EP2005501A1 - Méthode et apparail de fabrication d'un systeme de batterie - Google Patents

Méthode et apparail de fabrication d'un systeme de batterie

Info

Publication number
EP2005501A1
EP2005501A1 EP06739824A EP06739824A EP2005501A1 EP 2005501 A1 EP2005501 A1 EP 2005501A1 EP 06739824 A EP06739824 A EP 06739824A EP 06739824 A EP06739824 A EP 06739824A EP 2005501 A1 EP2005501 A1 EP 2005501A1
Authority
EP
European Patent Office
Prior art keywords
battery
die
mould
plates
melting metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP06739824A
Other languages
German (de)
English (en)
Other versions
EP2005501A4 (fr
Inventor
Gustavo Daniel Bruni
Julian Prado
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of EP2005501A1 publication Critical patent/EP2005501A1/fr
Publication of EP2005501A4 publication Critical patent/EP2005501A4/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/64—Carriers or collectors
    • H01M4/70—Carriers or collectors characterised by shape or form
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/50—Current conducting connections for cells or batteries
    • H01M50/531—Electrode connections inside a battery casing
    • H01M50/534—Electrode connections inside a battery casing characterised by the material of the leads or tabs
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/10—Primary casings; Jackets or wrappings
    • H01M50/102—Primary casings; Jackets or wrappings characterised by their shape or physical structure
    • H01M50/112—Monobloc comprising multiple compartments
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/50—Current conducting connections for cells or batteries
    • H01M50/528—Fixed electrical connections, i.e. not intended for disconnection
    • H01M50/529—Intercell connections through partitions, e.g. in a battery casing
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/50—Current conducting connections for cells or batteries
    • H01M50/531—Electrode connections inside a battery casing
    • H01M50/536—Electrode connections inside a battery casing characterised by the method of fixing the leads to the electrodes, e.g. by welding
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/50—Current conducting connections for cells or batteries
    • H01M50/531—Electrode connections inside a battery casing
    • H01M50/54—Connection of several leads or tabs of plate-like electrode stacks, e.g. electrode pole straps or bridges
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

Definitions

  • the present invention relates to a new method and apparatus for manufacturing a battery assembly and the battery assembly obtained by the method and apparatus, and preferably the invention refers to a method for making a safe and reliable interconnection of the battery plates with less manufacturing steps as compared to typical methods .
  • a battery is comprised of a battery box including a plurality of inner partitions for defining the elements or elements where the positive and negative plates are arranged. Each plate is provided with a plate lug upwardly extending in order to be interconnected to form the circuitry of the battery.
  • There are several techniques to connect the lugs but there is one important aspect that must be taken into account by any of the procedures and this aspect is that the connection between the lugs must be reliable, otherwise, if only one connection fails to provide a continuous electrical conductivity the battery does not work.
  • US No. 3,944,436 to Gaide discloses a method comprising the steps of inserting the plate lugs in an elementary mould connecting together the plate lugs by rods formed by melting lead, and making the connection between the rods associated with plates of opposite polarities of two adjacent elements of the accumulator.
  • the elementary mould comprises a channel common to two adjacent elements of the accumulator and is provided onto the plates in the battery box.
  • the elementary mould comprises two channels with each of them having the plate lugs of same polarity fitted in them.
  • the connections between the plates of one element and the plates of an adjacent element are formed by melting the lugs 46, 48 of both positive and negative plates, such melting being effected either by means of a blow-pipe or a heating rod, or by casting lead in the channels 42 and 43 of the moulds 40 or 40; or by means of turns through which a high-frequency current flows.
  • This method requires of elementary moulds to be arranged onto the plates in a manner that each lug passes through a notch of the mould, making the process to be cumbersome and time consuming .
  • US Patent No. 5,505,744 to Eberle et al US Patent No. 5,505,744 to Eberle et al .
  • the first step gathers a group of battery plates with lugs protruding from a non- metallic case.
  • a second step consists of immersing the protruded lugs in a mould filled with a molten lead by rotating the lugs downward direction.
  • the mould is shaped for strap cavities 114 and 112 where the lugs are immersing, and cavities for two terminals 116 and 118, as shown in Figs. 11-13.
  • the group of plates of this patent is all arranged in only one battery box without partitions as it is typical in a battery with several elements. Under these circumstances this patent does not approach the problem of interconnecting the plates in one element with the plates in an adjacent element involving, in this interconnection, the necessary battery partition.
  • US No. 6,059,848 to Shannon et al discloses an improved battery design which utilizes the battery cover of the container as a mold to make the cast electrical circuits, including the external terminals.
  • the battery cover includes a plurality of plate strap mold wells which receive molten lead, with the mold wells being separated by a partition wall and including an aperture formed in the partition wall to allow molten lead to flow between adjacent plate strap mold wells and connect thereof.
  • Terminal mold wells have terminal apertures through which molten lead flows to form an external terminal with the aid of an external terminal mold.
  • a meltable sealant material is pre-applied to the plurality of mold wells to become fluid under the temperature of molten lead and to solidify when cooled to prevent leakages of electrolyte and gasses.
  • the cover is simultaneously fixed to the battery box while die-casting the straps of the circuitry. While the problem of failure in the connection of plate lugs has been partially solved and the time of manufacturing process has been reduced, there exist the drawback that the quality control of the plate straps can not be carried out in a proper manner as long as, when the straps are cooled down and in solid status, it would be necessary to remove the cover and open the battery to control the plate straps and interconnections .
  • each positive polarity plate in one cell element includes an upstanding lug 10 and each negative plate in the cell element in the next adjacent compartment includes an upstanding lug 12.
  • the positive plate lugs 10 of one cell element are aligned with each other and with similarly aligned negative plate lugs 12 in the next cell element on opposite sides of the opening 8 in the partition 6.
  • the positive polarity lugs 10 are surrounded by a trough 14 and the negative polarity lugs 12 are surrounded by a trough 16.
  • the troughs 14 and 16 remain with the battery and if they are made from thermoplastics they may be temporarily flanked by blocks of metal to support the sides of the troughs 14 and 16 against drooping under the heat from the melt. After solidification, the blocks are removed. Again, this method is cumbersome as long as it requires the use of additional pieces and tools such as the troughs 14, 16.
  • An apparatus and the obtained battery is also provided.
  • It is a further object of the present invention to provide an apparatus for making a battery comprising a battery box or container and a battery cover fixed to the box, the box including a plurality of partitions defining separate elements receiving said battery plates, the partitions including alternate orifices to communicate each adjacent pair of elements and the battery plates comprises positive battery plates and negative battery plates with each battery plate having a plate lug and with the plate lugs of the positive battery plates being aligned at one side of the battery box and the plate lugs of the negative battery plates being aligned at another side of the battery- box, the apparatus comprising at least one mould for die- casting a melting metal, the mould having a number of element die sections separated by gaps and each gap is designed for receiving one of said partitions of the battery box and for accommodating one orifice of the partition to fluidly communicate two adjacent element die sections, wherein the mould comprises a mould body having a lower portion with at least one inlet for the melting metal and an upper portion having said element die sections, with the inlets for the melting metal being connected to inner conduit
  • It is a further object of the present invention to provide a battery comprising a battery box or container and a battery cover fixed to the box, the box including a plurality of partitions defining separate elements receiving said battery plates, the partitions including orifices to communicate each adjacent pair of elements and the battery plates comprises positive battery plates and negative battery plates with each battery plate having a plate lug and with the plate lugs of the positive battery plates being aligned at one side of the battery box and the plate lugs of the negative battery plates being aligned at another side of the battery box, wherein the plate lugs are interconnected by plate straps obtained by die-casting a melting metal around the plate lugs, with the plate lugs of an element being interconnected with the plate lugs of an adjacent element through one of said orifices in the battery partition.
  • Figure 1 shows a top perspective view of a battery box or container with some battery plates being inserted into the cells or elements and some elements being empty, with the battery cover not shown for clarity purposes, all according to a preferred embodiment of the present invention
  • FIG. 2 shows a top perspective view of the battery of Figure 1 with the plate straps, according to the invention, already formed into the battery container;
  • Figure 3 shows a cross section view along cutting line III-III of Figure 2;
  • Figure 4 shows a cross section view along cutting line IV-IV of Figure 2
  • Figure 5 shows a top perspective view of a mold according to a preferred embodiment of the invention to manufacture the plate straps of Figures 2 , 3 ;
  • Figure 6 is a perspective view of a battery of Figure 1, with all the plates arranged therein and the box inverted to be placed into a couple of molds of Figure 5, according to the invention;
  • Figure 7 shows a cross section of the mold taken along line VII-VII of Figure 5,-
  • Figure 8 shows a cross section of the mold taken along line VIII-VIII of Figure 5;
  • Figure 9 shows a cross section of the mold taken along line IX-IX of Figure 5, and
  • Figure 10 shows a cross section of the mold taken along line X-X of Figure 5.
  • a battery 1 comprising a battery box or container 2 and a plurality of battery partitions 3 defining separate cells or elements 4.
  • a pack of battery plates 5 is arranged within each element 4, with a pack 5 being shown, in Figure 1, partially inserted in an end element, with another pack being entirely placed into another element and with other elements empty just for clarity purposes.
  • Each pack 5 is comprised of a plurality of battery- plates, namely positive plates 6 and negative plates 7, arranged in a manner that they are interleaved but with the positive plates isolated from the negative plates.
  • Each battery plate 6, 7 has a corresponding plate lug 8, 9, with plate lugs 8 of the positive battery plates being aligned at one side of the battery box and plate lugs 9 of the negative battery plates being aligned at another opposite side of the battery box as better shown in Figure 4.
  • Partitions 3 include orifices 10 in alternating side positions, that is, when a partition has an orifice at one side of box 2, the adjacent partitions have their respective orifices 10 at the opposite side, as illustrated in Figure 1. Each orifice communicates one element with the adjacent one.
  • the battery assembly as shown in Figure 2, to which reference will be made below in connection to the particular aspects of the invention, is to be closed by a battery cover, not shown, typically sealed by heat welding for example, onto box 2.
  • the lugs are firmly interconnected by straps 11 and the straps are interconnected in pairs through orifices 10 by means of interconnecting bridges 12.
  • two adjacent straps interconnected by a bridge 12 are indicated by reference number 13 and two adjacent straps 11 not interconnected through partition 3 are indicated by reference number 14 in Figure 2.
  • Straps 11, 13 making a safe and reliable mechanical and electrical interconnection of the lugs are integral pieces of metal, obtained by die- casting, such as lead, through a corresponding orifice 10, as it is more clearly shown in Figure 3.
  • the battery assembly also includes a negative terminal 15 and a positive terminal 16 forming integral part of plate straps 11.
  • a cover, not shown, will be sealed onto box 2 as it is well known, with the cover having corresponding metal terminals to be connected to terminal 15 and 16.
  • the battery is manufactured, according to the invention, by a new method to which reference will be made below, in an apparatus, also according to one aspect of the invention, as illustrated in Figures 5 to 10.
  • the apparatus comprises a die-casting station generally indicated by reference number 17 in Figure 6.
  • Station 17 comprises at least one mould 18, preferably two moulds 18, more clearly shown in the perspective view of Figure 5 and the cross sections of Figures 7-10.
  • a mould 18 is provided at each opposite side of the apparatus, and one mould is for receiving the positive plates of a cell and the other opposite mould is for receiving the negative plates of the same cell .
  • the plates are arranged in a manner that the positive plates of an element are adjacent to the negative plates of an adjacent element or cell.
  • Mold 18 comprises a mould body having a lower portion 19 with at least one inlet 20 for introducing the melting metal and an upper portion 21 having the element die sections, one of them indicated by a bracket and numeral reference 22.
  • Inlet 20 for the melting metal is connected to inner conduits 23 for conducting the melting metal into the element die sections.
  • Each element die section comprises a die sump 24 and a die channel 25 for receiving the plate lugs to be connected by the melting metal.
  • Die channel 25 and die sump 24 are both separated by an overflow wall, preferably a ramp-like wall 26.
  • Die sump 24 includes at least one inlet orifice 27. Orifices 27 are in fluid communication with conduits 23 for receiving the melting metal from the inner conduits 20 in the mould body. Thus, melting metal is received into die sump 24 in an amount that, when desired, it overflows the overflow wall 26 to be poured into die channel 25 when the plate lugs are placed into the die channel.
  • the die sumps comprise two end die sumps each one including a terminal well 28.
  • end sumps designed with wells 28 for forming terminals 15, 16.
  • end sumps may include only one orifice 27 as shown in Figure 8.
  • Element die sections 22 are separated by gaps 29 and each gap is designed for receiving one partition 3 as shown in Figure 7 in a manner that orifice 10 is accommodated in such a way that when the melting metal is poured into channel 25 it may flow through orifice 10 to interconnect adjacent element die sections 22 and elements 4 as shown in Figure 3.
  • interconnection through orifices 10 may be made at any level of partition 3, at or above straps 11, 13 , it is preferably that interconnections or bridges 12 are located above straps 11 in order to have a distance with the electrolyte in the battery in order to prevent any electrolyte from short circuiting the system by passing from one element to the adjacent one.
  • some gaps include an interconnecting well 30 having a bottom deeper than the bottom of adjacent die channels 25.
  • gaps including an interconnecting well 30 are alternated with gaps free of any interconnecting well.
  • the gaps of one mould including an interconnecting well are offset respective the gaps of the other mould including the interconnecting wells.
  • each gap has a width designed to fittingly receive a battery partition 3 in a sealing manner to prevent the melting metal from leaking out of the element die sections.
  • each gap has a depth designed to receive a battery partition 3 in a manner that orifice 10 of the partition remains placed to fluidly connect adjacent element die sections, either at the same level of straps 11 or alternatively in a manner that the orifice of the partition remains placed in the interconnecting well 30 to fluidly connect adjacent element die sections.
  • Body mould 18 may be made of any appropriate material, such as steel or any resin capable of resisting the temperatures employed in melting the metal, such as lead, at between 350 0 C - 450 0 C.
  • Heating and cooling means may be provided.
  • Heating means may comprise any typical resistance 31 or any other heat source such as vapour conduits and the like. These heating means, while illustrated only in the cross section of Figure 10, they may be arranged in any desired section according to the needs.
  • cooling means may comprise conduits 32 for circulating cooling water for example for cooling the lead into channel 25 to remove the battery once straps 11 are solidified.
  • the method for manufacturing the inventive battery comprises the steps of providing the battery box and inserting the battery plates into the elements of the battery box as it is shown in Figure 1. With all the plate packs inserted into the box, the battery box is inverted as shown in Figure 6 and then it is lowered onto a couple of moulds 18 in die-casting station 17. In such a manner, the lugs 8 and 9 are arranged into respective die channels 25 of molds 18 and partitions 3 are inserted into gaps 29 as shown in Figure 7. Thus, orifices 10 remain into corresponding interconnecting wells 30 in a way that each element die section 22 is fluidly communicated in pairs through corresponding orifices 10.
  • a melting metal preferably lead
  • inlet 20 conduits 23 and orifices 27 in order to fill up sumps 24.
  • the melting lead is over supplied in a manner that the lead overflows ramp wall 26 and pours into die channels 25.
  • the melting metal flows around lugs 8, 9, into channel 25, enters into interconnecting wells 30 and flow through orifices 10, forming a continuous strap a shown in Figure 3 , to mechanically and electrically connect the plate lugs.
  • the melting metal introduced into the element die sections receiving the positive battery plates is at a first higher temperature of 420 0 C and the melting metal introduced into the element die sections receiving the negative battery plates is at a second lower temperature of 380 0 C. These selected temperatures may be controlled by the heating means 31.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Connection Of Batteries Or Terminals (AREA)

Abstract

L'invention concerne une méthode pour interconnecter les cosses de plaques des éléments d'une batterie, la méthode comprenant le fait de retourner le boîtier de la batterie y compris les plaques à l'intérieur, d'insérer les cosses de plaques dans les sections de matrice correspondantes, d'introduire du plomb fondu dans la section de matrice pour connecter les cosses et de passer au travers des orifices correspondants dans les compartiments de la batterie pour interconnecter les cosses d'éléments adjacents. L'invention concerne également un appareil et la batterie réalisée.
EP06739824A 2006-03-28 2006-03-28 Méthode et apparail de fabrication d'un systeme de batterie Withdrawn EP2005501A4 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US2006/011261 WO2007111600A1 (fr) 2006-03-28 2006-03-28 méthode et appareil DE fabriCATION D'un SYSTEME DE batterie

Publications (2)

Publication Number Publication Date
EP2005501A1 true EP2005501A1 (fr) 2008-12-24
EP2005501A4 EP2005501A4 (fr) 2009-09-02

Family

ID=38541425

Family Applications (1)

Application Number Title Priority Date Filing Date
EP06739824A Withdrawn EP2005501A4 (fr) 2006-03-28 2006-03-28 Méthode et apparail de fabrication d'un systeme de batterie

Country Status (4)

Country Link
EP (1) EP2005501A4 (fr)
AR (1) AR060175A1 (fr)
BR (1) BRPI0621564A2 (fr)
WO (1) WO2007111600A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007063190B4 (de) * 2007-08-06 2013-08-29 Daimler Ag Batterie, bestehend aus mehreren Einzelzellen, insbesondere für einen Hybridantrieb
CN110402501A (zh) * 2017-01-27 2019-11-01 Cps科技控股有限公司 电池带

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3703589A (en) * 1965-12-20 1972-11-21 Globe Union Inc Battery and method of making the same
US3988169A (en) * 1973-09-12 1976-10-26 Chloride Batteries Australia Limited Method of molding connectors in electrical accumulators
US4108417A (en) * 1975-07-30 1978-08-22 Dale Products, Inc. Battery post and connector strap mold
US4327890A (en) * 1977-11-10 1982-05-04 Mac Engineering Battery strap and post cast-on multi use mold
JPH06236753A (ja) * 1993-02-10 1994-08-23 Shin Kobe Electric Mach Co Ltd 蓄電池用極板群のストラップ形成方法
US20020194715A1 (en) * 2001-06-22 2002-12-26 Watters Jimmy H. Method and apparatus for manufacturing battery plates

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3451142B2 (ja) * 1994-11-18 2003-09-29 本田技研工業株式会社 温度制御機構を備えたバッテリ組立体
US5836371A (en) * 1996-12-30 1998-11-17 Gnb Technologies, Inc. Method and apparatus for attaching terminal post straps to a battery plate group
US5885731A (en) * 1997-04-29 1999-03-23 Enersafe Corp. Weldless battery using cover as mold to cast plate straps, through the partition connections and terminals

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3703589A (en) * 1965-12-20 1972-11-21 Globe Union Inc Battery and method of making the same
US3988169A (en) * 1973-09-12 1976-10-26 Chloride Batteries Australia Limited Method of molding connectors in electrical accumulators
US4108417A (en) * 1975-07-30 1978-08-22 Dale Products, Inc. Battery post and connector strap mold
US4327890A (en) * 1977-11-10 1982-05-04 Mac Engineering Battery strap and post cast-on multi use mold
JPH06236753A (ja) * 1993-02-10 1994-08-23 Shin Kobe Electric Mach Co Ltd 蓄電池用極板群のストラップ形成方法
US20020194715A1 (en) * 2001-06-22 2002-12-26 Watters Jimmy H. Method and apparatus for manufacturing battery plates

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO2007111600A1 *

Also Published As

Publication number Publication date
BRPI0621564A2 (pt) 2016-08-16
WO2007111600A1 (fr) 2007-10-04
EP2005501A4 (fr) 2009-09-02
AR060175A1 (es) 2008-05-28

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