing-friendly mass for the production of enamel bodies |
DE102016219295.7A DE102016219295A1 (en) | 2016-09-26 | 2016-10-05 | Continuous process for the preparation of perfume-containing fused bodies |
DE102016219294.9A DE102016219294A1 (en) | 2016-09-26 | 2016-10-05 | Process for the preparation of bitter-bodied enamel bodies |
DE102016219570.0A DE102016219570A1 (en) | 2016-10-07 | 2016-10-07 | Processing-friendly mass for the production of enamel bodies |
DE102017203496 | 2017-03-03 | ||
DE102017203494 | 2017-03-03 | ||
DE102017203501 | 2017-03-03 | ||
DE102017203500 | 2017-03-03 | ||
PCT/EP2017/074099 WO2018055111A1 (en) | 2016-09-26 | 2017-09-22 | Solid particulate compositions comprising water-soluble carrier polymer and perfume |
Publications (1)
Publication Number | Publication Date |
---|---|
EP3516031A1 true EP3516031A1 (en) | 2019-07-31 |
Family
ID=61690197
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP17776991.6A Withdrawn EP3516031A1 (en) | 2016-09-26 | 2017-09-22 | Solid particulate compositions comprising water-soluble carrier polymer and perfume |
Country Status (2)
Country | Link |
---|---|
EP (1) | EP3516031A1 (en) |
WO (1) | WO2018055111A1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3722399A1 (en) * | 2019-04-12 | 2020-10-14 | Henkel AG & Co. KGaA | Solid composition containing perfume |
EP3722405A1 (en) | 2019-04-12 | 2020-10-14 | Henkel AG & Co. KGaA | Fixed composition containing perfume |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102006016578A1 (en) * | 2006-04-06 | 2007-10-11 | Henkel Kgaa | Solid textile softening composition with a water-soluble polymer |
DE102006034051A1 (en) * | 2006-07-20 | 2008-01-24 | Henkel Kgaa | Process for the preparation of a solid textile-softening composition |
DE102009029292A1 (en) * | 2009-09-09 | 2011-03-10 | Henkel Ag & Co. Kgaa | Firm, scented composition |
US10240111B2 (en) * | 2014-11-21 | 2019-03-26 | Colgate-Palmolive Company | Laundry additive |
US10822741B2 (en) * | 2016-02-09 | 2020-11-03 | International Flavors & Frangrances Inc. | Scent booster compositions |
-
2017
- 2017-09-22 EP EP17776991.6A patent/EP3516031A1/en not_active Withdrawn
- 2017-09-22 WO PCT/EP2017/074099 patent/WO2018055111A1/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
WO2018055111A1 (en) | 2018-03-29 |
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