EP2534336B1 - Improvements in hydrocarbon recovery - Google Patents

Improvements in hydrocarbon recovery Download PDF

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Publication number
EP2534336B1
EP2534336B1 EP11700374.9A EP11700374A EP2534336B1 EP 2534336 B1 EP2534336 B1 EP 2534336B1 EP 11700374 A EP11700374 A EP 11700374A EP 2534336 B1 EP2534336 B1 EP 2534336B1
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EP
European Patent Office
Prior art keywords
steam
injector
aicd
production
tubing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Not-in-force
Application number
EP11700374.9A
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German (de)
English (en)
French (fr)
Other versions
EP2534336A2 (en
Inventor
Haavard Aakre
Rex Man Shing Wat
Vidar Mathiesen
Bjørnar WERSWICK
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Equinor Energy AS
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Statoil Petroleum ASA
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Publication of EP2534336A2 publication Critical patent/EP2534336A2/en
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    • E—FIXED CONSTRUCTIONS
    • E21—EARTH OR ROCK DRILLING; MINING
    • E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/16—Enhanced recovery methods for obtaining hydrocarbons
    • E21B43/24—Enhanced recovery methods for obtaining hydrocarbons using heat, e.g. steam injection
    • E21B43/2406—Steam assisted gravity drainage [SAGD]
    • E—FIXED CONSTRUCTIONS
    • E21—EARTH OR ROCK DRILLING; MINING
    • E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B34/00—Valve arrangements for boreholes or wells
    • E21B34/06—Valve arrangements for boreholes or wells in wells
    • E21B34/08—Valve arrangements for boreholes or wells in wells responsive to flow or pressure of the fluid obtained
    • E—FIXED CONSTRUCTIONS
    • E21—EARTH OR ROCK DRILLING; MINING
    • E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/12—Methods or apparatus for controlling the flow of the obtained fluid to or in wells

Definitions

  • the present invention relates to a thermal hydrocarbon recovery apparatus and an associated method.
  • the invention relates to thermal hydrocarbon recovery by steam injection.
  • hydrocarbon reserves are known to be present in the Earth's subsurface in oil or tar sands.
  • the hydrocarbons found in these settings take the form of bitumen or heavy crude oil which is particularly dense and viscous and does not flow naturally.
  • a well can be drilled into a hydrocarbon bearing formation and hydrocarbons such as petroleum and gas will readily flow from the hydrocarbon-bearing geological formation through the well to the Earth's surface due to higher pressures of the formation compared with the Earth's surface.
  • the viscous bitumen and heavy crude oil is more difficult to extract, although it is possible to do this using thermal hydrocarbon recovery techniques.
  • the key principle of thermal recovery is to heat up the oil sands so that the bitumen or heavy oil becomes sufficiently viscous that it will flow, allowing it then to be extracted from the formation in its heated and flowable condition.
  • One technique for doing this involves drilling a well and then injecting steam through the wellbore into the formation to heat up the formation and the heavy oil. Thereafter, the oil is extracted through the wellbore to the surface. Several cycles of heating and extraction would typically be carried out.
  • the method typically uses a single wellbore both for injecting the steam and for extracting and moving the oil to the surface, and is known as a "huff and puff' system.
  • SAGD steam assisted gravity drainage
  • a steam heated region of the formation above and around the injector wellbore is formed, known as a steam "chamber".
  • This causes the heavy oil to heat up and drain downwards under gravity towards the producer wellbore that has been warmed up during initial circulation.
  • the drainage of oil allows the steam to rise up further through the steam chamber toward its periphery enabling continuous growth of the steam chamber.
  • the steam then condenses and flows downwards together with the mobile oil under the influence of gravity to the producing wellbore beneath.
  • the injector and producer wellbores comprise horizontal sections that run roughly parallel and horizontally in the geological formation and are spaced a few metres apart from each other with the injector wellbore located above the producer wellbore, for example by a spacing of around 5 m.
  • the production rate may need to be limited to maintain the mobile hydrocarbon layer in the present SAGD technique. This may be done for example by controlling the lift pump operating inside the production pipe to control drawdown pressure in the tubing or by reducing the steam injection from the injector wellbore. Temperature also needs to be controlled to maintain a fluid trap around the producer tubing. Specifically, the temperature in the region around the producer wellbore has to be kept cooler than the steam chamber temperature, i.e. "sub-cool", in order for a suitable fluid trap to build up and be maintained.
  • ICDs inflow control devices
  • ICDs inflow control devices
  • channel or nozzle type ICDs these are disposed on the production tubing or liner to provide fluid connection between the tubing interiors and the geological formation in specific locations along the tubing sections.
  • ICDs in the producer tubing impose an additional pressure drop between the formation and the tubing to hinder steam breakthrough and to maintain the fluid trap around the tubing. Nevertheless, avoiding steam breakthrough and forming a suitable sub-cool trap around the producer tubing are significant challenges associated with present thermal recovery techniques.
  • a wellbore hydraulic effect occurs, which limits the length of horizontal tubing usable in the SAGD. In turn, this means that numerous wells typically need to be drilled to provide the necessary coverage to thermally recover heavy oil from a given region.
  • the maximum length of a horizontal section for SAGD is around 500-1000 m. This is because the amount of steam entering the geological formation (exiting the wellbore) and the amount continuing further downstream inside the wellbore is significantly dependent on the localised pressure balance, as shown in Figure 2 .
  • ICDs fixed flow path inflow control devices
  • the injector wellbore are fitted in the injector wellbore and are disposed on the tubing or the liner to provide fluid connection between the respective tubing interiors and the geological formation in specific locations along the tubing sections.
  • the ICDs provide an outlet for the steam into the formation.
  • the injector tubing is pressurised to a pressure above the formation pressure, and steam can thereby be forced through the ICDs.
  • ICDs are provided along the length of the tubing allowing steam to be injected at specific locations along the tubing providing high steam injectivity at those locations.
  • ICDs in the injector tubing imposes an additional pressure drop between the tubing and the formation. This enables more steam, which would otherwise 'leak off' into a receptive formation, to be channelled along the injection wellbore through a horizontal section of the wellbore.
  • a problem associated with using these ICDs in the injector tubing is that the steam flow rate is driven by the pressure differential, as seen in Figure 1 . Since formation pressure varies somewhat along the length of the tubing and over time, a change in the pressure differential can be caused and then, due to the sensitivity of flow rate to a change in the pressure differential, it can be hard therefore to control the desired steam rates so as to form a suitable steam chamber.
  • the technique has been adapted to make use of the critical flow rate for fixed flow path orifice/channel and nozzle ICDs, which is a predictable, constant flow rate known occur at the speed of sound.
  • the steam injection rate is up to a point dependent on the pressure differential but at this critical flow rate, the steam injection flow rate cannot be increased any further, even if the pressure differential is made larger.
  • a drawback is that this requires a pressure differential to be generated in the tubing of approximately twice the formation pressure in order to create this effect using conventional tubing and ICD arrangements. Since the need of doubling the pressure differential also applies at the toe section, which is furthest away, it will require significantly higher overall steam pressure at the wellhead.
  • Injection into the formation in this critical flow mode requires therefore an undesirably large amount of energy, and the high speed of the fluid can impart significant erosion and damage to the equipment.
  • the steam exiting the ICDs is typically turbulent and may require additional diffusers in order to harness and direct the flow of steam into the formation as required.
  • the use of diffusers also causes dissipation of energy from the flow.
  • thermo hydrocarbon recovery apparatus According to a first aspect of the present invention, there is provided a thermal hydrocarbon recovery apparatus according to claim 1.
  • a method of designing a thermal hydrocarbon recovery apparatus of claim 1 is set out in claim 14.
  • Disclosed arrangements may provide thermal hydrocarbon recovery apparatus comprising at least one flow control device for autonomously adjusting a flow of fluid through the flow control device, the at least one flow control device provided to a tubing for location in a wellbore, the flow control device being arranged to fluidly connect a geological formation with an inside of the tubing, and wherein the tubing is further arranged for at least one of: injecting steam into the geological formation for heating hydrocarbons; and moving steam heated hydrocarbons from the geological formation to the surface, wherein at least some of the flow control devices comprise a body defining a flow path through the AICD and defining a recess containing a movable valve body, arranged so that movement of fluid along said flow path causes the valve body to move by exploiting the Bernoulli effect thus controlling the flow of fluid along said flow path.
  • the apparatus may comprise a first, injector tubing for injecting steam into the geological formation for heating hydrocarbons, and a second, producer tubing for moving steam heated hydrocarbons from the geological formation to the surface, wherein the at least one flow control device may be provided to at least one of the injector tubing and the producer tubing. At least one flow control device may be provided to each of the injector tubing and the producer tubing.
  • the producer tubing may be provided with at least one flow control device configured to autonomously permit flow of heated oil and water but restrict flow of steam through the flow control device from the formation.
  • the producer tubing may be provided with a plurality of said flow control devices spaced apart from each other along a length of the tubing.
  • the injector tubing may be provided with a plurality of said flow control devices spaced apart from each other along a length of the injector tubing, wherein each flow control device may be configured to permit flow of steam through the control device at a predetermined flow rate.
  • the flow control devices may be arranged to produce a predetermined profile of steam injectivity along a length of the injector tubing.
  • Different flow control devices may be configured to produce substantially the same steam flow rate.
  • the flow control devices may be configured to permit flow of steam therethrough at a substantially constant flow rate, where the steam in the injector tubing is pressurised sufficiently.
  • the injector tubing may comprise an injector tubing section arranged to extend substantially horizontally and in spaced parallel relationship with a producer tubing section of the producer tubing.
  • the injector tubing and producer tubing may be spaced apart from one another by a distance of less than 5 m, less than 4 m, less than 3 m, less than 2 m and/or less than 1 m. For example, they may be spaced apart by a distance of between around 1 and 2 m.
  • the injector tubing may comprise a plurality of steam injector tubing sections arranged to be located within respective substantially horizontal wellbore sections, and a connecting injector tubing section which is arranged to extend between a surface well head and a subsurface location for fluidly connecting each of the plurality of steam injector tubing sections with the surface well head.
  • the producer tubing may comprise a plurality of producer injector tubing sections arranged to be located within respective substantially horizontal wellbore sections, and a connecting producer tubing section which is arranged to extend between a surface well head and a subsurface location for fluidly connecting each of the plurality of producer injector tubing sections with the surface well head.
  • the geological formation may be an oil sand and the hydrocarbons to be recovered may be viscous hydrocarbons.
  • the apparatus may take the form of a steam assisted gravity drainage system.
  • Disclosed arrangement may also provide use of an autonomously adjustable flow control device in a thermal oil recovery system in which steam is injected into a geological formation to heat hydrocarbons and the steam-heated hydrocarbons are moved from the geological formation to the surface.
  • the use may provide the effect of discriminating against steam inflow into a tubing of the recovery system which tubing may be arranged for moving hydrocarbons from the hydrocarbon formation to the surface.
  • the use may provide the effect of controlling the formation of a steam chamber to safeguard against steam breakthrough and/or provide the effect of assured recovery of oil under steam breakthrough conditions.
  • Disclosed arrangements may also provide a method of thermal recovery of hydrocarbons from a geological formation, the method comprising the steps of:
  • the method may be a method of assured recovery, or production, of oil under steam breakthrough conditions. Thus, it may safeguard production and prevent damage to equipment even if steam is present against the outer surface of a producer tubing. It may also be a method of controlling steam chamber formation.
  • the method may use any features of the apparatus defined above, where appropriate.
  • FIG. 3A and 3B there is shown a process for thermally recovering hydrocarbons from an oil sand by steam assisted gravity drainage (SAGD).
  • SAGD steam assisted gravity drainage
  • the present examples are described particularly with reference to the SAGD method, but it will be appreciated that embodiments described herein are equally applicable to other steam assisted thermal recovery methods including for example the single tubing cyclical "huff and puff" method mentioned above or non-cyclic continuous steam drive systems or the like.
  • FIGS 3A and 3B a section of the Earth's subsurface is shown with an oil sand formation 12 located at depth.
  • An injection well 14 and a production well 16 are provided one above the other comprising horizontal injector and producer tubing sections 14h,16h, separated by a vertical spacing of around 5 m.
  • Injection of steam from the injector tubing section 14h generates a mushroom shaped heated region or "steam chamber" 18 in the oil sand layer above and around the wellbore section 14h.
  • a convection process is initiated by which bitumen or heavy oil in the oil sand is heated and drains downwards whilst the steam rises through the steam chamber. As it reaches a cooler outer area of the chamber the steam condenses.
  • the heated bitumen becomes mobile and drains downward together with condensed water as indicated by arrows 18a.
  • the bitumen or heavy oil is flowable and is drawn into the producer tubing under formation pressure and/or with assistance of a production lift pump (not shown) inside the production tubing section 16h by which the mobilised bitumen or heavy oil together with the condensed water is returned to the surface production well head 19.
  • the injector tubing section 14h and the producer tubing section 16h are both fitted with multiple flow control devices 14f, 16f in the wall of the tubing sections and are spaced apart from each other along the length of the respective tubing sections.
  • the tubing referred to here can be a liner or sand screen (in direct contact with the geological formation) or an internal tubing that locates inside the liner/screen. These devices provide fluid connection and passage between the geological formation 12 and the interiors of the production and injection tubing sections 14h, 16h.
  • the flow control devices in this example are so-called autonomous inflow control devices (AICDs). These devices comprise a housing and a "floating disc" inside the housing to define a flow path for fluid through the valve. Importantly, the floating disc creates a flow restriction. However, the disc is movable within the housing to alter the flow path restriction.
  • AICDs autonomous inflow control devices
  • the AICDs provide two particular effects, which contribute to the production of hydrocarbon and the injection of steam. Firstly, the disc moves in response to the stagnation pressure and the velocity of fluid. This means that it autonomously adjusts its position and flow path to conserve energy, following the principles of Bernoulli's equation. Thus, for a given pressure differential between the inside of the tubing and the geological formation, the flow can be choked or shut off altogether when a lower viscosity fluid is encountered at the restriction, and as the disc moves to close the flow path due to low pressure. The disc movement is caused by high stagnation pressure on one side and faster flowing low viscosity fluid that creates a lower dynamic pressure on the other.
  • the autonomous valve when the autonomous valve is subjected to single-phase flow such as steam the floating disc will remain open, whilst its position within the housing is balanced by the stagnation pressure created at the back of the disc and the flowing "dynamic" pressure formed at the front of the disc. The higher the flow rate, as induced by a larger differential pressure across the valve, the dynamic flowing pressure at the front of the disc becomes lower. This pulls the disc closer to its 'SHUT' position and reducing the flow rate automatically. Effectively the autonomous valve will yield an "almost" constant flow rate once a threshold maximum differential pressure is reached.
  • the flow valves for the production tubing section 16h for the present SAGD system makes use of the first of these operating principles, as can be seen with reference firstly to Figures 4A and 4B .
  • Figure 4B there is shown a plot 20 of differential pressure (between the wellbore formation and the drawdown pressure in the tubing) against flow rate for the AICDs used in the production tubing section.
  • the plot 20 displays performance graphs for water 20a, oil 20b, and gas/steam 20c showing the flow rate behaviour through the valve. All of the curves 20a-20c show a rapid increase in differential pressure whilst flow rate increases.
  • the AICDs 16f in the producer tubing 16h are designed to discriminate against the steam based on the autonomous adjustability of the AICDs.
  • the AICD is designed to permit flow of heated oil or liquid bitumen and condensed water through the AICD, but prevent steam flow. Should any steam break through to the production tubing section, flow of steam through the AICD will be blocked off or choked since the viscosity of the steam is significantly lower than that of the liquid oil or bitumen or water, which causes the floating disc of the AICD to restrict the flow path in the valve. The stagnation pressure then keeps the valve 'SHUT' until steam is replaced by oil or liquid flow. As a result, the risk of drawing steam into the production well bore is greatly reduced. Damage to the lift pump by steam is avoided whilst there is adequate inflow of oil and water through the AICDs in the rest of the wellbore to meet the withdrawal rate of the pump.
  • FIG. 5A the fluid discrimination and shut off functionality of the AICD is shown.
  • the production tubing section 14h is shown with the AICD 14f provided in a wall of the section 14h.
  • a layer of molten liquid bitumen plus water 18t drained from the steam chamber 18 lies along and around an outer surface of the production tubing section 14h, and is presented to the AICD.
  • Flow is permitted through the AICD and into the producer tubing to the well head as indicated.
  • FIG 5B a steam breakthrough scenario is illustrated, and the AICD has blocked off the steam due to its sensitivity and discrimination against low viscosity steam.
  • the remaining parts of the producer tubing equipped also with AICDs, will continue to produce the bitumen and water unhindered until they are 'SHUT' by the encroaching steam.
  • the AICDs ensure that any steam entering the production tube is less than 5% by weight of the total fluid entering the production tube.
  • steam is drawn close to but not through the production tubing, so as to operate effectively at "zero-subcool".
  • This improves the overall thermal recovery process, firstly because the steam injection can be performed more 'aggressively' without the fear of the steam short-circuiting into the production well below. More heat energy can be used to facilitate the steam chamber growth and accelerate the recovery of oil.
  • the steam chamber extends to the close vicinity of the producer tubing instead of being shielded by an overlying liquid trap that has to be kept cooler (subcool), a warmer and hence a more effective drainage process takes place in this critical near well bore region.
  • the autonomous discrimination against steam flow is also beneficial in terms of the entire 'horizontal' section of the production well regardless of the elevation of the well trajectory.
  • sections at a higher elevation may have steam drawn into it initially, at which point the AICDs close momentarily and temporarily until water and molten oil build up again and they re-open.
  • sections at other elevations may follow a different open-close cycle and the AICDs will open and close in response to steam being drawn into those other sections at different times.
  • the graph 30 shows a characteristic performance curve 32 for the AICD, which indicates a rapidly increased flow rate for increased differential pressure.
  • a lower threshold differential value 34a the flow rate no longer changes significantly which means that provided the pressure differential is somewhere above the threshold, a stable flow rate into the formation is achieved.
  • a constant flow rate of steam is selected and applied under pressure into the injection tubing to ensure that the pressure differential across the AICD is above the threshold 34a.
  • the injection pressure is applied to the tubing at a fixed output level, sufficiently above the threshold 34a to account for and reduce sensitivity to possible variations in pressure in the formation, which may impact on the pressure differential.
  • the threshold 34a represents the minimum differential pressure that is required for the AICD located furthest away from the wellhead.
  • an operating region 36 of pressure differentials which ensures flow through the AICD at the maximum and 'near constant' flow rate. This may be defined based on expected variations in differential pressure for a given hydrocarbon reservoir scenario. This can also be defined based on the total length of the injection tubing, either in a single or 'multi-branch' configuration. In general, each AICD may be configured differently depending on its position within the system.
  • the operating region extends to an upper threshold pressure differential 34b. It might be possible to generate pressure at significantly higher differentials, above an upper threshold value 34b but it is typically unnecessary to design the steam injection system in this way since by operating at a fixed output level in the operating region 36, a constant maximum flow rate is achievable already.
  • the steam flow rate for each AICD varies over time by less than 10% of a mean value.
  • the physical properties of steam e.g. density, vary with temperature.
  • a typical mean steam flow rate may be between 0.3 and 10 m 3 /hr, or between 0.7 and 0.9 m 3 /hr, and the threshold value 34a may be between 8 and 12 kPa.
  • the range values quoted here are for steam around a mean temperature of 155 degrees C, and for the same AICD these range values will be different at, say 230 degrees C.
  • the appropriate steam temperature is chosen in the field.
  • Each AICD will have a 'near constant' flow rate, but one location may require 2 to 10 times more steam than another location, for example.
  • the AICDs in the injector tubing 14h are preferably individually designed so that each AICD outputs a specific (same or different) flow rate according to the need for growing the steam chamber. This may be carried out by adjusting the sensitivities of the AICDs so that different pressure differentials in different AICDs produce the respective maximum flow rates. Producing a specific 'near constant' maximum flow rate at each AICD along the injector tubing also means that steam can be targeted more precisely along the horizontal well, for example evenly for homogeneous sand producing a relatively flat injectivity profile along the length of the wellbore section or specifically distributed to compensate for the heterogeneity in reservoirs with other lithologies.
  • the AICD design for the injector tubing takes into account that pressure in the steam injector tubing is higher at an upstream end, and that fluid which is not passed into one AICD flows to successive AICDs downstream, resulting in a reduced pressure in the tubing and therefore a reduced differential pressure across each AICD.
  • the AICD are designed therefore to have a flow rate behaviour such that a maximum and "near constant" flow rate can be generated for the expected differential pressure for the particular AICD along the tubing.
  • the size, dimensions and/or materials may be selected to provide the desired flow behaviour, and this could apply also to the producer tubing.
  • the size and dimensions or scale of the AICDs in different positions along the tubing may be different in order to produce different flow rate responses when subjected to a pressure differential.
  • This constant flow rate behaviour is achieved at relatively low differential pressures, in contrast to the previously used flow devices that relied on achieving critical flow.
  • Figure 7 a system for thermal recovery of hydrocarbons from a large geographical region is shown in which the producer and injector tubing sections are provided with AICDs.
  • Figure 7 shows generally an SAGD arrangement 40 which has a plurality of horizontal injection tubing sections 40s extending away in opposing directions from a joining pipe section 40j which is also a horizontal tubing section connecting the horizontal sections 40s.
  • the joining pipe section 40j is then connected to a well head at the Earth's surface via a single vertical section 40v.
  • the arrangement 40 also includes a plurality of horizontal producer tubing sections 40p arranged in a similar way and connected to the surface well head via a single vertical section 40w.
  • the steam injection sections 40s are located above the production sections 40p to provide the steam assisted drainage required.
  • producer tubing and injector tubing are located, in use, in production and injection wellbores of the production and injection wells.
  • the producer and/or injector tubing may take the form of a wellbore liner or sandscreen or the like and that the AICDs may be fitted to the liner and/or sandscreen.
  • the producer tubing and/or injector tubing may take the form of a separate production pipe and/or injector pipe located, in use, within wellbores provided with a liner and/or sandscreen or the like, and that the AICDs may be fitted to the separate production and/or injector pipe.
  • the AICD itself may be fitted with a mesh or the like or be otherwise arranged to shut out and prevent inflow of sand or other particles from the formation.

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Geophysics And Detection Of Objects (AREA)
  • Extraction Or Liquid Replacement (AREA)
EP11700374.9A 2010-02-12 2011-01-19 Improvements in hydrocarbon recovery Not-in-force EP2534336B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CA2692939A CA2692939C (en) 2010-02-12 2010-02-12 Improvements in hydrocarbon recovery
PCT/EP2011/050696 WO2011098328A2 (en) 2010-02-12 2011-01-19 Improvements in hydrocarbon recovery

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EP2534336A2 EP2534336A2 (en) 2012-12-19
EP2534336B1 true EP2534336B1 (en) 2018-09-26

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US (1) US20130000883A1 (es)
EP (1) EP2534336B1 (es)
CN (1) CN102892974B (es)
CA (1) CA2692939C (es)
EA (1) EA023605B1 (es)
MX (1) MX339348B (es)
WO (1) WO2011098328A2 (es)

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WO2011098328A3 (en) 2012-03-01
EP2534336A2 (en) 2012-12-19
WO2011098328A2 (en) 2011-08-18
CA2692939A1 (en) 2011-08-12
CN102892974B (zh) 2016-11-16
EA201290778A1 (ru) 2013-03-29
EA023605B1 (ru) 2016-06-30
CA2692939C (en) 2017-06-06
US20130000883A1 (en) 2013-01-03
CN102892974A (zh) 2013-01-23
MX2012009325A (es) 2012-11-30
MX339348B (es) 2016-05-19

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