EP0597682A1

EP0597682A1 - Removing fibres from pulp

Info

Publication number: EP0597682A1
Application number: EP93308961A
Authority: EP
Inventors: Margaret Anne Brew; John Robert Schmidt; Steven Dirk Bennett
Original assignee: Mead Corp
Current assignee: Mead Corp
Priority date: 1992-11-10
Filing date: 1993-11-10
Publication date: 1994-05-18
Anticipated expiration: 2013-11-10
Also published as: DE69312639T2; DE69312639D1; FI934955A0; EP0597682B1; FI934955A; CA2108321A1

Abstract

Coarse fibres are removed from a lignocellulosic pulp by spraying a slurry of the pulp against a rotating disk filter. A first fraction of the pulp passes through the filter and constitutes an accepts fraction. A second fraction is retained on the filter, contains an enriched concentration of coarse fibres from the pulp and constitutes a rejects fraction. The accepts and rejects fractions are removed from the filter.

Description

This invention generally relates to a process for removing coarse fibres from a lignocellulosic pulp.
Mechanical pulp often contains significant quantities of incompletely separated fibers. These coarse fibers, also referred to as shives or fiber bundles, are retained on a 28 mesh screen during a Bauer/McNett classification. The coarse fibers are typically weak, have poor bonding characteristics, and contribute to poor print quality in the final sheet of paper.
Existing processes for removing the coarse fraction from mechanical pulp utilize either perforated or slotted screen baskets. The rejected stock from these screens is returned to a reject refining system wherein the coarse fraction is rendered acceptable by further refining. This method for separating coarse fiber from the mechanical pulp for further treatment is inefficient.
Coarse fraction removal efficiency is a function of the mass reject rate and the screen configuration. As the mass reject rate increases, a larger portion of the coarse fraction in the feed stock is rejected. At mass reject rates of 25%, the removal efficiency of the coarse fibers approaches 50%. Even with extremely fine slotted screen baskets increases in the system removal efficiency to about 60% require an increase in the mass reject rate to over 30%. Thus, high removal efficiencies are achieved at the expense of overloading the reject refining system.
Therefore, it has become apparent that a need exists for an improved method for fractionating mechanical pulp which results in a significantly higher coarse fraction removal efficiency at a significantly lower mass reject rate.
As will become apparent from the detailed description below, methods in accordance with this invention make use of a rotating disk filter.
The use of rotating disk filters, also known as spray disk filters, in the paper pulp processing industry has previously been proposed. However, their use has been designed to remove impurities such as agglomerated inks from the pulp by carrying the impurities through the filter (see International Application WO 90/06396). The acceptable fraction of the pulp remains on the filter with the impurities being rejected by passing through the filter with a waste stream.
In accordance with the present invention, in a first aspect thereof, there is provided a method for removing coarse fibres from a lignocellulosic pulp, comprising the steps of: spraying a lignocellulosic pulp slurry containing said coarse fibres against a rotating disk filter such that a first fraction of said pulp passes through said filter and constitutes an accepts fraction and a second fraction of said pulp is retained on said filter and contains an enriched concentration of said coarse fibres and constitutes a rejects fraction; and removing said accepts fraction and said rejects fraction from said filter.
It will thus be seen that methods in accordance with the present invention work directly opposite to the previous proposals for use of rotating disk filters.
Pulp stock at a controlled consistency is suitably sprayed against the rotating disk filter through a plurality of spray nozzles positioned perpendicular to the disk. The accepted stock passes through the fabric and is collected in a tank or transported for further use. The rejected stock remains on the disk and is through off the fabric by the centrifugal force generated by the rotating disk and is collected separately.
Removal efficiency of this method is a function of mass reject rate, which is dependent on the fabric mesh size covering the disk, the feed stock flow and consistency, and the spray nozzle pressure.
In a second and alternative aspect thereof, the invention provides a method for removing coarse fibre from a mechanical pulp comprising the steps of: spraying a mechanical pulp slurry against a first rotating disk filter; passing a first accepts fraction of said pulp slurry through said first disk filter; retaining a first rejects fraction of said pulp on said first disk filter; conveying said first accepts fraction to a second rotating disk filter; spraying said first accepts fraction against said second rotating disk filter; passing a second accepts fraction of said pulp through said second disk filter; retaining a second rejects fraction on said second disk filter; collecting said second accepts fraction; and removing said first rejects fraction and said second rejects fraction from said disk filters.
The invention provides, in a third alternative aspect thereof, a method for removing coarse fibre from a mechanical pulp fraction comprising the steps of: spraying a mechanical pulp slurry against a first rotating disk filter; passing a first accepts fraction of said pulp slurry through said disk filter; retaining a first rejects fraction of said pulp on said first disk filter; removing said first rejects fraction from said first disk filter by centrifugal force through a reject chute; conveying a said first rejects fraction to a second rotating disk filter; spraying said first rejects fraction against a second rotating disk filter; passing a second accepts fraction through said second disk filter; retaining a second rejects fraction on said second disk filter; and removing said second rejects fraction from said disk filter through a reject chute.
The invention is hereinafter more particularly described by way of example only with reference to the accompanying drawings, in which:-

Fig. 1 is a perspective view of apparatus useful in carrying out a method in accordance with the present invention;
Fig. 2 is a perspective view of the apparatus of Fig. 1 together with additional elements of the system;
Fig. 3 is a perspective view of a plurality of spray disk filters incorporated as a processing system suitable for performing an example of the method of this invention;
Fig. 4 is a flow diagram of one filtration system in accordance with the present invention in which the accepts fraction is filtered twice; and
Fig. 5 is a flow diagram of another filtration system in accordance with the present invention in which the rejects fraction is filtered twice and the accepts fractions are combined.

An improved method for fractionating mechanical pulp has been developed using a spray disk filter system, generally designated 10, as shown in Fig. 1. Fig. 1 illustrates two spray disk filters A and B arranged in a back-to-back relationship, each operating in an identical manner. The spray disk filter 10 is a conventional apparatus manufactured by the Celleco Corporation. Hereinbelow filter A will be described. It is to be understood that the description of filter A pertains similarly to all filters.
Filter A consists of a disk 12 with its inside face covered by a fabric screen 14. Lignocellulosic pulp, and more particularly mechanical pulp stock 16, at a controlled consistency, is sprayed against the inner faces of disk 12, which is rotating, through a plurality of stationary spray nozzles 18 oriented perpendicular to the disks. A first fraction of the pulp passes through the filter and constitutes an accepts fraction and a second fraction of the pulp is retained on the filter and constitutes an enriched concentration of coarse fibers and constitutes a rejects fraction. The coarse fraction removed will typically range from +14 to +28 mesh.
As shown in Fig. 2, the fabric covered disks 12 are mounted on a centre drive shaft 20. The disks are typically about eight feet (2.4384m) in diameter with the outer 18 inches (45.72cm) of the radius being covered by fabric 14. The fabric screens are usually made out of nylon or woven stainless steel. In one commercially available design, the fabric screen is divided into sectors individually mounted around the outer radius of the disk by support members 22. By utilizing sections of fabric, the screen can be easily installed and sections can be replaced when necessary. Screens are commercially available from the filter manufacturer.
The centre shaft 20 is coupled to a variable speed motor 24 (typically 25 horsepower - 1.86 x 10⁴ Watts) via a drive assembly 26 which rotates the center shaft therefore turning both disks at the same speed. Normal operating speeds depend upon a number of factors including pulp slurry consistency and the diameter of the disks, with the speeds ranging from about 10 to about 60 rpms. A preferred operating speed for an eight foot (2.4384m) diameter disk is about 33 rpms.
The disks 12 and the shaft assembly are enclosed within a housing 28 with the motor 24 and drive assembly 26 mounted outside the housing. A removable lid (not shown) covers the upper portion of the housing 28 and provides access to the filters for maintenance.
Mechanical pulp stock 16 (Fig. 1) is introduced into headers 30 through feed ports 32 located in the housing 28. A midfeather 31 separates the headers 30. The pulp 16 typically has a consistency ranging from about 0.30 to about 1.50 percent of pulp to water and preferably from about 0.5 to 1.0 percent.
The headers 30 feed a manifold of nozzles 18 located on the surface of the headers. In one commercial design, on each header there are located between 44 and 58 full-cone nozzles each having a one-half inch (1.27cm) diameter discharge orifice 37 (Fig. 1). The nozzles are oriented at 90° to the disks, however the orientation can be varied such that the nozzles are positioned at an angle of about 40 to about 130° with respect to the direction of the disks 12. Pulp stock is sprayed into chamber 11 against the rotating inner face 13 of fabric screen 14 through the nozzles 18 under a gauge pressure ranging from about 10 to about 35 psig (6.9 to 24.1 x 10⁴N/m²) and preferably 15 to 20 psig (10.3 to 13.8 x 10⁴N/m²). The pulp is sprayed against the fabric screen 14 at a flow rate ranging from about 14 to about 48 gpm/ft² (151 to 517 g/m³) and preferably 23 to 36 gpm/ft² (248 to 388 g/m³). A first fraction of the pulp passes through the fabric screen 14 and constitutes an accepts fraction 34 and a second fraction of the stock is retained on the fabric screen and constitutes an enriched concentration of coarse fibers and constitutes a rejects fraction 36.
The accepts fraction 34 of the stock passes through the fabric to the outside of the disk 12 where it is collected in a chamber 38 located behind the disk 12. Chamber 38 is separated from the chamber 11 by the fabric screen 14 and a seal (not shown). The rejects fraction 36 which does not pass through the fabric is retained and removed from the fabric screen 14 via a combination of centrifugal force and a cleaning shower described below. The accepts fraction 34 contained in chamber 38 flows by gravity out of the chamber through an exit conduit 40. The rejects fraction 36 after being thrown off the screen flows by gravity to the bottom of the chamber 11 exits the housing through a rejects chute 42 for further processing or disposal through rejects conduit 44.
The spray disk filter is preferably also equipped with cleaning showers 46. There are two high pressure fabric cleaning bars 47 located on the feed side and the outlet side of each disk. These showers act to spray water and remove any fiber that may tend to clog the fabric. The showers on the inner feed side 13 are oriented at 90° to the fabric and will flush through the fabric to the outside of the disk. The showers on the outlet side 15 are oriented at 90° to the fabric and will spray towards the feed side. Two intermittent high pressure, rotating cleaning showers (not shown) are located in the top of the headers. These spray for ninety seconds on one hour intervals and act to keep the internal surfaces of the headers 30 clean.
The mesh size of the fabric, the feed stock consistency and flow, and the nozzle pressure are all controlled to prevent formation of a pulp mat on the fabric screen 14.
Feedstock consistency ranges and nozzle pressures ranges have been disclosed above. Several different media including nylon or woven stainless steel can be utilized having a mesh ranging from about 300 to about 1000 microns, with a preferred mesh ranging from about 450 to about 800 microns. Higher consistency results in higher removal efficiency. Since the fabric screen 14 acts as a barrier, for a given disk area, disk speed and stock flow rate, higher consistencies result in more fiber being present at the fabric surface at any given point in time. At higher consistencies a thicker mat will form on the fabric. The mat will act as a barrier and will further filter out coarse fibers. While a higher stock consistency is desirable, it is limited because as the consistency increases, the mass reject rate also increases.
Other factors affecting coarse fraction removal efficiency are nozzle pressure, feed stock flow rate, and feed stock coarse fraction content 3% to 10% of total fiber. These factors appear to have less impact on separation efficiency than media size and feed stock consistency when in the ranges previously discussed.
Disk speed is another factor affecting coarse fraction removal efficiency. Disk speed impacts efficiency in one of two ways. At high feed stock consistencies, higher disk speeds aid in minimizing mat formation by increasing the centrifugal force used to remove the coarse fraction from the feed side of the disks. Disk speed can be used to fine tune the effect of media size through the concept of apparent aperture modification. At higher disk speeds, any opening appears smaller. This effect is expected to be minimal because of the relative velocities of the disk and the stock flow.
Fig. 2 illustrates the present invention using two disks, however the invention can incorporate any number of disks. For example, a plurality of disk filtration systems 60, 62, 64, 66 each corresponding to the system shown in Fig. 2 may be mounted on a single drive shaft 20 as shown in Fig. 3. The mode of operation of the filters in Fig. 3 is identical to that discussed with reference to Figs. 1 and 2. The accepts fraction 34 is collected from the system in a stock chest 46, with the rejects fraction 36 being collected in a separate stock chest 48.
For even higher coarse fraction removal efficiencies, the accepts fraction 34, and the rejects 36 fractions can be filtered a second time as schematically illustrated in Figs. 4 and 5 respectively.
In Fig. 4 the mechanical pulp stock 16 is sprayed onto a first rotating disk filter or plurality of filters 50 such that a first fraction 34 passes through the filter(s) and constitutes an accepts fraction A and a second fraction 36 is retained on the filter(s) and constitutes a rejects fraction R. The accepts fraction A is conveyed to a second rotating disk filter(s) 52 such that a third fraction 54 of the pulp passes through the filter(s) and constitutes a second accepts fraction A' and a fourth fraction 56 of the pulp is retained on the second filter(s) 52 and constitutes a second rejects fraction R'. In implementing this system, the operating conditions of the first and second filtration systems can be the same but will preferably be different and optimized to provide the best balance of pulp quality and operation efficiency. Thus, the two filtration systems may employ different filter media, meshsize, consistency, rotational speed, etc. Furthermore, in a commercial setting first filtration systems may be a first bank of 1 to 8 filters and second filtration system 52 may be a second bank of 1 to 8 filters mounted on the same or a different drive shaft.
Alternatively, in Fig. 5 the mechanical pulp stock 16 is sprayed onto a first rotating disk filter(s) 50 such that a first fraction 34 passes through the filter(s) and constitutes an accepts fraction A and a second fraction 36 is retained on the filter(s) and constitutes a rejects fraction R. The rejects fraction R is then conveyed to a second rotating disk filter(s) 52 wherein it is sprayed on the filter(s) such that a third fraction 54 of the pulp passes through the second filter(s) and constitutes a second accepts fraction A' and a fourth fraction 56 is retained on the second filter(s) and constitutes a second rejects fraction R'. Normally, the second station of filters can contain a smaller number of filters because once the stock has been filtered a first time, a lesser amount of stock remains to be filtered for the second time.
The spray disk filter system of the present invention has resulted in significantly higher coarse fraction removal efficiencies at significantly lower mass rejects rate. Removal efficiencies of 80 to 95% are achievable at system mass reject rates of 15 to 60%. Removal efficiency is defined as: $\frac{(shives fed - shives accepted)}{(shives fed)} X 100%$

and mass reject rate defined as: $\frac{(fiber fed - fiber accepted)}{(fiber fed)} X 100%$
The accepts from the filter are more dilute than the feed (have a lower consistency) for both of the processes depicted in figures 4 and 5. No further consistency adjustment is necessary for secondary processing of the accepts such as in figure 4. The rejects, however, are more concentrated (have a higher consistency) for both processes depicted in figures 4 and 5. Depending on the secondary media size, it may be necessary to further dilute the rejects stream before processing as in figure 5. A recommendation is to dilute to a consistency similar to that of the first disk feed consistency if both disks are equipped with the same size media.
The invention has been disclosed with respect to its preferred parameters in which test runs have been performed with the following non-limiting examples:

Example #1

A prototype spray disk filter with a single 3 foot (91.44cm) diameter disk and 3 inlet nozzles was used. In theory, the degree of fractionation can be affected by several operating variables including mesh size, nozzle angle, disk speed, nozzle pressure, and pulp consistency. Two series of trials were performed to evaluate the capability of the spray disk filter to fractionate mechanical pulp. The variables evaluated and the ranges evaluated are summarized in Table 1.

Table 1

Spray Disk Filter Trial Conditions
	June 26-27	August 14-15
Media Size (micron)	600, 800 & 1000	300, 480, 540, 600, 800 and 1000
Consistency (%)	0.60 - 1.54	0.28 - 1.14
Number of Nozzles	1	3
Nozzle Angle (degree)	90	90
Nozzle Pressure (psig)	25	15 - 30
(N/m²)	17.2 x 10⁴)	(10.3 to 20.7 x 10⁴)
Disk Speed (rpm)	96	96

Mechanical pulp stock from a refined pulp surge chest was shipped for trials. A total of 21 trial runs were conducted during two trial periods (June 26-27 and August 14-15, 1991). Trial runs were conducted such that three different system configurations were evaluated. In the first, the spray disk filter was used as a single stage screening device. Two 2-stage configurations were also evaluated. Stock was screened through a primary stage spray disk filter and the accepted stock was screened through a second stage spray disk filters as shown in Fig. 4. In the second approach, the rejected stock (coarse fraction) from the primary spray disk filter was screened through a secondary spray disk filter as shown in Fig. 5.
Flow rates and consistencies were measured for each trial run. Samples were collected from the feed, accept and reject for Bauer/McNett fiber classifications. During the trials, freeness was measured on the feed, accept and reject streams. The trial conditions, fiber classifications, mass balance, mass reject rate, volume reject rate and efficiency calculations for each trial run are summarized in Table 1.

In general, +28 fraction removal efficiency, mass reject rate, and volume reject rate all decrease with increasing media size. Consistency has the opposite effect. Higher consistencies result in higher efficiency, higher mass reject rate and higher volume reject rate. When flow rate or +28 fraction are included in the models for mass reject rate, volume reject rate or efficiency, they have less effect on the performance of the filter.

Table 1

System 1 (Fig. 4)
	Primary Stage	Secondary Stage
Media	480 micron	480 micron
Feed Consistency	0.25%
Feed +28 Fraction	13.3%
Nozzle Pressure
	15 psig (10.3 x 10⁴N/m²)	15 psig
Flow rate	100 gpm
System Mass Reject Rate		34.3%
System +28 Removal Efficiency		97.9%

	Primary Stage	Secondary Stage
Media	800 micron	540 micron
Feed Consistency	0.50%
Feed +28 Fraction	13.3%
Nozzle Pressure
	20 psig (13.8 x 10⁴N/m²)	20 psig
Flow rate	100 gpm
System Mass Reject Rate		25.6%
System +28 Removal Efficiency		91.6%

System 2 (Fig. 5)
	Primary Stage	Secondary
Stage
Media	480 micron	480 micron
Feed Consistency	0.75%
Feed +28 Fraction	13.3%
Nozzle Pressure
	15 psig (10.3 x 10⁴N/m²)	15 psig
Flow rate	100 gpm
System Mass Reject Rate		13.7%
System +28 Removal Efficiency		80.7%

Example #2

A commercial size spray disk filter unit with two 7'5'' (2.2606m) diameter disks and 112 spray nozzles was evaluated in a mechanical pulp mill. Operating variables studied were mesh size, disk speed, nozzle pressure, pulp consistency, and feed flow rate. Three series of trials were conducted February 13, 1992 to July 31, 1992. The variables studied are summarized in the table below.

Pilot Plant Spray Disk Filter Trials Conditions
Media Size (microns)	450, 600, and 800
Feed Consistency (%)	0.43 - 1.46
Nozzle Pressure (psi)	10 - 30 (6.9 to 20.7 x 10⁴N/m²)
Disk Speed (rpm)	25 - 41
Feed Flow rate (gpm)	471 - 1454

The pilot plant unit was installed such that it would be operated in three different configurations: 1) both disks fed in parallel; (2) series operation with disk 1 accepts (fine fraction) feeding disk 2; (3) series operation with disk 1 rejects (coarse fraction) feeding disk 2.
The installation included feed flow measurement and control for both disks, feed consistency measurement and control for both disks, and in-line pressure measurement for the feed to both disks. The level in the intermediate storage tank was measured and controlled. Combined accepts flow rate was measured in-line.
Pilot plant trials were conducted in which the system operated in configuration 3: primary disk coarse fraction was filtered a second time by the secondary disk. Flow rates and consistencies were measured during each trial. Samples were collected from disk 1 feed, disk 2 feed, disk 1 accepts, disk 2 accepts, disk 1 rejects, disk 2 rejects, and combined accepts. These samples were then classified on a Bauer/McNett classifier and the freeness was measured using the Canadian Standard Freeness test. Results are summarized in the following table.
In general, +28 fraction removal efficiency, mass reject rate, and volumetric reject rate all decreased with increasing media size. Higher consistencies, however, had the opposite effect; +28 removal efficiency, mass reject rate, and volumetric reject rate all increased with increasing consistency. Flow rate and disk speed were found to have a less significant effect on efficiency, mass reject rate, and volumetric reject rate.
It should be noted that the fiber source for this mechanical pulp mill was aspen. Optimum filter operating conditions are likely to vary for different fiber sources depending on individual fiber characteristics.

Claims

A method for removing coarse fibres from a lignocellulosic pulp, comprising the steps of: spraying a lignocellulosic pulp slurry containing said coarse fibres against a rotating disk filter such that a first fraction of said pulp passes through said filter and constitutes an accepts fraction and a second fraction of said pulp is retained on said filter and contains an enriched concentration of said coarse fibres and constitutes a rejects fraction; and removing said accepts fraction and said rejects fraction from said filter.
A method according to Claim 1, wherein said pulp is a mechanical pulp.
A method according to Claim 1 or Claim 2, wherein said disk filter is positioned with its centre axis horizontally oriented and said pulp is sprayed on said filter in a horizontal direction.
A method according to any preceding claim, wherein said disk filter is formed from a filter medium having a pore size ranging from about 300 to about 1000 microns.
A method according to any preceding claim, wherein said pulp slurry has a consistency ranging from about 0.1 to about 2.0 percent.
A method according to any preceding claim, wherein said disk filter rotates at about 10 to about 60 rpm.
A method according to any preceding claim, wherein said pulp slurry is sprayed against the disk filter under pressure ranging from gauge pressure of about 15 to 35 pounds force per square inch (1.03 to 2.41 x 10⁵N/m²).
A method according to any preceding claim, wherein said pulp slurry is sprayed against the disk filter through nozzles oriented at an angle of about 40 to 130° with respect to the direction of rotation of said filter.
A method according to any preceding claim, wherein said pulp slurry is sprayed against the disk filter at a flow rate ranging from about 14 to about 48 gpm/ft² (151 to 517 g/m³).
A method according to Claim 3, wherein the method is conducted under conditions which provide a removal efficiency ranging from about 80 to about 95 percent at a total system mass reject rate ranging from about 15 to about 60 percent.
A method according to Claim 10, wherein the coarse fibres removed are greater than 28 mesh.
A method according to any preceding claim, including the additional steps of: conveying said accepts fraction to a second rotating disk filter; spraying said accepts fraction against a second said rotating disk filter such that a third fraction of said pulp passes through said filter and constitutes a second accepts fraction and a fourth fraction of said pulp is retained on said second filter and contains an enriched concentration of said coarse fibres and constitutes a second rejects fraction.
A method according to any of Claims 1 to 11, including the additional steps of: conveying said rejects fraction to a second rotating disk filter; spraying said rejects fraction against said second rotating disk filter such that a third fraction of said pulp passes through said filter and constitutes a second accepts fraction and a fourth fraction of said pulp is retained on said second filter and contains an enriched concentration of said coarse fibres and constitutes a second reject fraction.
A method according to Claim 12, wherein said second accepts fraction is filtered a third and fourth time.
A method according to Claim 13, wherein said second rejects fraction is filtered a third and fourth time.
A method according to any of Claims 12 to 15, wherein said method is performed using a plurality of first and second disk filters mounted for rotation on separate drive shafts.
A method according to any of Claims 1 to 11, wherein said method is performed using a plurality of disk filters mounted for rotation on a common drive shaft.
A method for removing coarse fibre from a mechanical pulp comprising the steps of: spraying a mechanical pulp slurry against a first rotating disk filter; passing a first accepts fraction of said pulp slurry through said first disk filter; retaining a first rejects fraction of said pulp on said first disk filter; conveying said first accepts fraction to a second rotating disk filter; spraying said first accepts fraction against said second rotating disk filter; passing a second accepts fraction of said pulp through said second disk filter; retaining a second rejects fraction on said second disk filter; collecting said second accepts fraction; and removing said first rejects fraction and said second rejects fraction from said disk filters.
A method for removing coarse fibre from a mechanical pulp fraction comprising the steps of: spraying a mechanical pulp slurry against a first rotating disk filter; passing a first accepts fraction of said pulp slurry through said disk filter; retaining a first rejects fraction of said pulp on said first disk filter; removing said first rejects fraction from said first disk filter by centrifugal force through a reject chute; conveying a said first rejects fraction to a second rotating disk filter; spraying said first rejects fraction against a second rotating disk filter; passing a second accepts fraction through said second disk filter; retaining said second rejects fraction on said second disk filter; and removing said second rejects fraction from said disk filter through a reject chute.