EP0223537A3 - Process for devolatilizing molten oxymethylene polymer process for devolatilizing molten oxymethylene polymer - Google Patents

Process for devolatilizing molten oxymethylene polymer process for devolatilizing molten oxymethylene polymer

Info

Publication number
EP0223537A3
EP0223537A3 EP86308761A EP86308761A EP0223537A3 EP 0223537 A3 EP0223537 A3 EP 0223537A3 EP 86308761 A EP86308761 A EP 86308761A EP 86308761 A EP86308761 A EP 86308761A EP 0223537 A3 EP0223537 A3 EP 0223537A3
Authority
EP
European Patent Office
Prior art keywords
molten
polymer
devolatilizing
stage
oxymethylene polymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP86308761A
Other versions
EP0223537A2 (en
EP0223537B1 (en
Inventor
Douglas W. Steele
George S. Nash
John W. Dorsey
Ronald S. Christy
Timothy L. Burns
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Celanese Corp
Original Assignee
Celanese Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Corp filed Critical Celanese Corp
Priority to AT86308761T priority Critical patent/ATE82992T1/en
Publication of EP0223537A2 publication Critical patent/EP0223537A2/en
Publication of EP0223537A3 publication Critical patent/EP0223537A3/en
Application granted granted Critical
Publication of EP0223537B1 publication Critical patent/EP0223537B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/82—Heating or cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D19/00—Degasification of liquids
    • B01D19/0042—Degasification of liquids modifying the liquid flow
    • B01D19/0052—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
    • C08G2/28—Post-polymerisation treatments
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/78—Processes of molding using vacuum
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S525/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S525/927—Polyamide admixed with oxyalkylene-containing polymer

Abstract

A process is provided for removing volatile materials from a molten oxymethylene polymer, according to which the molten poly­mer is passed through a rotating disk polymer processor having at least three stages; a first devolatilization stage, then a stabil­ization stage and then a second devolatilization stage. The molten polymer in the first devolatilization stage is maintained at a tem­perature above its melting point in the temperature range of from about 160°C to about 220°C and at a vapor space pressure of from about 0.1 to about 300 Torr. The polymer in the stabilization stage is maintained in the molten state at a temperature of from 160°C to about 220°C. The polymer in the second devolatilization stage is maintained in the molten state at a temperature of from about 160°C to 190°C and at a vapor space pressure of from about 0.1 to about 100 Torr.
EP86308761A 1985-11-12 1986-11-11 Process for devolatilizing molten oxymethylene polymer Expired - Lifetime EP0223537B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT86308761T ATE82992T1 (en) 1985-11-12 1986-11-11 PROCESS FOR DEGASSING FUSED POLYMETHYLENE OXIDE.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/797,054 US4692290A (en) 1985-11-12 1985-11-12 Process for devolatilizing molten oxymethylene polymer
US797054 1985-11-12

Publications (3)

Publication Number Publication Date
EP0223537A2 EP0223537A2 (en) 1987-05-27
EP0223537A3 true EP0223537A3 (en) 1988-07-27
EP0223537B1 EP0223537B1 (en) 1992-12-02

Family

ID=25169772

Family Applications (1)

Application Number Title Priority Date Filing Date
EP86308761A Expired - Lifetime EP0223537B1 (en) 1985-11-12 1986-11-11 Process for devolatilizing molten oxymethylene polymer

Country Status (10)

Country Link
US (2) US4692290A (en)
EP (1) EP0223537B1 (en)
JP (1) JPH0643477B2 (en)
KR (1) KR950007989B1 (en)
CN (1) CN1009649B (en)
AT (1) ATE82992T1 (en)
BR (1) BR8605580A (en)
CA (1) CA1264391A (en)
DE (1) DE3687216T2 (en)
ES (1) ES2053446T3 (en)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0264926B1 (en) * 1986-10-24 1992-04-08 Boehringer Ingelheim Kg Process for the preparation and purification of thermally instable compounds
US5206308A (en) * 1989-05-12 1993-04-27 Hoechst Celanese Corporation Grafting of amine functional polymers onto functionalized oxymethylene polymers and the resulting graft polymers thereof
US5236645A (en) * 1990-09-21 1993-08-17 Basf Corporation Addition of additives to polymeric materials
CN1035510C (en) * 1990-09-29 1997-07-30 化学工业部晨光化工研究院一分院 One-step process for after-treating molten polyformaldehyde
US5372765A (en) * 1993-06-01 1994-12-13 Chi Mei Corporation Continuous process for extrusion of thermoplastic resin
US5688897A (en) * 1994-04-07 1997-11-18 Asahi Kasei Kogyo Kabushiki Kaisha Method for producing a stabilized oxymethylene copolymer
US5976141A (en) * 1995-02-23 1999-11-02 Synthes (U.S.A.) Threaded insert for bone plate screw hole
JP3789555B2 (en) * 1996-06-19 2006-06-28 ポリプラスチックス株式会社 Polyacetal resin composition
JP3210872B2 (en) * 1996-12-13 2001-09-25 ポリプラスチックス株式会社 Method for producing stabilized oxymethylene copolymer
ATE331475T1 (en) * 2003-03-20 2006-07-15 Stryker Trauma Sa BONE CONNECTION DEVICE
JP2005264101A (en) * 2004-03-22 2005-09-29 Asahi Kasei Chemicals Corp Polyacetal resin
KR100574165B1 (en) * 2004-10-08 2006-04-27 한국엔지니어링플라스틱 주식회사 Polyoxymethylene Resin Composition Having an Excellent Heat Stability
US9101426B2 (en) 2012-10-11 2015-08-11 Stryker Trauma Sa Cable plug
JP5814414B2 (en) * 2014-03-31 2015-11-17 ポリプラスチックス株式会社 Process for producing polyacetal copolymer
US10499968B2 (en) 2014-08-08 2019-12-10 Stryker European Holdings I, Llc Cable plugs for bone plates
CN111497057A (en) * 2020-04-28 2020-08-07 陕西洪贝为商贸有限公司 High polymer material preheats oven

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4194841A (en) * 1976-02-02 1980-03-25 Zehev Tadmor Method and apparatus for processing polymeric materials
US4366305A (en) * 1980-11-20 1982-12-28 Mitsubishi Gas Chemical Company, Inc. Process for heat stabilizing oxymethylene copolymers
US4529320A (en) * 1983-09-14 1985-07-16 Usm Corporation Rotary processors and method for devolatilizing materials

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2735840A (en) * 1956-02-21 Vacuum pump
US3027352A (en) * 1958-02-28 1962-03-27 Celanese Corp Copolymers
US3219623A (en) * 1960-04-21 1965-11-23 Celanese Corp Stabilization of oxymethylene copolymers with an hydroxy containing reactant
US3318848A (en) * 1963-06-20 1967-05-09 Celanese Corp Melt hydrolysis of oxymethylene copolymers
US3418280A (en) * 1964-12-31 1968-12-24 Celanese Corp Stabilization of oxymethylene copolymers by alkaline hydrolysis
US3336262A (en) * 1965-11-05 1967-08-15 Tenneco Chem Branched chain polyoxymethylene polycarboxylates
US3433861A (en) * 1966-01-12 1969-03-18 Celanese Corp Production of dyed,shaped oxymethylene polymers
US3545041A (en) * 1968-01-10 1970-12-08 Bryce Maxwell Apparatus for mixing devolatizing and extruding
JPS5417993A (en) * 1977-07-11 1979-02-09 Mitsubishi Chem Ind Ltd Method of stabilizing polyoxymethylene
US4213709A (en) * 1978-12-01 1980-07-22 Usm Corporation Rotary processor
JPS55157617A (en) * 1979-05-28 1980-12-08 Mitsubishi Gas Chem Co Inc Thermal stabilization of oxymethylene copolymer
US4362852A (en) * 1981-09-16 1982-12-07 Allied Corporation Devolatilizing molten polymer with a rotary disk processor
US4389119A (en) * 1982-01-04 1983-06-21 Usm Corporation Rotary processors
US4411532A (en) * 1982-01-04 1983-10-25 Usm Corporation Rotary processor
US4486099A (en) * 1983-09-14 1984-12-04 Usm Corporation Rotary processors and devolatilizing methods for particulate materials

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4194841A (en) * 1976-02-02 1980-03-25 Zehev Tadmor Method and apparatus for processing polymeric materials
US4366305A (en) * 1980-11-20 1982-12-28 Mitsubishi Gas Chemical Company, Inc. Process for heat stabilizing oxymethylene copolymers
US4529320A (en) * 1983-09-14 1985-07-16 Usm Corporation Rotary processors and method for devolatilizing materials

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN, Unexamined Applications, C Field, Vol. 5, No. 31, February 25, 1981 The Patent Office Japanese Government page 89 C 45 * Kokai-No. 55-157 617 (Mitsubishi Gas Kagaku K.K.) * *

Also Published As

Publication number Publication date
BR8605580A (en) 1987-08-18
CN86107755A (en) 1987-07-08
JPS62119219A (en) 1987-05-30
US4692290A (en) 1987-09-08
US4744934A (en) 1988-05-17
EP0223537A2 (en) 1987-05-27
ATE82992T1 (en) 1992-12-15
DE3687216D1 (en) 1993-01-14
JPH0643477B2 (en) 1994-06-08
CN1009649B (en) 1990-09-19
DE3687216T2 (en) 1993-04-22
KR950007989B1 (en) 1995-07-24
KR870005024A (en) 1987-06-04
CA1264391A (en) 1990-01-09
ES2053446T3 (en) 1994-08-01
EP0223537B1 (en) 1992-12-02

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