EP1556708A1 - Method and apparatus for diagnosis injectors - Google Patents
Method and apparatus for diagnosis injectorsInfo
- Publication number
- EP1556708A1 EP1556708A1 EP02808107A EP02808107A EP1556708A1 EP 1556708 A1 EP1556708 A1 EP 1556708A1 EP 02808107 A EP02808107 A EP 02808107A EP 02808107 A EP02808107 A EP 02808107A EP 1556708 A1 EP1556708 A1 EP 1556708A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- injector
- tester
- coil
- signal
- voltage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 12
- 238000003745 diagnosis Methods 0.000 title description 4
- 239000000446 fuel Substances 0.000 claims abstract description 37
- 238000012545 processing Methods 0.000 claims description 38
- 238000013500 data storage Methods 0.000 claims description 23
- 230000004044 response Effects 0.000 claims description 3
- 238000002485 combustion reaction Methods 0.000 abstract description 4
- 239000000523 sample Substances 0.000 description 13
- 238000012360 testing method Methods 0.000 description 7
- 238000002347 injection Methods 0.000 description 5
- 239000007924 injection Substances 0.000 description 5
- 230000015654 memory Effects 0.000 description 5
- 230000002159 abnormal effect Effects 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000010835 comparative analysis Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R31/00—Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
- G01R31/34—Testing dynamo-electric machines
- G01R31/346—Testing of armature or field windings
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02M—SUPPLYING COMBUSTION ENGINES IN GENERAL WITH COMBUSTIBLE MIXTURES OR CONSTITUENTS THEREOF
- F02M65/00—Testing fuel-injection apparatus, e.g. testing injection timing ; Cleaning of fuel-injection apparatus
Definitions
- the disclosure generally relates to a method and apparatus for determining operational status of a coil, and more specifically, to a fault detection method and apparatus for evaluating fuel injectors having an injector coil based on signals obtained during the operations thereof.
- An internal combustion engine employs various numbers of fuel injectors for supplying fuels.
- Electronic fuel injectors are the most commonly used fuel injectors for non-diesel engines.
- An electronic fuel injector may include a plurality of electromagnetically actuated fuel injection valves that are sequentially charged with a determinable quantity of fuel during a fuel metering interval and which during a subsequent interval are caused to inject fuel into the engine.
- Fig. 1 is an exemplary circuit for controlling the operation of a fuel injector.
- An injector coil 10 such as a solenoid coil, is disposed associating with each injection valve, and is used to control the opening/closing thereof.
- the injector coil 10 is coupled to a voltage source 12 on one end and to a switch 14 on the other end.
- the switch 14 controls the coupling of the injector coil 10 to the ground.
- the on/off of the switch is controlled by a controller or processor, such as a PCM (powertrain control module), ECU (electronic control unit), or ECM (electronic control module).
- PCM powertrain control module
- ECU electronic control unit
- ECM electronic control module
- the current energizes the injector coil, or, produces a magnetic field, that activates the pintle on one of the injection valves to allow fuel to be injected through a valve opening into the combustion chamber of a cylinder.
- switch 14 When switch 14 is open, no current flows through the injector coil 10. The pintle thus returns to its original position and closes the injector valve.
- This disclosure describes a method and apparatus for conveniently diagnosing fuel injectors having an injector coil and a power source that charges the injector coil during an energizing period.
- An exemplary tester monitors signals from the fuel injectors. The tester diagnoses the fuel injectors based on the monitored signals.
- the tester includes a data port for receiving signals, a data storage device, and a data processing unit coupled to the data port and the data storage device.
- the data storage device bears instructions to cause the tester upon execution of the instructions by the data processing unit to receive a first signal representing a first energizing state of the injector coil during the energizing period and a second signal representing a second energizing state of the injector coil during the energizing period.
- the data processing unit determines a first operational status of the injector based on a level difference between the first energizing state and the second energizing state.
- the first and second signals represent voltages of the injector coil during a period that the voltage source sends current to the injector coil.
- the signals may be obtained before or during the conduction of the diagnosis of the injector.
- the signals may be stored in the data storage device and accessible by the data processing unit.
- the data processing unit calculates a difference between the first and second signal, and determines whether the difference falls between a predetermined range. If the difference is outside the predetermined range, the tester indicates that the injector coil has a high resistance.
- the tester may be further configured to determine a second operational status of the injector based on levels of at least one of the first energizing state and the second energizing state.
- the data processing unit may access data representing injector voltages obtained during the time that the voltage source sends current to the injector coil, and determines whether the injector voltage is lower than a threshold voltage, for example, a voltage near zero volt. If the injector voltage is higher than the threshold voltage, the tester indicates that the injector coil having an unacceptable resistance. For example, the tester may indicate the injector coil as shorted or partially shorted.
- FIG. 1 is an exemplary circuit for controlling the operation of a fuel injector
- FIG. 2 shows a waveform of the voltage of an injector coil relative to the ground displayed on an oscilloscope under a large scale
- Fig. 3 depicts the same injector voltage shown in Fig. 2, but under a microscopic scale
- FIGS. 4a and 4b are injector voltage waveforms obtained from two injectors, one has normal resistance, while the other has a resistance higher than that of a normal injector;
- FIGS. 5a-5b show injector voltage waveforms obtained from two injectors, one has normal resistance, while the other has a resistance lower than a normal injector;
- FIG. 6 shows an exemplary tester used to carry out fuel injector diagnoses
- FIG. 7 is a flow chart showing steps of an exemplary diagnosis.
- FIG. 8 is a flow chart showing steps of another embodiment in diagnosing an injector coil using an exemplary tester.
- An exemplary tester for conveniently diagnosing injectors having an injector coil is disclosed.
- the tester determines various operational statuses of the injector based on signals generated thereby.
- One of the signals used by the tester is the voltage of the injector coil relative to the ground.
- Fig. 2 shows a waveform of the signal displayed on an oscilloscope under a large scale, such " as a 50 volt scale.
- the injector coil voltage represents the energizing status of the injector coil, and may be measured at any point between the injector coil and the switch, or at any other equivalent points that are known to people skilled in the art to determine the energizing status of the injector coil.
- the voltage waveform of Fig. 2 is obtained from point A in Fig. 1.
- FIG. 2 The waveform in Fig. 2 includes five zones: zone A, B, C, D and E, although zones B and D cover only a very short period of time.
- zone A switch 14 is open and no current flows through injector coil 10.
- the measured injector voltage is about the same as that of voltage source 12.
- zone B a control signal from the ECU or PCM closes switch 14, which pulls the injector voltage to near ground.
- Current starts to flow through injector coil 10 and voltage source 12 starts to energize injector coil 10.
- the current flowing through injector coil 10 increases steadily in zone C and approaches a saturated current level.
- Zone C is usually referred to as the energizing period.
- a control signal from the controller or data processor opens switch 14. Current stops flowing through injector coil 10. The magnetic field built by the injector coil thus collapses. Energy built up in injector coil 10 is released as a voltage pulse inductive kick exceeding the level of voltage source 12. At this point, the magnetic field weakens and is no longer sufficient to activate the pintle. In zone E, the pintle is released. The mechanical movement of the pintle relative to the coil causes the voltage hump in zone E.
- the waveform shown in Fig. 2 is observed using a large voltage scale ranging from 0-75 volts. Under such observation scale, when injector coil 10 is being energized in zone C, the injector voltage appears to be constant. However, when the waveform is observed in a microscopic scale, such as around 0.00 volt to 2.00 volt level, the waveform in zone C shows different characteristics.
- Fig. 3 shows a waveform of the same injector voltage as shown in Fig.
- Zone C in Fig. 3 is comparable to zone C of Fig. 2, which corresponds to the injector voltage when the injector coil is being energized. Although zone C in Fig. 1 shows a nearly constant voltage level, zone C in Fig. 3, on the other hand, shows that the injector voltage in fact changes with time when the injector coil is being energized. The tester determines the operational status of the injector based on characteristics of the injector voltage obtained when the injector is being energized.
- Figs. 4a and 4b depict injector voltage waveforms obtained from two injectors from the same vehicle respectively.
- the injector of Fig. 4a has a high resistance, while the injector of Fig. 4b is normal.
- Two sample voltages, VT1 and VT2 are obtained during a period when the injector coil is being energized.
- VT1 is sampled within 200 ms after the injector coil starts being energized
- VT2 is sampled within 200 ms before the injector coil stops being energized.
- the voltage difference between VT2 and VT1 is defined as " ⁇ V.”
- the tester can determine whether the injector has a normal or high resistance based on the value of ⁇ V.
- ine tester receives voltage signals from the * ihje ' cfof ' by ''' means ' of " a signal probe coupled thereto and determines ⁇ V for the injector accordingly.
- the tester determines if ⁇ V of the injector falls within a predetermined voltage range corresponding to the vehicle model or injector type under test.
- the predetermined voltage range corresponding to each vehicle model and/or injector type can be obtained empirically.
- the value ranges can be stored in a data storage device of the tester. For example, a predetermined
- the data processing unit determines that the injector under test has an abnormal injector. On the other hand, if ⁇ V falls within the predetermined voltage range, the data processing unit indicates that the injector resistance may be acceptable. The determination result may be sent to a monitor for display.
- Figs. 5a shows a voltage waveform of an injector having a resistance lower than normal
- Fig. 5b depicts a voltage waveform of a normal injector.
- the waveform in Fig. 5a appears to have an acceptable ⁇ V, unlike the normal waveform in Fig. 5b, the waveform in Fig. 5a does not pull the signal all the way to near the ground.
- the level of the injector voltage obtained when the injector coil is being energized is an indication of whether the injector has a resistance smaller than that of a normal injector.
- the tester samples two injector voltages, VT1 and VT2.
- VT2 to calculate ⁇ V during a period when the injector coil is being energized.
- the same sampled voltages can be used to determine whether the injector has a resistance lower than that of a normal injector.
- VT1 is used. If VT1 is greater than a predetermined voltage value, then the tester determines that the injector under test has a resistance smaller than that of a normal injector. In one embodiment, the tester indicates that the injector is shorted or nearly shorted. Otherwise, the injector is considered to have a normal resistance.
- the predetermined voltage value used to determine the status of the injector may vary from vehicle model to vehicle model, and from injector type to injector type.
- the predetermined values for different vehicle models or injector types can be determined empirically and stored in the tester. For a typical SFI (Sequential
- Fuel hijection) injector having a resistance ranging from 10 ⁇ to 20 ⁇ , the
- predetermined value may be set at 0.5 volt.
- the injector voltages during which the injector coil is being energized mayjrieed
- VT2 - VT1 V, wherein V falls between 0.15 volts - 0.85 volts
- injector voltage variations may also be used to evaluate the operational status of an injector. For example, the rate of voltage change during the energizing period may be used and compared with a threshold value or value range. The threshold values or value ranges corresponding to different vehicle models or injector types may be obtained empirically. Other methods based on injector voltage variations may also be adopted without departing from the broader spirit and scope of the disclosure.
- Fig. 6 shows an exemplary tester 60 used to carry out fuel injector diagnoses as described above.
- the tester may be a stand-alone tester or part of an onboard vehicle computer.
- the tester 60 includes a data port 61 for receiving signals, a data storage device 62 for storing data and instructions, and a data processing unit 63 coupled to the data port 61 and the data storage device 62.
- the tester may include a display 64, such as a monitor or LCD (Liquid Crystal Display), and an input device 65, such as a keyboard, mouse, push buttons, touch screen panels or voice control devices, for providing a user interface to communicate with an operator of the tester 60.
- a display 64 such as a monitor or LCD (Liquid Crystal Display)
- an input device 65 such as a keyboard, mouse, push buttons, touch screen panels or voice control devices, for providing a user interface to communicate with an operator of the tester 60.
- the data processing unit 63 is configured to perform numerous tasks by executing machine-readable instructions, such as processing signals, calculating signal levels, providing a user interface to the operator, displaying instructions and diagnostic results, and receiving commands from the operator, etc.
- the data port 61 includes one or more data channels for connecting to sensors, signal probes and/or peripheral devices. Various types of data channels may be implemented, such as USB ports, PS/2 ports, serial ports, parallel ports, LEEE-1394 ports, infra red communication ports, proprietary ports, and/or network connectors 66 for connecting to a remote computer 75 via a data transmission network 70. Signals received from the data port 61 are coupled to the data processing unit 63 and data storage device 62 for storage and or processing.
- the data storage device may include volatile and/or non-volatile memories.
- Volatile memories 67 include a random access memory (RAM) or other dynamic storage device for storing information and instructions to be executed by the data processing unit. Volatile memories 67 also may be used for storing voltage readings, temporary variables or other intermediate information during execution of instructions to be executed by the data processing unit.
- Non-volatile memories 68 may include read only memories (ROM), hard disks, CD-ROM, DVD-ROM or other static storage devices for storing static information and instructions.
- the data storage device 62 may read data and/or instructions from machine readable media (not shown) including, for example, a floppy disk, a flexible disk, hard disk, magnetic tape, or any other magnetic medium, a CD-ROM, any other optical medium, punch cards, paper tape, any other physical medium with patterns of holes, a RAM, a PROM, and EPROM, a FLASH-EPROM, any other memory chip or cartridge, or any other medium from which a data processing system can read.
- machine readable media including, for example, a floppy disk, a flexible disk, hard disk, magnetic tape, or any other magnetic medium, a CD-ROM, any other optical medium, punch cards, paper tape, any other physical medium with patterns of holes, a RAM, a PROM, and EPROM, a FLASH-EPROM, any other memory chip or cartridge, or any other medium from which a data processing system can read.
- the tester 60 is controlled in response to the data processing unit 63 executing one or more sequences of one or more instructions contained in the data storage device 62. Such instructions may be read into one type of memory device from another machine-readable medium. Execution of the sequences of instructions causes the tester 60 to perform the process as described herein. In alternative embodiments, hard-wired circuitry may be used in place of or in combination with software instructions to implement the disclosure. [0038] In one embodiment, upon the control ' of the Instructions, the tester 6U receives voltage signals from a signal probe coupled to an injector to obtain signals representing injector voltages. Numerous voltage signals may be sampled and stored in the data storage device.
- the sampled signals include at least a first injector voltage and a second injector voltage obtained during a period when the voltage source sends currents to the injector coil.
- the sample signals may include, for example, VT1 and VT2 as shown in Figs. 4a and 4b.
- the tester 60 determines whether the injector has a resistance higher than that of a normal injector based on the voltage difference between VT1 and VT2 ( ⁇ V), as discussed earlier.
- the tester 60 may separately determine whether the injector has a resistance lower than that of a normal injector based on an injector voltage obtained during a period during which the voltage source sends current to the injector coil, as discussed earlier.
- the data processing unit may, for example, compare VT1 with a threshold value stored in the data storage device 62, or obtained from a remote computer 75 connecting to the tester via a data transmission network 70.
- Using voltage signals to determine the operational status is more convenient than using current signals because there is no need to hook up a cumbersome current probe either intrusively or non-intrusively.
- the voltage signals can be obtained with simple voltage access points near the PCM or ECU that controls the injector.
- Fig. 7 is a flow chart showing steps of diagnosing an injector coil using an exemplary tester as described above.
- a user first connects a voltage probe of the tester to point A as shown in Fig. 1 (step 701).
- the tester obtains injector voltage waveforms during the operation of the vehicle (Step 703).
- the tester identifies sample voltage signals VT1 and VT2 (Step 705).
- the tester compares VT1 with a first threshold value, such as 0.5 volt (Step 707): If Vf ⁇ is larger than "' the " ' fifst threshold value, the tester determines that injector coil has a resistance smaller than that of a normal injector (Step 09).
- the tester continues to calculate the voltage difference ⁇ V between VT1 and VT2 (Step 711).
- the tester compares ⁇ V with a second threshold value, such as 0.15 volt to determine whether the injector coil has a resistance higher than an acceptable level (step 713). If the ⁇ V is smaller than the predetermined value, then the tester indicates that the injector coil has a resistance larger than that of a normal injector (step 715). Otherwise, the tester indicates that the injector coil is normal (Step 717).
- a second threshold value such as 0.15 volt
- Fig. 8 is a flow chart showing steps of another embodiment in diagnosing an injector coil using an exemplary tester as described above.
- the tester obtains injector voltage waveforms.
- the user verifies if there is a normal voltage source. For a vehicle using an injector having a resistance ranging
- the voltage source ranges from 13.2 volt to 14.6 volt. If the voltage
- step 821 If the voltage source is not stable or if the voltage source is not within the normal voltage range, the user needs to check and repair the voltage source, such as fixing open voltage source or open circuit problem, if required (step 821).
- the tester determines if the ECU/PCM energizes the injector by turning the injector on or off regularly (step 805). If not, the tester may alert the user to verify the reasons. There are a number of reasons that the ECU/PCM does not turn on and off the injector even with a normal voltage source. For example, a fault in the anti-theft system, no rpm signal, " ef c. " " The mos ' t ' c ⁇ mm ⁇ n reasons for a specific injector driver to fail to operate consistently are either a bad ECU/PCM injector driver, or a shorted injector.
- a shorted injector may be the cause of the damaged ECU/PCM injector driver. After the shorted injector and/or its circuit is repaired, many times the PCM/ECU works normally. This is because the PCM/ECU shuts off a specific injector driver to protect each individual transistorized injector driver.
- step 805 the tester determines that the ECU/PCM energize the injector properly, the tester retrieves sample voltages VTl and VT2 and calculates ⁇ V based on VTl and VT2 (step 807).
- step 811 the tester compares VTl with a first threshold value, such as 0.5 volt. If VTl is larger than the first threshold value, the tester alerts the user to check the PCM/ECU power ground. If the ground condition is normal, the injector will indicate that the injector coil has a resistance smaller than that of a normal injector (Step 825). The tester may alert the user to check and replace the injector coil.
- a first threshold value such as 0.5 volt.
- step 811 determines that VTl is smaller than the first threshold value
- the tester compares ⁇ V with a second threshold value, such as 0.85 volt to determine whether the injector coil has a resistance higher than an acceptable level (step 813). If ⁇ V is greater than the second threshold value, then the tester indicates that the injector circuit has a low resistance i.e. short or partially shorted injector/circuit (step 827).
- the tester determines if ⁇ V is less than a third threshold value, such as 0.15 volt (step 815). If ⁇ V is less than the third threshold value, the tester indicates that a high resistance exists in the injector circuit (step 829). The tester may alert the user to check resistance of injector manually. The resistance should not be more than 20 ohm. Otherwise, a replacement of the injector coil is required. The tester may also alter the user to check injector harness connections because many times a high resistance may be caused by corrosion at the injector terminal connections. [0048] If, in step 815, the tester determines that ⁇ V is greater than the third threshold value, the tester then determines that the injector has an acceptable resistance (step 817).
- a third threshold value such as 0.15 volt
- the tester may alert the user to conduct a manual comparative analysis on the injector to determine if the injector has a normal resistance. For example, in the case where that ⁇ V falls within 20% of the threshold values, the tester generates a message indicating a manual test on the injector's resistance may be necessary.
- the same technique may also apply to determinations of VTl or other signals with threshold values.
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Fuel-Injection Apparatus (AREA)
- Electrical Control Of Air Or Fuel Supplied To Internal-Combustion Engine (AREA)
Abstract
Description
Claims
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/US2002/035088 WO2004042412A1 (en) | 2002-11-01 | 2002-11-01 | Method and apparatus for diagnosis injectors |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP1556708A1 true EP1556708A1 (en) | 2005-07-27 |
Family
ID=32311625
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP02808107A Withdrawn EP1556708A1 (en) | 2002-11-01 | 2002-11-01 | Method and apparatus for diagnosis injectors |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP1556708A1 (en) |
| JP (1) | JP2006504900A (en) |
| CN (1) | CN1695063A (en) |
| AU (1) | AU2002368328A1 (en) |
| CA (1) | CA2502110A1 (en) |
| WO (1) | WO2004042412A1 (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9429126B2 (en) * | 2014-06-05 | 2016-08-30 | Caterpillar Inc. | System and method for detecting short-to-ground fault |
| US10161340B1 (en) * | 2017-10-02 | 2018-12-25 | GM Global Technology Operations LLC | Fuel injection system and method for a vehicle propulsion system |
| CN107782563A (en) * | 2017-10-18 | 2018-03-09 | 重庆市弘鼎圣科技有限公司 | Car fault auto-detecting system |
| US12136160B2 (en) | 2022-04-27 | 2024-11-05 | Snap Inc. | Augmented reality experience power usage prediction |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2231630A1 (en) * | 1972-06-28 | 1974-01-17 | Volkswagenwerk Ag | PROCEDURE AND EQUIPMENT FOR THE FUNCTIONAL CHECK OF AN ELECTROMAGNETIC VALVE, IN PARTICULAR A FUEL INJECTION VALVE |
| JPH0392542U (en) * | 1990-01-12 | 1991-09-20 | ||
| DE19738967B4 (en) * | 1997-09-05 | 2007-09-06 | Schleich Antriebs- Und Steuerungstechnik Gmbh | Method for testing the function of an electric coil |
-
2002
- 2002-11-01 WO PCT/US2002/035088 patent/WO2004042412A1/en not_active Ceased
- 2002-11-01 CA CA002502110A patent/CA2502110A1/en not_active Abandoned
- 2002-11-01 AU AU2002368328A patent/AU2002368328A1/en not_active Abandoned
- 2002-11-01 CN CN02829839.XA patent/CN1695063A/en active Pending
- 2002-11-01 JP JP2004549814A patent/JP2006504900A/en not_active Withdrawn
- 2002-11-01 EP EP02808107A patent/EP1556708A1/en not_active Withdrawn
Non-Patent Citations (1)
| Title |
|---|
| See references of WO2004042412A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2004042412A1 (en) | 2004-05-21 |
| JP2006504900A (en) | 2006-02-09 |
| AU2002368328A1 (en) | 2004-06-07 |
| WO2004042412A9 (en) | 2004-10-28 |
| CN1695063A (en) | 2005-11-09 |
| CA2502110A1 (en) | 2004-05-21 |
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