EP1286805A1 - Friction stir spot welding method and apparatus - Google Patents
Friction stir spot welding method and apparatusInfo
- Publication number
- EP1286805A1 EP1286805A1 EP00970327A EP00970327A EP1286805A1 EP 1286805 A1 EP1286805 A1 EP 1286805A1 EP 00970327 A EP00970327 A EP 00970327A EP 00970327 A EP00970327 A EP 00970327A EP 1286805 A1 EP1286805 A1 EP 1286805A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- shoulder
- pin
- friction stir
- welding
- members
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000003466 welding Methods 0.000 title claims abstract description 41
- 238000003756 stirring Methods 0.000 title claims abstract description 23
- 238000000034 method Methods 0.000 title claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 15
- 239000000523 sample Substances 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 230000035515 penetration Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000001965 increasing effect Effects 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K20/00—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
- B23K20/12—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating the heat being generated by friction; Friction welding
- B23K20/122—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating the heat being generated by friction; Friction welding using a non-consumable tool, e.g. friction stir welding
- B23K20/1245—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating the heat being generated by friction; Friction welding using a non-consumable tool, e.g. friction stir welding characterised by the apparatus
- B23K20/125—Rotary tool drive mechanism
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K20/00—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
- B23K20/12—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating the heat being generated by friction; Friction welding
Definitions
- the present invention relates to a new improved method of friction stir welding of members, more particularly to a spot welding method, and furthermore to apparatuses to conduct such method.
- Friction stir welding is a new friction welding process representing a disruptive welding technology.
- the principles of the process and applied apparatus disclosed by WO93/10935 are based on a relative cyclic movement between a non- consumable probe of a harder material than the workpieces to be joined and the workpieces. Urging the rotating probe into the assembled adjacent workpieces along their joining line creates a plasticized region in the workpieces due to a generated frictional heat. Thus no heat is generated as in conventional friction stir welding due to a relative motion between the workpieces to be joined.
- This new welding method having the advantage of solid state bonding, has been successfully implemented on providing plate and profile seam joints not previously feasible and gains increasing popularity for numerous joining applications.
- Another object of the present invention is to provide improved modifications of friction stir welding apparatuses ensuring a substantial keyhole filling during/after the probe's retraction from the joined members.
- Fig. 1 illustrates schematically the novel principle of the improved friction stir welding by means of controlled and variable forces (exercised in the joined-to-be members).
- Fig. 2 shows schematically in a vertical cross-sectional view a construction principle of the applicable friction stir welding apparatus.
- Fig. 3 shows schematically in a vertical cross-sectional view another variant of the friction stir welding apparatus.
- the friction stir welding as described in WO93/10935 is incorporated herein by reference to the extent consistent with the present invention.
- Fig. 1 the principle of the novel friction stir welding based on a shoulder being movable independently of the pin and exercising controlled and variable (down) forces on the pre-assembled joined-to-be members is illustrated schematically as steps 1a-1 e in the basic welding cycle.
- a motor driven rotating cylindrical pin 1 is mounted in a rotating cylindrical shoulder 2 with the pin being movable along their combined central axis (from hereon denominated z-axis) independently of the shoulder during the welding cycle.
- the movement of the pin along the z-axis is controlled by an actuator (not shown in the Figure), the actuator being e.g. a milling machine, friction stir welding machine, arm of a welding robot, a hand held machine or any other applicable means.
- the movement of the shoulder along the z-axis is force controlled during the welding cycle.
- the shoulder's z-axis rotation velocity and direction can be chosen independently from the pin or be identical.
- An extra containment shoulder 21 encompassing the shoulder 2 independent of said shoulder's z-axis rotation can be an option to aid refilling of the keyhole.
- the pin itself can be either smooth, have a modified surface, or have a reverse pitch with regard to its direction of rotation; thus further enhancing the refilling of the keyhole.
- the basic welding cycle contains the following steps as shown in Figure 1 :
- Step b Penetration
- an extra containment shoulder 21 shown schematically co-axially arranged to and enveloping the shoulder 2, is lowered down to the surfaces of members A,B.
- the function of the containment shoulder 21 is to keep the excessive upcoming material under the shoulder 2 also during the following steps c and d.
- Step d Retracting
- Step e illustrates the completion of the welding cycle showing substantially reduced volume of the hole 10 by a simple "plunge/lift” operation of the tool keeping the shoulder under down force.
- Figure 2 illustrates in a cross-sectional view the apparatus for making friction stir welds with force controlled shoulder and friction stir welded spot welds in a simple form, having the shoulder 2 and pin 1 rotating at the same rotational velocity. The apparatus can also make shoulder down force controlled butt welds.
- the apparatus comprises conventionally a frame 5 that is mountable at the end of e.g. a robot arm (not shown in the Figure), milling machine, friction stir welding machine or any other applicable means.
- a hand held variant might also be viable.
- power source e.g. a motor 4
- the friction stir weld pin either with or without reversed thread pitch is fixed, thus rotating at motor speed.
- the shoulder 2 is constructed in such a manner that it has a loose splined fit with tool holder 3 and pin 1 and therefore can slide along the z-axis over the tool holder, while the rotational velocity of the shoulder is identical to that of tool holder and pin.
- Other means for restriction of the rotational freedom e.g.
- the shoulder is mounted inside an axial truss bearing 7 which is mounted in a hollow piston 9, the piston being part of a hollow hydraulic or pneumatic actuator, thus ensuring the down force control over the shoulder.
- Other means of actuation are conceivable/applicable.
- the frame 5 contains two motors, the top motor 4 having an axle going through the hollow axle of the bottom motor 4' and driving the tool holder 3 through an extension.
- the shoulder extension in itself forms a hollow axis 8 and can slide in the hollow motor axle 10 with a loose splined fit.
- the shoulder z-axis rotational degree of freedom is now constricted, effectively making the shoulder rotate with the same velocity as the hollow axle of the bottom motor. Only loose fit between shoulder and tool holder is now present, thus ensuring additionally z-axis rotational degree of freedom between these two.
- the constraining shoulder can typically for both principles be spring loaded and attached to the cover plate 11 of the piston.
- An obvious advantage of the independently rotating pin and shoulder is to separate function of heat input from the shoulder and the induced deformation by the pin rotation, which are both a function of their rotational velocity. This means more flexibility and better control with regard to the welding process parameters. Furthermore, the automatic positioning of the shoulder on the welded members will also cope with the thickness variations in the weld members ensuring uniform seam welds of improved quality when applied on butt welded members.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Pressure Welding/Diffusion-Bonding (AREA)
Abstract
Modified method for friction stir welding process where the shoulder (2) being independently movable of the pin (1) exercises controlled and variable forces on the assembled joined-to-be members so that the down force under retraction of the pin exceeds the plasticity limit of excess material collected under the shoulder.
Description
"Fricition stir spot welding method and apparatus"
The present invention relates to a new improved method of friction stir welding of members, more particularly to a spot welding method, and furthermore to apparatuses to conduct such method.
Friction stir welding is a new friction welding process representing a disruptive welding technology. The principles of the process and applied apparatus disclosed by WO93/10935 are based on a relative cyclic movement between a non- consumable probe of a harder material than the workpieces to be joined and the workpieces. Urging the rotating probe into the assembled adjacent workpieces along their joining line creates a plasticized region in the workpieces due to a generated frictional heat. Thus no heat is generated as in conventional friction stir welding due to a relative motion between the workpieces to be joined. This new welding method, having the advantage of solid state bonding, has been successfully implemented on providing plate and profile seam joints not previously feasible and gains increasing popularity for numerous joining applications.
However, provision of so-called keyholes resulting from retraction of the probe by termination of the welding requiring normally removal of such inadequately filled part of the seam weld represents certain limitations to even broader applications.
Thus, e.g. in spot welding processes being presently extensively applied in robotazing of assembling operations in vehicle building (welding of steel sheets to the supporting structure of the vehicle body), the use of aluminium as sheet material has so far been eliminated due to the low strength joints resulting from classical Al-welding methods (TIG, MIG).
Drawbacks linked to the presently known/applied friction stir welding apparatuses - large down load forces on the welded members and presence of keyholes - have so far eliminated possible application of friction stir welding technology in this field.
It is therefore an object of the present invention to provide a novel improved method of friction stir welding providing a weld avoiding the above difficulties connected to the existence of the keyholes.
Another object of the present invention is to provide improved modifications of friction stir welding apparatuses ensuring a substantial keyhole filling during/after the probe's retraction from the joined members.
These and other objects are met by provision of a novel modified friction stir welding method and novel apparatus as defined in the attached patent claims 1 and 4, respectively.
Other objects, specific features and advantages of the present invention will become apparent from the following detailed description of the preferred embodiments of the apparatus and the mode of operation according to the invention with reference to the accompanying drawings, Figs. 1 -3, where
Fig. 1 illustrates schematically the novel principle of the improved friction stir welding by means of controlled and variable forces (exercised in the joined-to-be members).
Fig. 2 shows schematically in a vertical cross-sectional view a construction principle of the applicable friction stir welding apparatus.
Fig. 3 shows schematically in a vertical cross-sectional view another variant of the friction stir welding apparatus.
The friction stir welding as described in WO93/10935 is incorporated herein by reference to the extent consistent with the present invention.
Referring to Fig. 1 , the principle of the novel friction stir welding based on a shoulder being movable independently of the pin and exercising controlled and variable (down) forces on the pre-assembled joined-to-be members is illustrated schematically as steps 1a-1 e in the basic welding cycle.
A motor driven rotating cylindrical pin 1 is mounted in a rotating cylindrical shoulder 2 with the pin being movable along their combined central axis (from hereon denominated z-axis) independently of the shoulder during the welding cycle. The movement of the pin along the z-axis is controlled by an actuator (not shown in the Figure), the actuator being e.g. a milling machine, friction stir welding machine, arm of a welding robot, a hand held machine or any other applicable means. The movement of the shoulder along the z-axis is force controlled during the welding cycle. The shoulder's z-axis rotation velocity and direction can be chosen independently from the pin or be identical. An extra containment shoulder 21 encompassing the shoulder 2 independent of said shoulder's z-axis rotation can be an option to aid refilling of the keyhole. The pin itself can be either smooth, have a modified surface, or have a reverse pitch with regard to its direction of rotation; thus further enhancing the refilling of the keyhole.
The basic welding cycle contains the following steps as shown in Figure 1 :
Step a Initial contact
The rotating pin 1 is brought in contact with the to be welded members A,B, and a positive down force F1 is applied on the shoulder to get it in contact with the to be welded members. The pressure exerted by the shoulder is chosen to be less than the yield strength of the to be welded material. The shoulder can optionally rotate to give additional heat input to aid the plasticizing process.
Step b: Penetration
While the down force F1 on the shoulder is maintained (or eventually reduced), the rotating pin is moved into the to be welded components. Optionally an extra containment shoulder 21 , shown schematically co-axially arranged to and enveloping the shoulder 2, is lowered down to the surfaces of members A,B. The function of the containment shoulder 21 is to keep the excessive upcoming material under the shoulder 2 also during the following steps c and d.
Step c: Initial welding
While the down force F1 on the shoulder is maintained (or eventually reduced), penetration of the pin continues until the full penetration depth has been reached. In this step initial solid state bonding between the two components takes place. The material displaced by the pin is in this step moved upwards and collects under the shoulder, while the relative (vertical) position of the shoulder is dependent on/adapted to the actual amount/volume of the displaced material by the pin 1.
Step d: Retracting
While the pin is retracted, the down force on the shoulder F1 is increased to such an extent that the plasticity limits of the excessive material under the shoulder is exceeded. This will lead to back extrusion of excessive material along the perimeter of the pin into the gap occurring under the pin while retracting. This back extruded material is integrally bonded in the gap under the pin due to the deformation exerted on it by the rotating pin, effectively leaving a plugged up hole containing solid state bonded material when the retraction is complete. Thus the welding operation is accomplished without any lateral translation movement of the shoulder.
Step e illustrates the completion of the welding cycle showing substantially reduced volume of the hole 10 by a simple "plunge/lift" operation of the tool keeping the shoulder under down force.
Figure 2 illustrates in a cross-sectional view the apparatus for making friction stir welds with force controlled shoulder and friction stir welded spot welds in a simple form, having the shoulder 2 and pin 1 rotating at the same rotational velocity. The apparatus can also make shoulder down force controlled butt welds.
This "automatic" positioning of the shoulder on the surfaces of the joined-to-be members is possible due to the fact that no special positioning means are applied/ necessary according to the novel inventive construction principle of the tool.
The apparatus comprises conventionally a frame 5 that is mountable at the end of e.g. a robot arm (not shown in the Figure), milling machine, friction stir welding machine or any other applicable means. A hand held variant might also be viable. In the frame 5 power source, e.g. a motor 4, is mounted which axle is driving a tool holder 3. The friction stir weld pin, either with or without reversed thread pitch is fixed, thus rotating at motor speed. The shoulder 2 is constructed in such a manner that it has a loose splined fit with tool holder 3 and pin 1 and therefore can slide along the z-axis over the tool holder, while the rotational velocity of the shoulder is identical to that of tool holder and pin. Other means for restriction of the rotational freedom, e.g. a keyway solution, are also applicable. The shoulder is mounted inside an axial truss bearing 7 which is mounted in a hollow piston 9, the piston being part of a hollow hydraulic or pneumatic actuator, thus ensuring the down force control over the shoulder. Other means of actuation are conceivable/applicable.
An alternative construction apparatus having independently rotating pin and shoulder is shown in Figure 3.
In this case the frame 5 contains two motors, the top motor 4 having an axle going through the hollow axle of the bottom motor 4' and driving the tool holder 3 through an extension. The shoulder extension in itself forms a hollow axis 8 and can slide in the hollow motor axle 10 with a loose splined fit. The shoulder z-axis rotational
degree of freedom is now constricted, effectively making the shoulder rotate with the same velocity as the hollow axle of the bottom motor. Only loose fit between shoulder and tool holder is now present, thus ensuring additionally z-axis rotational degree of freedom between these two. The constraining shoulder can typically for both principles be spring loaded and attached to the cover plate 11 of the piston.
An obvious advantage of the independently rotating pin and shoulder is to separate function of heat input from the shoulder and the induced deformation by the pin rotation, which are both a function of their rotational velocity. This means more flexibility and better control with regard to the welding process parameters. Furthermore, the automatic positioning of the shoulder on the welded members will also cope with the thickness variations in the weld members ensuring uniform seam welds of improved quality when applied on butt welded members.
Other technical solutions to obtain independent z-axis rotational direction and velocity between pin and shoulder are possible within the scope of the invention.
Claims
1. Welding method for spot joining of assembled members, characterized in that the welding is conducted by a friction stir welding process applying shoulder and rotating pin where the shoulder is movable independently of the pin and exercises controlled predetermined and variable forces on the assembled joined-to-be members, wherein the down force on the shoulder under retraction of the pin exceeds the plasticity limit of excessive welded material collected under the shoulder, thereby forcing thus plasticized material downward under retraction of the pin.
2. Welding method according to claim 1 , characterized in that the shoulder and the pin rotate independently of each other.
3. Welding method according to claim 1 or 2, characterized in that the flow of the plasticized material is additionally controlled by the pin surface configuration adapted for reverse flow and compacting of the plasticized material.
4. Modified apparatus for friction stir welding comprising a shoulder (2) and rotating pin (1), the shoulder being provided with means (9) to exercise controlled and variable down forces F1 on the assembled joined-to-be members (A,B).
5. Apparatus according to claim 1 , characterized in that the pin (1) and the shoulder (2) are provided with separate power sources (4,4') ensuring their independent rotation. Apparatus according to claim 5 or 6, characterized in that a containment shoulder (21) is co-axially arranged enveloping the shoulder (2).
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO995093 | 1999-10-19 | ||
| NO995093A NO995093D0 (en) | 1999-10-19 | 1999-10-19 | Method and apparatus for spot welding |
| PCT/NO2000/000344 WO2001028732A1 (en) | 1999-10-19 | 2000-10-18 | Friction stir spot welding method and apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP1286805A1 true EP1286805A1 (en) | 2003-03-05 |
Family
ID=19903879
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP00970327A Withdrawn EP1286805A1 (en) | 1999-10-19 | 2000-10-18 | Friction stir spot welding method and apparatus |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP1286805A1 (en) |
| AU (1) | AU7972600A (en) |
| NO (1) | NO995093D0 (en) |
| WO (1) | WO2001028732A1 (en) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3400409B2 (en) * | 2000-04-28 | 2003-04-28 | マツダ株式会社 | Joining method and joining device |
| US6302315B1 (en) | 2000-05-01 | 2001-10-16 | General Tool Company | Friction stir welding machine and method |
| JP3429475B2 (en) | 2000-05-08 | 2003-07-22 | 川崎重工業株式会社 | Spot joining apparatus and spot joining method |
| JP3538406B2 (en) | 2001-10-17 | 2004-06-14 | 川崎重工業株式会社 | Friction stir welding equipment |
| US6732900B2 (en) | 2002-04-02 | 2004-05-11 | Mts Systems Corporation | Friction stir welding spindle with axially displaceable spindle shaft |
| US6913186B2 (en) | 2003-09-11 | 2005-07-05 | The Boeing Company | Apparatus and method for friction stir welding with a variable speed pin |
| US7641096B2 (en) | 2005-01-24 | 2010-01-05 | The Boeing Company | Friction stir welding apparatus |
| US8052030B2 (en) | 2005-01-24 | 2011-11-08 | The Boeing Company | Apparatus for friction stir welding using spindle-in-spindle |
| DE102005019758B4 (en) * | 2005-04-28 | 2007-12-13 | Hydro Aluminium Deutschland Gmbh | Method and apparatus for joining at least two components made of dissimilar materials |
| DE102005029882A1 (en) * | 2005-06-27 | 2006-12-28 | Gkss-Forschungszentrum Geesthacht Gmbh | Friction stir welding apparatus includes first inner segment surrounding a pin and having first friction surface segment surrounding the first inner segment and rotationally driven independently of the first inner segment |
| EP1884308B1 (en) * | 2006-08-04 | 2010-04-28 | Sumitomo Light Metal Industries, Ltd. | Method of friction stir welding together dissimilar metal members with a double acting rotary tool for filling of the hole created by the probe |
| US8141859B2 (en) | 2007-11-02 | 2012-03-27 | The Boeing Company | Apparatus and method for effecting pin-to-shoulder tool separation for a friction stir welding pin tool |
| WO2009109668A1 (en) | 2008-03-03 | 2009-09-11 | Fundacion Fatronik | Machine-tool for friction stir welding |
| JP2013522259A (en) | 2010-03-15 | 2013-06-13 | ロレアル | Composition containing dibenzoylmethane-based blocking agent and hydrophilic or water-soluble merocyanine-based UV blocking agent, and method for photostabilizing dibenzoylmethane-based blocking agent |
| US8961941B2 (en) | 2010-03-15 | 2015-02-24 | L'oreal | Composition comprising a dibenzoylmethane screening agent and a merocyanine dicyano or cyanoacetate derivative; method for the photostabilization of the dibenzoylmethane screening agent |
| JP5588385B2 (en) * | 2011-03-18 | 2014-09-10 | 川崎重工業株式会社 | Friction stir spot welding apparatus and friction stir spot welding method |
| JP5815961B2 (en) * | 2011-03-18 | 2015-11-17 | 川崎重工業株式会社 | Friction stir spot welding apparatus and friction stir spot welding method |
| CN102319952A (en) * | 2011-06-14 | 2012-01-18 | 兰州理工大学 | Spot welding method and device for light alloy-steel key-free hole stirring friction |
| DE102011111750B3 (en) * | 2011-08-24 | 2012-12-13 | Technische Universität München | Friction friction welding device and method for joining workpieces by means of a friction stir welding process |
| PT2596898E (en) | 2011-11-25 | 2015-01-14 | Helmholtz Zentrum Geesthacht Zentrum Für Material Und Küstenforschung Gmbh | Friction welding tool with a self-clamping device |
| CN103801817A (en) * | 2012-11-15 | 2014-05-21 | 上海航天设备制造总厂 | Double-speed rotating stirring tool for thick plate welding |
| EP3235585B1 (en) * | 2014-12-15 | 2021-01-20 | Kawasaki Jukogyo Kabushiki Kaisha | Friction stir spot welding device and friction stir spot welding method |
| JP2016128178A (en) * | 2015-01-09 | 2016-07-14 | 株式会社Ihi | Friction agitation joining device |
| US9915046B2 (en) | 2015-12-15 | 2018-03-13 | HFW Solutions, Inc. | Self alignment structure for applications joining extruded members |
| JP6796565B2 (en) * | 2017-09-08 | 2020-12-09 | 川崎重工業株式会社 | Double-acting friction stir welding point joining method |
| JP7173081B2 (en) * | 2020-04-08 | 2022-11-16 | Jfeスチール株式会社 | Friction stir welding method for aluminum alloy plate and steel plate |
| JP7487651B2 (en) * | 2020-12-04 | 2024-05-21 | 日本軽金属株式会社 | Rotation tool, joining device and joining method |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9125978D0 (en) * | 1991-12-06 | 1992-02-05 | Welding Inst | Hot shear butt welding |
| DE19630271C2 (en) * | 1996-07-26 | 2002-06-06 | Burkhardt Suthoff | Method for connecting a plasticizable workpiece to another workpiece |
| JP3897391B2 (en) * | 1997-03-25 | 2007-03-22 | 昭和電工株式会社 | Friction stir welding method for metal joining members |
-
1999
- 1999-10-19 NO NO995093A patent/NO995093D0/en unknown
-
2000
- 2000-10-18 WO PCT/NO2000/000344 patent/WO2001028732A1/en not_active Ceased
- 2000-10-18 EP EP00970327A patent/EP1286805A1/en not_active Withdrawn
- 2000-10-18 AU AU79726/00A patent/AU7972600A/en not_active Abandoned
Non-Patent Citations (1)
| Title |
|---|
| See references of WO0128732A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| AU7972600A (en) | 2001-04-30 |
| WO2001028732A1 (en) | 2001-04-26 |
| NO995093D0 (en) | 1999-10-19 |
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