EP0649458A4 - AQUEOUS LUBRICATION AND SURFACE CONDITIONING FOR MOLDED METAL SURFACES. - Google Patents

AQUEOUS LUBRICATION AND SURFACE CONDITIONING FOR MOLDED METAL SURFACES.

Info

Publication number
EP0649458A4
EP0649458A4 EP93916982A EP93916982A EP0649458A4 EP 0649458 A4 EP0649458 A4 EP 0649458A4 EP 93916982 A EP93916982 A EP 93916982A EP 93916982 A EP93916982 A EP 93916982A EP 0649458 A4 EP0649458 A4 EP 0649458A4
Authority
EP
European Patent Office
Prior art keywords
alkoxylated
process according
lubricant
aqueous solution
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP93916982A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP0649458A1 (en
Inventor
Sami B Awad
Timm L Kelly
Gary L Rochfort
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel Corp
Original Assignee
Henkel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel Corp filed Critical Henkel Corp
Priority to EP99203252A priority Critical patent/EP0969078A3/en
Publication of EP0649458A1 publication Critical patent/EP0649458A1/en
Publication of EP0649458A4 publication Critical patent/EP0649458A4/en
Withdrawn legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
    • C10M107/20—Lubricating compositions characterised by the base-material being a macromolecular compound containing oxygen
    • C10M107/30—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M107/32—Condensation polymers of aldehydes or ketones; Polyesters; Polyethers
    • C10M107/34—Polyoxyalkylenes
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    • C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
    • C10M125/18—Compounds containing halogen
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    • C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
    • C10M129/04—Hydroxy compounds
    • C10M129/06—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
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    • C10M129/08—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least 2 hydroxy groups
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    • C10M129/40—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 8 or more carbon atoms monocarboxylic
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    • C10M129/52—Carboxylic acids; Salts thereof having carboxyl groups bound to a carbon atom of a six-membered aromatic ring polycarboxylic
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/063—Complexes of boron halides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/065—Organic compounds derived from inorganic acids or metal salts derived from Ti or Zr
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/066—Organic compounds derived from inorganic acids or metal salts derived from Mo or W
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/30—Refrigerators lubricants or compressors lubricants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/32—Wires, ropes or cables lubricants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/34—Lubricating-sealants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/36—Release agents or mold release agents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/38—Conveyors or chain belts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/40—Generators or electric motors in oil or gas winning field
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/42—Flashing oils or marking oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/44—Super vacuum or supercritical use
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/50—Medical uses
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/01—Emulsions, colloids, or micelles

Definitions

  • This invention relates to processes and compositions which accomplish at least one, and most preferably all, of the following related objectives when applied to formed metal surfaces, more particularly to the surfaces of cleaned aluminum and/or tin plated cans: (i) reducing the coefficient of static friction of the treated surfaces after drying of such surfaces, without adversely affecting the adhesion of paints or lac ⁇ quers applied thereto; (ii) promoting the drainage of water from treated surfaces, without causing "water-breaks", i.e., promoting drainage that results in a thin, continuous film of water on the cans, instead of distinct water droplets separated by the relatively dry areas called "water-breaks" between the water droplets; and (iii) lowering the dryoff oven temperature required for drying said surfaces after they have been rinsed with water.
  • Aluminum cans are commonly used as containers for a wide variety of prod ⁇ ucts. After their manufacture, the aluminum cans are typically washed with acidic cleaners to remove aluminum fines and other contaminants therefrom. Environmental considerations and the possibility that residues remaining on the cans following acidic cleaning could influence the flavor of beverages packaged in the cans has led to an interest in alkaline or acid cleaning to remove such fines and contaminants.
  • cleaning of aluminum cans generally results in differential rates of metal surface etch on the outside versus on the inside of the cans. For example, optimum conditions required to attain an aluminum fine-free surface on the inside of the cans usually leads to can mobility problems on conveyors because of the increased roughness on the outside can surface.
  • Aluminum cans that lack a low coefficient of static friction (hereinafter often abbreviated as "COF") on the outside surface usually do not move past each other and through the trackwork of a can plant smoothly. Clearing the jams resulting from failures of smooth flow is inconvenient to the persons operating the plant and costly because of lost production.
  • COF of the internal surface is also important when the cans are processed through most conventional can decorators. The operation of these machines requires cans to slide onto a rotating mandrel which is then used to transfer the can past rotating cylinders which transfer decorative inks to the exterior surface of the cans. A can that does not slide easily on or off the mandrel can not be decorated properly and results in a production fault called a "printer trip".
  • the current trend in the can manufacturing industry is directed toward using thinner gauges of aluminum metal stock.
  • the down-gauging of alumi ⁇ num can metal stock has caused a production problem in that, after washing, the cans require a lower drying oven temperature in order to pass the column strength pressure quality control test.
  • lowering the drying oven temperature resulted in the cans not being dry enough when they reached the printing station, and caused label ink smears and a higher rate of can rejects.
  • One means of lowering the drying oven temperature would be to reduce the amount of water remaining on the surface of the cans after water rinsing.
  • it is advantageous to promote the drainage of rinse water from the treated can surfaces.
  • it is generally important to prevent the formation of surfaces with water-breaks as noted above.
  • Such water-breaks give rise to at least a per ⁇ ception, and increase the possibility in reality, of non-uniformity in practically important properties among various areas of the surfaces treated.
  • this reluctance is due to the presence of a carbon filter for the DI water (normal Stage 6) system, a filter that can become inadequately effective as a result of adsorption of lubricant and surface conditioner forming additives such as those in ME-40®; in other cases, it is due to a reluctance to make the engineering changes necessary to run ME-40.
  • the reduction in coefficient of friction provided by prior art treat ⁇ ments in either Stage 4 or Stage 6 can be substantially reduced, often to an unaccept ⁇ able level, if the treated cans are subjected to extraordinary heating after completion of the six process stages described above.
  • Such extraordinary heating of the cans in the drying oven occurs whenever a high speed production line is stalled for even a few minutes, an event that is by no means rare in practice.
  • the higher COF measurements correlate with the loss of mobility, thereby defeating the purpose of introducing mobility enhancing surfactants into can washing formulations.
  • the coefficient of fric- tion of a surface treated with a lubricant and surface conditioner is less easily dam ⁇ aged by heating when the lubricant and surface conditioner composition includes at least one of the following organic materials: alkoxylated or non-alkoxylated castor oil triglycerides and hydrogenated castor oil derivatives; alkoxylated and non-alkoxylated amine salts of a fatty acid including mono-, di-, tri-, and poly-acids; alkoxylated and non-alkoxylated amino fatty acids; alkoxylated and non-alkoxylated fatty amine N-ox- ides, alkoxylated and non-alkoxylated quaternary ammonium salts, alkyl esters of 2- substituted alkoxylated fatty alkyloxy acetic acids (briefly denoted hereinafter as "oxa- acid esters”) as described more fully in PCT Application US93/0
  • the composition including the organic materials should also include a metallic element selected from the group consisting of zirconi ⁇ um, titanium, cerium, aluminum, iron, tin, vanadium, tantalum, niobium, molybdenum, tungsten, and hafnium in metallic or ionic form, and the film formed on the surface as part of the lubricant and surface conditioner in dried form should include some of this metallic element along with organic material.
  • Preferred alkoxylated, especially ethoxylated, castor oil triglycerides that are commercially available include Trylox® 5900, Trylox® 5902, Trylox® 5904, Trylox® 5906, Trylox® 5907, Trylox® 5909, Trylox® 5918, and preferred hydrogenated castor oil derivatives include commercial materials such as Trylox® 5921 and Trylox® 5922, all available from Henkel Corporation. These materials are particularly useful as additives to final stage rinses, because they provide a dried lubricant and surface conditioner film on the treated surface that resists rise of the COF with heating beyond the minimum necessary to dry the surface.
  • organic materials comprise water-soluble alkoxyl ⁇ ated, preferably ethoxylated, propoxylated, or mixed ethoxylated and propoxylated materials, most preferably ethoxylated, and non-ethoxylated organic materials selected from amine salts of fatty acids including mono-, di-, tri-, and poly-acids, amino fatty acids, fatty amine N-oxides, and quaternary salts, and water soluble polymers.
  • Preferred amine salts of fatty acids include ammonium, quaternary ammonium, phosphonium, and alkali metal salts of fatty acids and derivatives thereof containing up to 50 moles of alkylene oxide in either or both the cationic or anionic species.
  • Amphoteric N and Amphoteric 400 iminodipropionate sod ⁇ ium salts available from Exxon Chemical Co.
  • Deriphat® 154 disodium N-tallow-beta iminodipropionate
  • Deriphat® 160 disodium N-lauryl-beta iminodipropionate, available from Henkel Corp.
  • Preferred amino acids include alpha and beta amino acids and diacids and salts thereof, including alkyl and alkoxyiminodipropionic acids and their salts and sarcosine derivatives and their salts.
  • Specific examples include Armeen® Z, N-coco-beta- aminobutyric acid, available from Akzo Chemicals Inc.; Amphoteric N, Amphoteric 400, Exxon Chemical Co.; sarcosine (N-methyl glycine); hydroxyethyl glycine; Hamposyl® TL-40 triethanolamine lauroyl sarcosinate, Hamposyl® O oleyl sarcosin- ate, Hamposyl® AL-30 ammoniumlauroyl sarcosinate, Hamposyl® L lauroyl sarcosin ⁇ ate, and Hamposyl® C cocoyl sarcosinate, all available from W.R.
  • amine N-oxides include amine oxides where at least one alkyl sub- stituent contains at least three carbons and up to 20 carbons. Specific examples include Aromox® C/12 bis-(2-hydroxyethyl)cocoalkylamine oxide.
  • Preferred quaternary salts include quaternary ammonium derivatives of fatty amines containing at least one substituent containing from 12 to 20 carbon atoms and zero to 50 moles of ethylene oxide and/or zero to 15 moles of propylene oxide where the counter ion consists of halide, sulfate, nitrate, carboxylate, alkyl or aryl sulfate, alkyl or aryl sulfonate or derivatives thereof.
  • Arquad® 12- 37W dodecyltrimethylammonium chloride Arquad® 18-50 octadecyltrimethylammoni- um chloride, Arquad® 210-50 didecyldimethylammonium chloride, Arquad® 218-100 dioctadecyldimethylammoniumchloride,Arquad®316(W)trihexadecylmethylammoni- um chloride, Arquad® B-100 benzyldimethyl(C 12 .
  • Preferred water-soluble polymers include homopolymers and heteropolymers of ethylene oxide, propylene oxide, butylene oxide, acrylic acid and its derivatives, maleic acid and its derivatives, vinyl phenol and its derivatives, and vinyl alcohol.
  • Specific examples include Carbowax® 200, Carbowax® 600, Carbowax® 900, Carbo ⁇ wax® 1450, Carbowax® 3350, Carbowax® 8000, and Compound 20M, all available from Union Carbide Corp.; Pluronic® L61, Pluronic® L81, Pluronic® 31R1, Pluron- ic® 25R2, Tetronic® 304, Tetronic® 701, Tetronic® 908, Tetronic® 90R4, and Tetronic® 150R1, all available from BASF Wyandotte Corp.; Acusol® 4 ION sodium salt of polyacrylic acid, Acusol® 445 polyacrylic acid, Acusol® 460ND sodium salt of maleic acid/olefin copolymer, and A
  • Additional improvements can often be achieved, particularly for lubricant and surface condition treatments applied before the final contact of the treated surface with an aqueous composition, by using an inorganic material selected from metallic or ionic zirconium, titanium, cerium, aluminum, iron, vanadium, tantalum, niobium, molybden ⁇ um, tungsten, hafnium or tin to produce a film combining one or more of these metals with one or more of the above-described organic materials.
  • an inorganic material selected from metallic or ionic zirconium, titanium, cerium, aluminum, iron, vanadium, tantalum, niobium, molybden ⁇ um, tungsten, hafnium or tin to produce a film combining one or more of these metals with one or more of the above-described organic materials.
  • a thin film is produced having a coefficient of static friction that is not more than 1.5, preferably not more than 1.2, more preferably not more than 1.0, or still more preferably not more than 0.80, and is less than the coefficient without such film, thereby improving can mobility in high speed conveying without interfering with subsequent lacquering, other painting, printing, or other similar decorating of the containers.
  • Preferred surfactants include ethoxylated and non-ethoxylated sulfated or sulfonated fatty alcohols, such as lauryl and coco alcohols. Suitable are a wide class of anionic, non-ionic, cationic, or amphoteric surfactants.
  • Alkyl polyglycosides such as C 8 - C, g alkyl polyglycosides having average degrees of polymerization between 1.2 and 2.0 are also suitable.
  • Other classes of surfactants suit- able in combination are ethoxylated nonyl and octyl phenols containing from 1.5 to 100 moles of ethylene oxide, preferably a nonylphenol condensed with from 6 to 50 moles of ethylene oxide such as Igepal® CO-887 available from Rhone-Poulenc; al- kyl/aryl polyethers, for example, Triton® DF-16; and phosphate esters of which Tri- ton® H-66 and Triton® QS-44 are examples, all of the Triton® products being avail ⁇ able from Union Carbide Co., and Ethox® 2684 and Ethfac® 136, both available from Ethox Chemicals Inc., are representative examples; polyethoxylated and/or polypropox- y
  • the lubricant and surface conditioner n accordance with this invention may comprise a phosphate acid ester or preferably an ethoxylated alkyl alcohol phosphate ester.
  • phosphate esters are commercially available under the trade name Gafac® PE 510 from GAF Corporation, Wayne, NJ, and as Ethfac® 136 and
  • organic phosphate esters may comprise alkyl and aryl phosphate esters with and without ethoxylation.
  • the lubricant and surface conditioner for aluminum cans may be applied to the cans during their wash cycle, during one of their treatment cycles such as cleaning or conversion coating, during one of their water rinse cycles, or during their final water rinse cycle.
  • the lubricant and surface conditioner may be applied to the cans after their final water rinse cycle, i.e., prior to oven drying, or after oven drying, by fine mist application from water or another volatile non-inflammable solvent solution. It has been found that the lubricant and surface conditioner is capable of de ⁇ positing on the surface to provide it with the desired characteristics.
  • the lubricant and surface conditioner may be applied by spraying and interacts with the surface through chemisorption or physiosorption to provide it with the desired dried lubricant and surface conditioner film.
  • the amount of lubricant and surface conditioner to be applied to the cans should be sufficient to reduce the coefficient of static friction on the outside surface of the cans to a value of about 1.5 or lower, and preferably to a value of about 1 or lower. Generally speaking, such amount should be on the order of from about 3 mg/m 2 to about 60 mg/m 2 of lubricant and surface conditioner on the outside surface of the cans.
  • Examples Group I Uncleaned aluminum cans from an industrial can manufacturer are washed clean in examples Type A with alkaline cleaner available from Parker+Amchem Divi- sion, Henkel Corporation, Madison Heights, Michigan, employing the Ridoline® 3060/ 306 process and in Examples Type B with an acidic cleaner, Ridoline® 125 CO from the same company.
  • a lubricant and surface conditioner composition comprising one of the following (i) about a 1 % by weight aqueous solution in deionized water of active organic material (I) as specified in Table 2 below; (ii) about 1 % of the active organic (I) in deionized water plus about 2 gm/1 (0.2 %) of the inorganic constituent (II) as specified in Table 2; (iii) about 1% active organic (I) in deionized water plus about 0.5 % of surfactant (lU) as specified in Table 2; (iv) about 1 % active organic (I), about 0.2% inorganic (II), and about 0.5% surfactant (IE) as specified in Table 2.
  • a lubricant and surface conditioner composition comprising one of the following (i) about a 1 % by weight aqueous solution in deionized water of active organic material (I) as specified in Table 2 below; (ii) about 1 % of the active organic (I) in deionized water plus about
  • compositions of the aqueous lubrication and surface conditioning treatment in this group the ones containing inorganic constituent (II) from Table 2 are applied in Stage 4 as defined above, while those not containing this ingredient are ap ⁇ plied immediately before final drying.
  • the cans after drying are evaluated for their coefficient of static friction using a custom built slip time tester.
  • This apparatus consisted of three timing stations attached to a motor driven inclinable ramp. Two cans are placed horizontally in each station and a third placed on top of them in the opposite direction. This TABLE 2
  • COF Tangent of [4.84 + (2.79-t)] where t is the time Slip Time in seconds. Fifteen slip times were collected, converted to COF's and then averaged to give the COF result discussed here. In some cases the tested cans were subjected to an additional bake out at 210° C for 5 minutes and the COF redetermined; this result is denoted hereinafter as "COF-2".
  • the COF produced on the surface is less than 1.5.
  • Mobility enhancer/rinse aid process solutions were prepared using deionized water with a conductivity less than 5 ⁇ siemens; unless otherwise noted, all other solutions were prepared in tap water.
  • Drawn and wall ironed alumi- num cans were obtained from commercial factory production.
  • B W single track seven stage conveyor belt type washer
  • CCW carousel type can washer
  • Foam heights were determined by placing 50 milliliters (hereinafter "mL") of the process solution in a 100 mL stoppered graduated cylinder and shaking vigorously for 10 seconds. The total volume of fluid, liquid plus foam, was determined immedi ⁇ ately and after 5 minutes of standing. These "foam heights” will be referred to herein- after as “IFH” (initial foam height) and “PFH” (persistent foam height) respectively.
  • IFN initial foam height
  • PFH persistent foam height
  • the water break characteristics of cans treated with candidate final rinse mobil ⁇ ity enhancers (“FRME's) were evaluated by visually rating the amount of waterbreak on each of the four major surfaces of the can: interior dome and sidewall and exterior dome and sidewall.
  • fluoride activity noted for Stage 2 above is defined and can conveniently be measured by means of a fluoride sensitive electrode as described in U. S. Patent 3,431,182 and commercially available from Orion Instruments.
  • Fluoride activity was measured relative to a 120E Activity Standard Solution commercially available from the Parker+Amchem ("P+A") Division of Henkel Corpor ⁇ ation by a procedure described in detail in P+A Technical Process Bulletin No. 968.
  • P+A Phase-Amchem
  • the Orion Fluoride Ion Electrode and the reference electrode provided with the Orion instrument are both immersed in the noted Standard Solution and the millivolt meter reading is adjusted to 0 with a Standard Knob on the instrument, after waiting if nec ⁇ essary for any drift in readings.
  • the electrodes are then rinsed with deionized or dis ⁇ tilled water, dried, and immersed in the sample to be measured, which should be brought to the same temperature as the noted Standard Solution had when it was used to set the meter reading to 0.
  • the reading of the electrodes immersed in the sample is taken directly from the millivolt (hereinafter often abbreviated "mv” or “mV”) meter on the instrument.
  • mv millivolt
  • mV millivolt
  • This device consisted of a power stabilized high intensity lamp and a fiber optic bun ⁇ dle conveying the light to the can surface.
  • the instrument is calibrated with a back silvered plane mirror to a measured reflectivity of 440. Once calibrated, the reflectivi ⁇ ties of fourteen cans were measured and averaged. With this device it was possible to measure the overall interior reflectivity and exterior dome reflectivity. Results are shown in Figures 1(a) - 1(d). II.3 Screening of Diverse Materials For FRME Activity.
  • the CCW was operated ac ⁇ cording to the following scheme, in which the extended Stage 3 rinse time simulated a production sequence wherein the normal Stage 3, 4, and 5 applications were used as rinses: Stage 1 sulfuric acid, pH 2.0, 30 sec, 54.4° C
  • Stage 2 RIDOLINE® 124C, 15 mL Free Acid, 3.4 g/L total of surfactant, Fluoride Activity -10 mV, 90 sec, 54.4° C
  • Stage 3 deionized water, 150 sec. (ca. 17.7 L)
  • Stage 4 as noted in Table 3, 30 sec, 29.4° C temperature Stage 5 not used
  • MacamineTM SO was predissolved by adding 15 % isopropanol.
  • IgepalTM 430 or poly vinyl alcohol 1.6 g/L of IgepalTM CO- 887 was added to obtain a homogeneous solution. Nitroguanidine was insoluble and was not investigated further. Results are shown in Table 3. Amine oxides with hydroxyethyl groups bonded to the amine oxide nitrogen, such as AromoxTM C/12 and T/12, and oxa-acid esters such as those identified in the table as OAE 1 - 4, are pre ⁇ ferred lubricants and surface conditioners, as are the ethoxylated castor oil derivatives considered in more detail below.
  • RO-(C 3 H 6 0) m -(C 2 H 4 0) n -CH 2 -C(0)0-CH 3 with the straight chain alkyl group R ranging from 8 to 18 carbon atoms in lenght, "m” being 0 or 1, and "n” ranging from 5 to an average of 8.5.
  • compositions with an equal total amount of EthoxTM MI-9 alone but also give further reductions in the COF.
  • the interactions are evidently complex and difficult to predict.
  • Stage 3 tap water Stage 4 not used Stage 5 deionized water Stage 6 as noted in Table 6, 0.2 g/L total active additive
  • Some surfactants were found that are better at promoting water drainage than the ethoxylated isostearic acids that are very effective in providing lubricant and sur ⁇ face conditioner films. However, the surfactants that are exceptionally good at pro ⁇ moting water drainage are much poorer than ethoxylated isostearic acids in reducing COF. Mixing the two types permits improvement in water drainage, while retaining the ability to achieve COF values that are adequate in many applications.
  • Some beverages packaged in aluminum cans are pasteurized, and unless the temperature and the composition(s) of the aqueous solution(s) with which cans are contacted during pasteurization are very carefully controlled, staining of the dome of the can often occurs during pasteurization.
  • An FRME combining fluozirconic acid and hydrogenated castor oil derivatives in proper concentrations has been found to provide both protection against dome staining during pasteurization and adequate lowering of the COF for most purposes.
  • Dome staining was evaluated by first removing the domes from the treated cans with a can opener. The domes were then placed in a water bath containing 0.2 g/L of borax at 65.6° C for 30 minutes, then rinsed in deionized water and dried in an oven. Staining resistance was evaluated visually by comparison with known satis- factory and unsatisfactory standards. Results are shown in Table 7. The last two con ⁇ ditions shown in the Table are highly satisfactory with respect to both COF and dome staining resistance during pasteurization.
  • This group illustrates use with tin cans.
  • Three types of materials were tried as lubricant and surface conditioner forming and water drainage promoting agents for tin cans: (i) EthoxTM MI- 14; (ii) a combination of 1 part by weight of PluronicTM 31R1 and 4 parts by weight of PlurafacTM D25; and (iii) TergitolTM Min-FoamTM IX.
  • the EthoxTM, TergitolTM, and PlurafacTM products are ethoxylated fatty acids or alcohols, with a poly ⁇ propylene oxide ⁇ block cap on the end of the poly ⁇ ethylene oxide ⁇ block in some cases, while the PluronicTM is a block copolymer of ethylene and propylene oxides, with poly ⁇ propylene oxide ⁇ block caps on the ends of the polymers. All were used at a concentration of 0.2 g/L of active material with deionized water in a final rinse before drying, after an otherwise conventional tin can washing sequence. Water retention and COF values were measured as generally described above. Results are shown in Table 8.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Health & Medical Sciences (AREA)
  • Lubricants (AREA)
  • Detergent Compositions (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
  • Chemically Coating (AREA)
  • Chemical Treatment Of Metals (AREA)
EP93916982A 1992-07-08 1993-07-08 AQUEOUS LUBRICATION AND SURFACE CONDITIONING FOR MOLDED METAL SURFACES. Withdrawn EP0649458A4 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP99203252A EP0969078A3 (en) 1992-07-08 1993-07-08 Process for treating formed metal surfaces

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US91048392A 1992-07-08 1992-07-08
US910483 1992-07-08
PCT/US1993/006359 WO1994001517A1 (en) 1992-07-08 1993-07-08 Aqueous lubrication and surface conditioning for formed metal surfaces

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EP0649458A4 true EP0649458A4 (en) 1996-02-14

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EP93916982A Withdrawn EP0649458A4 (en) 1992-07-08 1993-07-08 AQUEOUS LUBRICATION AND SURFACE CONDITIONING FOR MOLDED METAL SURFACES.

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JP (1) JPH07509261A (xx)
CN (1) CN1085244A (xx)
AU (1) AU675800B2 (xx)
BR (1) BR9306696A (xx)
CA (1) CA2135920A1 (xx)
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MX (1) MX9304090A (xx)
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US5935348A (en) * 1995-11-14 1999-08-10 Henkel Kommanditgesellschaft Auf Aktien Composition and process for preventing corrosion and reducing friction on metallic surfaces
GB9625652D0 (en) * 1996-12-11 1997-01-29 Novamax Technologies Limited The treatment of aluminium surfaces
CN1065787C (zh) * 1998-03-11 2001-05-16 日石三菱株式会社 拉深展薄罐的生产方法
US6190738B1 (en) * 1999-04-07 2001-02-20 Ppg Industries Ohio, Inc. Process for cleaning a metal container providing enhanced mobility
FR2825378B1 (fr) * 2001-05-31 2003-11-28 Univ Paris Curie Composition et procede pour le traitement d'alliages de magnesium
US6821633B2 (en) 2002-05-17 2004-11-23 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) Non-chromate conversion coating compositions, process for conversion coating metals, and articles so coated
CN1309812C (zh) * 2004-07-06 2007-04-11 中国石油化工集团公司 一种润滑油组合物及其应用
US7745381B2 (en) 2005-03-15 2010-06-29 Ecolab Inc. Lubricant for conveying containers
US7741257B2 (en) 2005-03-15 2010-06-22 Ecolab Inc. Dry lubricant for conveying containers
AU2011306381C1 (en) 2010-09-24 2016-10-20 Ecolab Usa Inc. Conveyor lubricants including emulsions and methods employing them
EP2589647A1 (de) * 2011-11-04 2013-05-08 Basf Se Quaternisierte Polyetheramine und deren Verwendung als Additive in Kraft- und Schmierstoffen
JP5885578B2 (ja) * 2012-05-14 2016-03-15 株式会社クラレ 潤滑剤
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MX9304090A (es) 1994-03-31
AU675800B2 (en) 1997-02-20
JPH07509261A (ja) 1995-10-12
WO1994001517A1 (en) 1994-01-20
CA2135920A1 (en) 1994-01-20
MD960241A (ro) 1998-04-30
ZA934846B (en) 1994-02-03
AU4665493A (en) 1994-01-31
CN1085244A (zh) 1994-04-13
BR9306696A (pt) 1998-12-08
EP0649458A1 (en) 1995-04-26
EP0969078A3 (en) 2000-02-23
EP0969078A2 (en) 2000-01-05

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