EP0040927A1 - Système de production d'un rideau de liquide pulvérisé pour l'application sur une bande en mouvement - Google Patents

Système de production d'un rideau de liquide pulvérisé pour l'application sur une bande en mouvement Download PDF

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Publication number
EP0040927A1
EP0040927A1 EP81302126A EP81302126A EP0040927A1 EP 0040927 A1 EP0040927 A1 EP 0040927A1 EP 81302126 A EP81302126 A EP 81302126A EP 81302126 A EP81302126 A EP 81302126A EP 0040927 A1 EP0040927 A1 EP 0040927A1
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EP
European Patent Office
Prior art keywords
liquid
air
curtain
moving surface
velocity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP81302126A
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German (de)
English (en)
Other versions
EP0040927B1 (fr
Inventor
Imants Reba
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
James River Corp of Nevada
Original Assignee
Crown Zellerbach Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Crown Zellerbach Corp filed Critical Crown Zellerbach Corp
Priority to AT81302126T priority Critical patent/ATE10261T1/de
Publication of EP0040927A1 publication Critical patent/EP0040927A1/fr
Application granted granted Critical
Publication of EP0040927B1 publication Critical patent/EP0040927B1/fr
Expired legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00—Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02—Spray pistols; Apparatus for discharge
    • B05B7/08—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point
    • B05B7/0807—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point to form intersecting jets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00—Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02—Spray pistols; Apparatus for discharge
    • B05B7/08—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point
    • B05B7/0884—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point the outlet orifices for jets constituted by a liquid or a mixture containing a liquid being aligned
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21G—CALENDERS; ACCESSORIES FOR PAPER-MAKING MACHINES
    • D21G7/00—Damping devices

Definitions

  • This invention relates to a method of and a system for producing a continuous liquid spray curtain capable of uniformly covering essentially the entirety of a moving surface, without substantial streaking thereof.
  • Prior art systems have been provided for spraying a liquid onto a moving surface.
  • a plurality of hydraulic nozzles can be employed for liquid spraying, the number of nozzles employed being determined by the width of the surface to be sprayed.
  • hydraulic nozzles emit a spray in a circular or elliptical pattern. This causes nonuniform coverage of the moving surface because the respective sprays emanating from adjacent hydraulic nozzles are difficult to interface one with the other over the entire width of the moving surface. Thus, streaking results due to these respective oversprayed or undersprayed areas.
  • Streaking is a particular problem in certain applications, such as, for example, spraying a creping adhesive onto a cellulosic web, or onto a thermal drying cylinder, since nonuniform adhesion of the web to the thermal drying cylinder results in a nonuniformly creped sheet having substandard physical properties. Furthermore, the dried, creped web will not wind evenly into a parent roll on the'papermaking reel if creping is nonuniform. This will lead to substantial problems when the parent roll is converted to product.
  • the exit velocity of the liquid in a hydraulic nozzle system determines the requisite degree of atomization of the liquid.
  • the liquid exit velocity is relatively high.
  • the exit velocity is primarily a function of the liquid supply pressure. A high liquid supply pressure presents severe operating hazards to equipment and personnel.
  • sonic nozzles typically spray particles of a smaller, more uniform size particle distribution than those produced by hydraulic spraying.
  • One of the major problems which can result from the use of a plurality of sonic nozzles for spraying onto a moving surface is that the finer the spray which is produced, the lower the momentum of the spray particles. This, in turn, reduces the effect of penetration by the spray particles of the boundary air layer between the nozzle and the moving surface, resulting in a significantly higher level of spray migration and a lower solids addition to the moving surface.
  • the same coverage problems associated with hydraulic nozzles are present herein because of the circular spray patterns produced by each adjacent sonic nozzle.
  • the sonic nozzles exhibit plugging problems similar to those described above for hydraulic nozzles.
  • U.S. Patent 1,888,791 describes an apparatus which discharges liquids through jets.
  • the discharge liquid intersects air streams outside the discharge orifices at a substantially maximum angle with respect to the central axis of the liquid jets so that the air streams impede the progress of the liquid jet flow and creates a back-pressure.
  • Any change in the air velocity or impingement angle will change the back-pressure.
  • any increase in the back-pressure such as caused by an increase in the air velocity, will result in a decrease in both the liquid velocity and in the amount of liquid sprayed.
  • a nonuniform moisture profile typically exists in which the edges of the webs are much drier than the central portion. Coverage of these webs with moisturizing liquids to a desired moisture level can be accomplished by the addition of water to increase the moisture level at the edges of the web.
  • Some prior art systems, such as sonic nozzles attempt to correct this problem by changing the flow rates of a plurality of individual.sonic nozzles in a given system so as to alter the moisture profile of the web. Instead, the system provides a random, nonuniform, uncoordinated spray pattern.
  • the above described problems associated with prior art systems have been overcome by the method of the present invention.
  • the subject method provides an essentially continuous liquid spray curtain capable of uniformly covering essentially the entirety of a moving web without substantial streaking thereof.
  • the liquid spray curtain is produced by discharging a plurality of streams of liquid to be sprayed from a discharge means at a relatively low discharge velocity.
  • a continuous, high velocity air curtain is also discharged which is directed toward the liquid streams and contacts same at a minimum contact angle ⁇ , measured from the center line of said liquid discharge means, of from about -10°, and preferably from about -5°, up to about +30°, and more preferably up to about+l0°.
  • the liquid velocity is substantially increased and the liquid is atomized, thereby forming a high velocity, continuous, uniform liquid spray curtain.
  • the high velocity liquid spray curtain exhibits a relatively high boundary layer penetration level in a controlled, extensive particle range. Accordingly, essentially the entire moving surface is covered with the liquid spray in a uniform manner, and without substantial interfacing or streaking problems, as previously described.
  • Spraying of a relatively high total solids liquid can be accomplished when the process of this invention is employed without the problems associated with the prior art.
  • the total liquid flow rate can be decreased at a given total solids level. This will, in turn, decrease the total water consumption and the thermal drying costs associated with the prior art solution levels.
  • the total amount of liquid sprayed on the moving surface in the method of the present invention is preferably only up to about 50%, and more preferably up to about 25%, as compared to hydraulic nozzles at the same total solids level.
  • the use of a higher total solids liquid results, to a great degree, from the subject liquid discharge means having a substantially higher total cross-sectional flow area per unit length (A.) than that of a comparable hydraulic discharge means (A h ).
  • the ratio of A X :A h at a given total solids flow rate is generally at least about 30, and preferably at least about 60, and more preferably at least about 120.
  • the liquid discharge velocity for the method of the present invention is relatively low and preferably is not greater than about 20 feet per second (6 metres/sec), and more preferably not greater than about 5 feet per second (1.5 metres/sec), and most preferably not more than about 2 feet per second (0.6 metres/sec). This is in total contradistinction to the aforementioned prior art methods which employ substantially high liquid flow velocities to overcome an impeding air flow and, in the case of the hydraulic and sonic nozzles, for overcoming the air boundary layer between the system and the surface.
  • the discharge velocity of the air curtain is preferably at least about 600 feet per second (180 metres/sec.), and more preferably at least about 1,000 feet per second (300 metres/sec.), and most preferably at least about 1,200 feet per second (365 metres/sec.). Furthermore, the respective liquid and air velocities are maintained so that substantial atomization of the liquid will result.
  • Moving surfaces of differing widths can be effectively sprayed by employing the method of this invention.
  • accurate, controlled, uniform coverage, especially at the surface edges, is difficult to maintain since the spray pattern produced by these prior systems is discontinuous.
  • the present method provides for readily adjusting the width of the continuous spray curtain, depending on the width of the moving surface to be sprayed. This is done by closing off or opening, in a controlled manner, only the outer-most liquid sprays so that the width of the curtain will correspond to the width of the moving surface. Such an adjustment can be made to quite a narrow tolerance range since the liquid discharge means are in close proximity one to the other.
  • each liquid header system includes labyrinth means which internally meters and longitudinally distributes the liquid flow, causing a constant span-wise pressure or static head to be maintained in a liquid reservoir which extends across the entire longitudinal distance of the discharge means.
  • labyrinth means which internally meters and longitudinally distributes the liquid flow, causing a constant span-wise pressure or static head to be maintained in a liquid reservoir which extends across the entire longitudinal distance of the discharge means. The presence of this liquid reservoir ensures that a constant, static liquid head will be maintained at the discharge means and that the liquid spray curtain will therefore operate at steady-state conditions.
  • Certain moving surfaces such as cellulosic webs on a paper machine, have a substantially nonuniform moisture profile, i.e., the moisture level is substantially lower at the edges than at the center.
  • the previously described conventional systems are not capable of effectively controlling the spray from both a quality and quantity standpoint so that the moisture profile of the web cannot be modified to the extent that it becomes uniform across the entire web surface.
  • an inverted moisture profile can be provided using the method of the present invention in which more moisture is sprayed at the edges of the moving surface than in the interior portion thereof while, at the same time, maintaining the same total amount of liquid spray addition.
  • Moisture profile measurement means can be provided for continuously monitoring the moisture profile of the web at a point upstream from the subject spray system. The flow rate can then be adjusted at various points in the individual liquid supply headers to compensate for these disparities.
  • a system 10 for producing a liquid spray curtain is generally depicted therein attached to and supported by a beam 70 and includes a liquid supply means 20 and an air supply means 40.
  • the liquid supply means in general, comprises at least one liquid supply header, in this case denoted "21" and “21 “', having a plurality of liquid supply lines 23 attached, at one end, thereto.
  • the liquid supply lines 23 are, at the other end, connected to a liquid supply conduit 22 which transports the liquid from a liquid storage means (not shown) employing a pump or other like means to provide the driving force for transporting the liquid.
  • Air supply means 40 comprises an air supply header 41 to which a plurality of air supply lines 61 are connected. At the other end, the air supply lines 61 are connected to air supply conduit 60 which transports air, under pressure, employing a compressor or like means to provide the driving force.
  • liquid supply headers 21 and 21' which discharge a plurality of liquid streams from discharge means 37 at a relatively low velocity, include inlet supply means 24 and 24' which supply-the appropriate liquid to supply chambers 25 and 25'.
  • liquid supply headers 21 and 21' are disposed at right angles one with respect to the other.
  • Liquid supply chambers 25 and 25' have located therewithin labyrinth means 26 and 26' for internally metering and longitudinally distributing the liquid flow.
  • labyrinth means 26 and 26' comprise, preferably, first compartments 27 and 27', in which the liquid is initially collected, the liquid being restrained from flowing freely by first barrier means 29 and 29'.
  • Liquid supply orifices 30 and 30' are also provided which permit a reduced flow of liquid to the second compartment 28 and 28', where the liquid is again collected.
  • the flow is restricted in this case by second barrier means 31 and 31'.
  • the liquid then moves to a liquid reservoir means 33 and 33' from labyrinth means 26 and 26', respectively, through liquid supply slots 32 and 32' in the respective second barrier means 31 and 31'.
  • discharge means 37 having an exit orifice 37', which is adapted for liquid communication with said reservoir, to provide a continuous, uniform flow rate of liquid.
  • liquid flow tubes 38 and 38' (in phantom), having exit orifices 39 and 39', are preferably disposed within discharge means 37 for further controlling the discharge of the liquid.
  • the discharge means 37 preferably has a narrowed end section 36 which provides, if necessary, means for readily maintaining liquid flow tubes 38 and 38' in proper position and alignment.
  • liquid flow tubes 38 and 38' are preferably in individual and alternative communication with the liquid in a pair of liquid supply headers 21 and 21', respectively. This permits a more controlled liquid flow and allows the system to continue in operation even if one of the headers requires maintenance.
  • air supply means 40 comprises an air supply header 41, which discharges a continuous, high velocity air curtain, from exit air slit 50, for contact with said liquid streams, as hereinafter provided.
  • the air supply header 41 includes means denoted "43" and "51” for adjusting the respective magnitudes of the exit air slit 50 and the air contact angle ⁇ , as hereinafter described.
  • Exit air slit 50 is preferably continuous along the entire longitudinal extent of the system 10.
  • Air supply chamber 49 is formed within the confines of said air supply header 41 and converges at its outermost end to form a continuous exit air slit 50.
  • the header 41 comprises a first sidewall member 46, a pair of endwall members 45 (only one shown), and a floor member 47, respectively, joined one to the other, and a second sidewall member 42 adapted for movement to a plurality of positions with respect to said first sidewall member 46.
  • the supply pressure of the air in conduit 60 substantially controls the velocity of the air being emitted from air slit 50.
  • the air supply pressure in conduit 60 is maintained at from about 5 psig (0.35 kgs/cm 2 ), up to about 40 psig (2.8 kgs/cm 2 ), and more preferably from about 10 psig (0.7 kgs/cm 2 ), up to about 25 psig (1.75 kgs/cm 2 ).
  • the quantity of air emitted from exit air slit 50 is controlled by the magnitude of the opening of slit 50.
  • the quantity of air emitted from slit 50 controls the penetration of the liquid spray curtain with respect to the boundary air layer.
  • the magnitude of slit 50 is chosen depending on the viscosity and quantity of the spray liquid, the distance from the spray exit to the moving surface, and the velocity of the moving surface.
  • the magnitude of exit air slit 50 is maintained at a slit opening of from about 0.002 inch (0.005 cm), up to about 1.010 inch (0.025 cm), and more preferably from about 0.003 inch (0.0076 cm), up to about 0.006 inch (0.015 cm).
  • second sidewall member 42 With respect to first sidewall member 46, depends upon air slit adjustment means 43, such as nut-and-bolt arrangement 43a' passing through bracing member 43b.
  • Bracing member 43b is connected to air supply header 41 by attachment means 43c, which, in this case, is a nut-and-bolt assembly.
  • An air flow guide means 48 is located at the outermost end of first sidewall member 46.
  • Guide means 48 is disposed with respect to the center line 37a of liquid discharge means 37 such that when said second sidewall member 42 is positioned with respect to air guide means 48, a high velocity, continuous air curtain is discharged from said exit slit which will contact said liquid streams at the previously described minimum contact angle.
  • air flow guide means 48 is disposed parallel to the center line of said liquid discharge means 37.
  • adjustment means 51 which is preferably a screw arrangement. As shown in Figure 2, adjustment means 51 is connected to bracing member 43b and air supply header 41, respectively.
  • Means 44 is preferably in the form of screen means which modifies the inlet air so that it assumes a uniform span-wise pressure distribution and a uniform exit velocity.
  • the liquid spray curtain 16 which is emitted is capable of uniformly covering essentially the entirety of the moving surface.
  • the liquid spray curtain 16 is formed by discharging a plurality of liquid streams from discharge means 37 and, in this case, through liquid flow tubes 38 and 38', at low discharge velocity.
  • the continuous air curtain is discharged from air slit 50, and is directed toward the discharging liquid streams emanating from discharge means 37.
  • a high velocity, continuous, uniform liquid spray curtain 16 (not shown) is formed, without impeding the liquid flow, but, contrarily, the liquid velocity, after the liquid exits from the orifices, is substantially increased, causing atomization of the liquid.
  • Curtain 16 exhibits a high boundary layer penetration level over a controlled, extensive particle size range without causing substantial streaking when sprayed onto a moving surface, and without exhibiting interfacing problems between the respective spray streams.
  • the total amount of liquid 15 being discharged from liquid discharge means 37 can be substantially lower than for the same liquid, at the same total solids level, employing, for example, a hydraulic nozzle system.
  • the use of a lower amount of liquid results to a large extent from the use of a larger number of individual discharge means 37, preferably including liquid flow tubes 38 and 38', having a relatively large total cross-sectional flow area per unit length of said header means 21 and 21', i.e., A , and a lower solution velocity.
  • the preferred A x of the discharge orifice 37' is from about 0.01 square inch per foot (0.02 cm 2 /metre) to about 0.09 square inch per foot (0.18 cm 2 /metre), and more preferably from about 0.02 square inch per foot (0.04 cm 2 /metre) to about 0.06 square inch per foot (0.12 cm 2 /metre).
  • a critical feature of this invention is the minimum contact angle 3 at which a continuous, high velocity air curtain is directed with respect to the liquid 15 being discharged at low velocity from discharge means 37.
  • the method of the present invention provides that a continuous air curtain contacts the liquid at an angle which will impel the liquid at a high velocity and will form a continuous, uniform liquid spray curtain having a relatively high boundary layer penetration level over a controlled, extensive particle- size range.
  • the minimum contact angle is preferably controlled, as in Figure 2, by air flow guide means 48 disposed in a plane substantially parallel to the center line 37a of discharge means 37.
  • the air flow guide means in conjunction with movable sidewall means 42a, adjust to cause the air to be discharged so as to produce the requisite minimum contact angles previously described.
  • a continuous, uniform, low velocity liquid stream is emitted from discharge means 37 due, to the most part, to the maintenance of a positive static pressure head on said discharge means.
  • the static head on discharge means 37 is, in turn, maintained by the positive static pressure within liquid reservoir 33. More specifically, by employing a liquid reservoir which extends below the entire extent of the inlet portions of discharge means 37, the reservoir 33 is substantially filled with liquid under pressure, and all of the discharge means 37 will, in turn, be filled with liquid under pressure, which will result in the uniform, continuous discharge of said liquid from said discharge means.
  • the positive pressure which is maintained in the liquid reservoir 33 is a direct consequence of labyrinths 26 and 26' which internally meter the liquid flow and facilitate the liquid communication from liquid reservoir 33 to discharge means 37.
  • Longitudinal extent of the liquid spray curtain can be adjusted, depending on the width of the moving surface to be sprayed, by providing, such as by inserting within discharge means 37, or by substituting for liquid flow tubes 38 and 38' which are hollow in construction, means for plugging said liquid streams, at points beyond the width of the moving surface, so that the liquid 15 cannot'pass therethrough.
  • the moisture profile of a moving surface having a lower moisture content at its edges than at its central portion can be adjusted employing the present system.
  • a means can be provided for measuring the moisture profile of the moving surface at a point prior to the subject linear nozzle system.
  • the liquid flow rate to the innermost points in the respective headers is reduced, thereby producing a liquid spray curtain having a moisture profile in which the outer edges of the moving surface are moisturized to a much greater extent than the central portion thereof, and a moisture profile results.
  • the spray liquid 15 can comprise any liquid material which can be effectively discharged from discharge means 37 without causing substantial plugging thereof.
  • the magnitude of the liquid materials which can be employed is far more substantial than those liquids which can be sprayed from hydraulic and sonic systems.
  • the present method requires only a low exit velocity and the area of liquid flow is substantially greater than in the previously described prior art systems.
  • various aqueous liquid solutions are employed as the liquid 15. Water, itself, can also be sprayed on a moving surface in order to moisturize the same, as described above.
  • a liquid adhesive solution can be sprayed on a cellulosic papermaking web, and after being sprayed with the subject liquid spray curtain, the web can be adhered to a thermal drying cylinder and then uniformly creped to produce a soft, bulky cellulosic web product. Furthermore, this same liquid spray curtain can also be sprayed directly onto a moving surface crossing the thermal drying cylinder.
  • Typical creping adhesives include various natural and synthetic materials which are well-known in the papermaking art. Exemplary materials include carboxymethyl cellulose, polyvinyl alcohol and animal glue.

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  • Paper (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Coating Apparatus (AREA)
EP81302126A 1980-05-19 1981-05-13 Système de production d'un rideau de liquide pulvérisé pour l'application sur une bande en mouvement Expired EP0040927B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT81302126T ATE10261T1 (de) 1980-05-19 1981-05-13 System zum erzeugen eines vorhangfoermigen fluessigkeitsspruehstrahls zum auftragen auf laufende bahnen.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US15102380A 1980-05-19 1980-05-19
US151023 1980-05-19

Publications (2)

Publication Number Publication Date
EP0040927A1 true EP0040927A1 (fr) 1981-12-02
EP0040927B1 EP0040927B1 (fr) 1984-11-14

Family

ID=22537014

Family Applications (1)

Application Number Title Priority Date Filing Date
EP81302126A Expired EP0040927B1 (fr) 1980-05-19 1981-05-13 Système de production d'un rideau de liquide pulvérisé pour l'application sur une bande en mouvement

Country Status (6)

Country Link
EP (1) EP0040927B1 (fr)
JP (1) JPS57500636A (fr)
AT (1) ATE10261T1 (fr)
CA (1) CA1174530A (fr)
DE (1) DE3167158D1 (fr)
WO (1) WO1981003372A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0498600A1 (fr) * 1991-02-06 1992-08-12 Minnesota Mining And Manufacturing Company Unité de pulvérisation pour former des jets en éventail
WO1997011783A1 (fr) * 1995-09-27 1997-04-03 Glaxo Group Limited Buse d'atomisation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1888791A (en) * 1930-09-27 1932-11-22 Harry C Cole Spraying method and machine
US3750955A (en) * 1971-09-10 1973-08-07 Honshu Paper Co Ltd Spray coating apparatus
US4072772A (en) * 1973-08-09 1978-02-07 Ppg Industries, Inc. Linear curtain spray applicator

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US958999A (en) * 1909-12-16 1910-05-24 Oscar Fordice Hydrocarbon-burner.
JPS516362A (en) * 1974-07-05 1976-01-19 Hitachi Plant Eng & Constr Co Gesuiodeitono kyokyusochi

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1888791A (en) * 1930-09-27 1932-11-22 Harry C Cole Spraying method and machine
US3750955A (en) * 1971-09-10 1973-08-07 Honshu Paper Co Ltd Spray coating apparatus
US4072772A (en) * 1973-08-09 1978-02-07 Ppg Industries, Inc. Linear curtain spray applicator

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0498600A1 (fr) * 1991-02-06 1992-08-12 Minnesota Mining And Manufacturing Company Unité de pulvérisation pour former des jets en éventail
WO1997011783A1 (fr) * 1995-09-27 1997-04-03 Glaxo Group Limited Buse d'atomisation
US5996576A (en) * 1995-09-27 1999-12-07 Glaxo Group Limited Atomising nozzle

Also Published As

Publication number Publication date
DE3167158D1 (en) 1984-12-20
CA1174530A (fr) 1984-09-18
ATE10261T1 (de) 1984-11-15
WO1981003372A1 (fr) 1981-11-26
JPS57500636A (fr) 1982-04-15
EP0040927B1 (fr) 1984-11-14

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